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1. 发明授权

US3644513A Polyfluoroisoalkoxyalkyl amido carboxylic acids and salts thereof 失效
标题翻译：聚氟代羟基烷基氨基羧酸及其盐
公开(公告)号：US3644513A
公开(公告)日：1972-02-22
申请号：US3644513D
申请日：1969-04-23
申请人： ALLIED CHEM
发明人： SWEENEY RICHARD F , PRICE ALSON K , KHAN AZIZ U
IPC分类号： A62D1/00 , C07C235/12 , C08K5/20 , C07C101/10 , C07F1/00
CPC分类号： A62D1/0014 , C07C235/12 , C08K5/20
摘要： POLYFLUOROISOALKOXYALKYL AMIDO CARBOXYLIC ACIDS OF THE FORMULA:

R1-CF(-R2)-CF(-CF(-R3)-R4)-O-R-CO-N(-R5)-R6-COOH

WHEREIN R1-R4 ARE EACH INDEPENDENTLY SELECTED FROM THE GROUP CONSISTING OF F, CL, ALKYL AND HALOALKYL GROUPS IN WHICH THE HALOGEN ATOMS ARE CL OR F; R1 AND R4 WHEN TAKEN TOGETHER ARE ALKYLENE OR HALOALKYLENE GROUPS WHICH FORM, WITH THE CARBON CHAIN THEREBETWEEN, A CYCLIC STRUCTURE; R IS A MEMBER SELECTED FROM THE GROUP CONSISTING OF ALKYLENE AND HALOALKYLENE; R5 IS A MEMBER SELECTED FROM THE GROUP CONSISTING OF HYDROGEN AND ALKYL, AND R6 IS A MEMBER SELECTED FROM THE GROUP CONSISTING OF ALKYLENE, MONOHYDROXYALKYLENE AND CARBOXYALKYLENE RADICALS; AND SALTS THEREOF CONTAINING A CATION SELECTED FROM THE GROUP CONSISTING OF LI, NA, K, RB, CS, CA, BA, MG, ZN, HG, AL, CR, SN, FE, AG, CU, CO, ZR, PB, MN, OR A RADICAL SELECTED FROM MORPHOLINO, AMMONIUM OR AN ALKYL OR HYDROXYALKYL SUBSTITUTED AMMONIUM RADICAL. PREPARATION BY REACTING CORRESPONDING POLYFLUOROISOALKOXYALKYL AMIDO CARBOXYLIC ACID FLUORIDES OR HALOSULFATES WITH AMINO ACIDS. THE NOVEL COMPOUNDS ARE USEFUL AS EMULSIFYING AGENTS, LEVELING AGENTS, OIL, STAIN AND WATER REPELLENT AGENTS, ADDITIVES TO DRY POWDER FIRE EXTINGUSHING COMPOSITIONS AND AS INTERMEDIATES TO VALUABLE OIL, STAIN AND WATER REPELLENT AGENTS.

2. 发明授权

US3560527A Beta-lactones of (1-hydroxyperfluorocycloalkyl) acetic acids and preparation thereof 失效
标题翻译：（1-羟基吡咯烷酮基）乙酸及其制备方法的试验
公开(公告)号：US3560527A
公开(公告)日：1971-02-02
申请号：US3560527D
申请日：1967-08-09
申请人： ALLIED CHEM
发明人： SWEENEY RICHARD F , PRICE ALSON K
IPC分类号： C07D305/14 , C07D3/00
CPC分类号： C07D305/14
摘要： FLUORINATED LACTONES HAVING THE FORMULA:

4,4-(-CF2-CF2-CNF2N-CF2-)OXETAN-2-ONE

WHEREIN N MAY BE 0-2 ARE PREPARED BY DEHYDRATING A CORRESPONDING (1-HYDROXYPERFLUOROCYCLOALKYL) ACETIC ACID HAVING THE FORMULA

HOOC-CH2-C(-OH)
WITH PHOSPHORUS PENTOXIDE. THE FLUORINATED LACTONES MAY ALSO BE PREPARED BY HEATING A CORRESPONDING ACID CHLORIDE OF THE ABOVE-DESCRIBED ACIDS TO DECOMPOSITION, OR BY HEATING A MIXTURE OF SUCH AN ACID WITH THIONYL CHLORIDE, IN THE PRESENCE OF AN ORGANIC TERTIARY AMINE CATALYST, FOR A PERIOD OF TIME, AND AT A SUFFICIENTLY HIGH TEMPERATURE, TO FORM THE CORRESPONDING SUBJECT FLUORINATED LACTONE. THE FLUORINATED LACTONES MAY BE CONVERTED TO SURFACE ACTIVE UNSATURATED ACIDS BY REACTION WITH ANHYDROUS SULFURIC ACID.

3. 发明授权

US3651069A Fluorocarbon derivatives 失效
标题翻译：氟代衍生物
公开(公告)号：US3651069A
公开(公告)日：1972-03-21
申请号：US3651069D
申请日：1968-08-01
申请人： ALLIED CHEM
发明人： SWEENEY RICHARD F , PRICE ALSON K
IPC分类号： D06M13/408 , C07D31/48
CPC分类号： D06M13/408
摘要： FLUORINATED QUARTERNARY AMMONIUM SALTS HAVING THE FORMULA

(RF-CO-NH-(CXH2X-N(-Z''))Y-CXH2X-NH-Z)Q(+).(Q/R)X R(-)

WHEREIN X AND Y ARE INTEGERS FROM 2 TO 6 AND 1 TO 4, RESPECTIVELY; RF IS A PERFLUOROALKYL OR A FLUORINATED ISOALKOXYALKYL RADICAL; Z IS H, A FLUORINATED ACYL RADICAL RFCO- WHEREIN RF IS AS DESCRIBED ABOVE, A VINYL SULFONE RADICAL OR A SULFONE-TERTIARY AMINE ADDUCT RADICAL; Z'' IS H, A FLUORINATED ACYL RADICAL RFCO- WHEREIN RF IS AS DESCRIBED ABOVE, A VINYL SULFONE RADICAL, A SULFONE-TERTIARY AMINE ADDUCT RADICAL, OR A -CXH2X-NHZ RADICAL WHEREIN X AND Z HAVE THE ABOVE MEANING, THERE BEING AT LEAST ONE FLUORINATED ACYL RADICAL AND ONE SULFONE-TERTIARY AMINE ADDUCT RADICAL IN THE MOLECULE REPRESENTED BY Z AND Z''; X IS AN ANION OF A SALT-FORMING ACID; Q IS AN INTEGER CORRESPONDING TO THE NUMBER OF SULFONE-TERTIARY AMINE ADDUCT RADICALS IN THE MOLECULE; AND R IS AN INTEGER CORRESPONDING TO THE VALENCY OF X. THESE SALTS ARE WATER- AND/OR OIL REPELLENCY AGENTS FOR MATERIALS SUCH AS TEXTILES AND PAPER.

4. 发明授权

US3576018A Acrylyl derivatives of fluorinated amides 失效
标题翻译：氟化物衍生物
公开(公告)号：US3576018A
公开(公告)日：1971-04-20
申请号：US3576018D
申请日：1968-08-01
申请人： ALLIED CHEM
发明人： SWEENEY RICHARD F , PRICE ALSON K
IPC分类号： D06M13/402 , D06M13/408 , C09F7/00
CPC分类号： D06M13/408 , D06M13/402
摘要： WHEREIN X AND Y ARE INTEGERS FROM 2 TO 6 AND 1 TO 4, RESPECTIVELY; WHEREIN RF IS A PERFLUOROALKYL OR A FLUORINATED ISOALKOXYALKYL RADICAL; Z IS H, ALKYL, HYDROXYALKY, A FLUORINATED ACYL RADICAL RFCO- WHEREIN RF IS AS DESCRIBED ABOVE, OR AN ACRYLYL RADICAL; Z'' IS H, ALKYL, HYDROXYALKY, A FLUORINATED ACYL RADICAL RFCO- WHEREIN RF IS AS DESCRIBED ABOVE, AN ACRYLYL RADICAL OR A RADICAL HAVING THE FORMULA -CXH2XNHZ WHEREIN Z IS AS DESCRIBED ABOVE, THERE BEING AT LEAST ONE FLUORINATED ACYL RADICAL RFCO- AND AT LEAST ONE ACRYLYL RADICAL IN THE MOLECULE REPRESENTED BY Z AND/OR Z''.

RF-CO-NH-(CXH2X-N(-Z''))Y-CXH2X-NH-Z

ACRYLYL DERIVATIVES OF FLUORINATED AMIDES USEFUL AS OILAND WATER-REPELLENCY AGENTS HAVE THE STRUCTURAL FORMULA

5. 发明授权

US3427349A 1-hydroxyperfluorocyclo alkyl acetic acid and corresponding chlorides 失效
标题翻译： 1-羟基吡咯烷酮酸乙酸和相应的氯化物
公开(公告)号：US3427349A
公开(公告)日：1969-02-11
申请号：US3427349D
申请日：1966-02-09
申请人： ALLIED CHEM
发明人： PRICE ALSON K , SWEENEY RICHARD F
IPC分类号： B29C65/00 , C07C61/32 , A61K27/00
CPC分类号： B29C66/00 , B29C65/02 , B29C65/38 , B29C66/919 , B29C66/929 , B29C66/949

6. 发明授权

US3674800A Derivatives pyridinium of polyfluoroisoalkoxyalkanamides 失效
标题翻译：衍生物聚氟代烷氧基胺的吡啶
公开(公告)号：US3674800A
公开(公告)日：1972-07-04
申请号：US3674800D
申请日：1969-04-14
申请人： ALLIED CHEM
发明人： SWEENEY RICHARD F , KHAN AZIZ URREHMAN , PRICE ALSON K , JONES EDWARD STEPHEN , OTTO JULIAN A
IPC分类号： C07C51/09 , C07C51/58 , C07C51/60 , C07C59/135 , C07C335/32 , C07D213/20 , C07D215/10 , D06M13/322 , D06M13/35 , D06M13/402 , D06M13/432 , C07D31/44
CPC分类号： C07D213/20 , C07C51/09 , C07C51/58 , C07C51/60 , C07C59/135 , C07C335/32 , C07D215/10 , D06M13/322 , D06M13/35 , D06M13/402 , D06M13/432
摘要： N-methylol and N-halomethyl derivatives of polyfluoroisoalkoxyalkanamides, and their substituted ammonium salts characterized in that an ether oxygen links a fluorinated carbon atom attached to two fluoroalkyl groups and at least one CF2- group. These compounds are useful as water and oil repellency agents.

7. 发明授权

US3651105A Chromium complexes of fluoroisoalkoxyalkyl carboxylic acids 失效
公开(公告)号：US3651105A
公开(公告)日：1972-03-21
申请号：US3651105D
申请日：1968-11-01
申请人： ALLIED CHEM
发明人： ANELLO LOUIS G , BOGHOSIAN EDWARD MICHAEL , JONES EDWARD S , MINHAS PRITAM S , PRICE ALSON K , SWEENEY RICHARD F
IPC分类号： C07C51/16 , C07F11/00 , C08H17/36
CPC分类号： C10M3/00 , C07C51/16 , C07F11/005 , C10M2227/09 , C10N2210/06 , C07C59/135
摘要： CHROMIUM COMPLEXES OF FLUOROCARBON CARBOXYLIC ACIDS CHARACTERIZED BY HAVING A POLYFLUOROISOALKOXYALKYL TAIL WHEREIN AN ETHER OXYGEN ATOM LINKS A FLUORINATED CARBON ATOM CONNECTED TO TWO FLUOROALKYL GROUPS AND AT LEAST ONE -CF2CF2-GROUP. THESE CHROMIUM COMPLEXES ARE USEFUL TO IMPART OIL AND WATER RESISTANCE TO VARIOUS SUBSTRATES, INCLUDING PAPER, LEATHER, AND THE LIKE.

8. 发明授权

US3577447A Alkanoyl derivatives of fluorinated amides 失效
标题翻译：氟化物的烷基衍生物
公开(公告)号：US3577447A
公开(公告)日：1971-05-04
申请号：US3577447D
申请日：1968-08-01
申请人： ALLIED CHEM
发明人： SWEENEY RICHARD F , PRICE ALSON K
IPC分类号： D21H17/07 , C09F7/00
CPC分类号： D21H17/07
摘要： ALKANOYL DERIVATIVES OF FLUORINATED AMIDES USEFUL AS OIL-REPELLENCY AGENTS HAVE THE STRUCTURAL FORMULA

RF-CO-NH-(CXH2X-N(-Z''))Y-CXH2X-NH-Z

WHEREIN X AND Y ARE INTEGERS FROM 2 TO 6 AND 1 TO 4 RESPECTIVELY; WHEREIN RF IS A PERFLUOROALKYL OR A FLUORINATED ISOLALKOXYALKYL RADICAL; Z IS H, ALKYL, HYDROXYALKYL, A FLUORINATED ACYL RADICAL RFCO-WHEREIN RF IS AS DESCRIBED ABOVE, OR A HYDROCARBON ACYL RADICAL; Z'' IS H, ALKYL, HYDROXYALKYL, A FLUOROINATED ACYL RADICAL RFCO- WHEREIN RF IS AS DESCRIBED ABOVE, A HYDROCARBON ACYL RADICAL OR A RADICAL OF THE FORMULA-CXH2XNHZ WHEREIN X AND Z ARE AS DESCRIBED ABOVE, THERE BEING AT LEAST ONE FLUORINATED ACYL RADICAL RFCO-AND AT LEAST ONE HYDROCARBON ACYL RADICAL IN THE MOLECULE REPRESENTED BY Z AND/OR Z''.

9. 发明授权

US3553250A Novel fluorinated acids and derivatives thereof 失效
标题翻译：新鲜氟化物及其衍生物
公开(公告)号：US3553250A
公开(公告)日：1971-01-05
申请号：US3553250D
申请日：1967-08-09
申请人： ALLIED CHEM
发明人： SWEENEY RICHARD F , PRICE ALSON K
IPC分类号： C07C61/16 , C07C69/74
CPC分类号： C07C2601/08
摘要： NOVEL PERFLUOROCYCLOALKYLIDENYL COMPOUNDS OF THE FORMULA:

X-CO-CH=C
WHEREIN N MAY BE 0-2 AND MAY BE OH, F, CL, OALKYL, OCYCLOALKYL, OR OM, WHEREIN M IS AN ALKALI METAL, ALKALINE EARTH METAL, OR-NH4, MAY BE DERIVED FROM THE CORRESPONDING (1-HYDROXYPERFLUOROCYCLOALKYL) ACETIC ACIDS OF THE FORMULA:

HOOC-CH2-C(-OH)
PERFLUOROCYCLOALKYLIDENYL COMPOUNDS OF THE ABOVE FORMULA WHEREIN X IS OH MAY BE PREPARED FROM THE CORRESPONDING (1 - HYDROXYPERFLUOROCYCLOALKYL) ACETIC ACIDS BY REACTING THE LATTER WITH CONCENTRATED (100%) H2SO4. THE RESULTING ACIDS MAY BE CONVERTED INTO THE CORRESPONDING ACID CHLORIDES, WHEREIN X IN THE ABOVE FORMULA IS CL, BY REACTION WITH BENZOTRICHLORIDE OR INTO THE CORRESPONDING ACID FLUORIDES, WHEREIN X IN THE ABOVE FORMULA IF F, BY REACTION WITH THIONYL CHLORIDE IN THE PRESENCE OF AN ORGANIC TERTIARY AMINE CATALYST SUCH AS PYRIDINE. THE CORRESPONDING ESTERS, WHEREIN X IN THE ABOVE FORMULA IS OALKYL OR OCYCLOALKYL, MAY BE PREPARED FROM EITHER OF THE ACID HALIDES BY REACTION OF THE LATTER WITH AN ALKANOL OR CYCLOALKANOL. THE ESTERS MAY ALSO BE PREPARED FROM PERFLUOROCYCLOALKANONES BY A WITTIG REACTION. SALTS OF THE ACIDS, WHEREIN X IN THE ABOVE FORMULA IS OM, MAY BE PREPARED BY REACTING THE ACIDS WITH AN ALKALI METAL OR ALKALINE EARTH METAL HYDROXIDE OR WITH AMMONIUM HYDROXIDE. THE PERFLUOROCYCLOALKYLIDENYL ACIDS AND SALTS THEREOF ARE USEFUL SURFACE ACTIVE AGENTS. ANY OF THE NOVEL COMPOUNDS WHEREIN X IS F, CL, OALKYL OR OCYCLOALKYL CAN BE CONVERTED TO THE CORRESPONDING ACIDS OR ACID SALTS.

10. 发明授权

US3674798A Polyfluoroisoalkoxyalkyl pyridinium salts 失效
标题翻译：聚氟代羟基烷基吡啶盐
公开(公告)号：US3674798A
公开(公告)日：1972-07-04
申请号：US3674798D
申请日：1969-12-15
申请人： ALLIED CHEM
发明人： PRICE ALSON K , SUKORNICK BERNARD
IPC分类号： C07C335/32 , C07D213/20 , D06M13/35 , D06M13/432 , C07D31/28
CPC分类号： C07D213/20 , C07C335/32 , D06M13/35 , D06M13/432
摘要： Compounds of the formula

WHEREIN R1-R4 are fluorine, chlorine or perhaloalkyl groups; X1X4 are hydrogen, halogen, or alkyl halide; Y is thiourea, pyridine, quinoline, or the alkyl or hydroxyalkyl derivatives thereof; A is an accompanying anionic moiety; r is an integer from 1-2, m and n are integers from 0-20, and s is an integer from 1 up to the total negative charge of A. These compounds are useful as surface active agents and for imparting water and oil repellent properties to various substrates such as textiles, leather and paper.

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