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1. 发明授权

US5220055A Process for producing aminocarboxylic acid salts 失效
标题翻译：生产氨基羧酸盐的方法
公开(公告)号：US5220055A
公开(公告)日：1993-06-15
申请号：US861893
申请日：1992-06-23
申请人： Yoshiaki Urano , Yukio Kadono , Takakiyo Goto
发明人： Yoshiaki Urano , Yukio Kadono , Takakiyo Goto
IPC分类号： B01J23/72 , B01J25/00 , B01J27/053 , B01J27/122 , B01J27/232 , B01J27/25 , B01J31/04 , C07B61/00 , C07C227/02 , C07C229/08 , C07C229/12 , C07C229/16
CPC分类号： B01J25/00 , B01J23/72 , C07C227/02
摘要： There is provided a novel process for producing aminocarboxylic acid salts useful as starting materials of agricultural chemicals and medicines, chelating agents, food additives, and so on. This process is characterized in that when producing an aminocarboxylic acid salt by an oxidative dehydrogenation reaction of an amino alcohol in the presence of an alkali metal hydroxide and/or an alkaline earth metal hydroxide, a copper-containing catalyst and water, the reaction is performed by adding an aluminum metal and/or an aluminum compound (e.g., sodium aluminate and aluminum hydroxide) to the reaction system.
摘要翻译： PCT No.PCT / JP91 / 01440 Sec。 371日期：1992年6月23日 102（e）日期1992年6月23日PCT 1991年10月21日PCT PCT。公开号WO92 / 06949 日期为1992年04月30日。提供了用作农药，螯合剂，食品添加剂等原料的氨基羧酸盐的新方法。该方法的特征在于，在碱金属氢氧化物和/或碱土金属氢氧化物，含铜催化剂和水的存在下，通过氨基醇的氧化脱氢反应制备氨基羧酸盐时，进行反应通过向反应体系中加入铝金属和/或铝化合物（例如铝酸钠和氢氧化铝）。

2. 发明授权

US06278007B1 (Poly)alkylene glycol higher alkyl ether derivative composition and detergent, lubricant, and dermatologic medicine for external use containing the composition 失效
标题翻译：（聚）亚烷基二醇高级烷基醚衍生物组合物和洗涤剂，润滑剂和皮肤外用药物，含有组合物
公开(公告)号：US06278007B1
公开(公告)日：2001-08-21
申请号：US09309011
申请日：1999-05-10
申请人： Toru Inaoka , Kenji Rakutani , Yukio Kadono , Yoshiyuki Onda
发明人： Toru Inaoka , Kenji Rakutani , Yukio Kadono , Yoshiyuki Onda
IPC分类号： C07B3508
CPC分类号： C10M105/18 , C07C43/11 , C07C69/003 , C07C69/24 , C08G65/2615 , C08G65/3312 , C10M105/40 , C10M107/34 , C10M2207/04 , C10M2207/289 , C10M2209/104 , C10M2209/105 , C10M2209/106 , C10M2209/109 , C11D1/72 , C11D1/721 , C11D1/74
摘要： A (poly)alkylene glycol higher alkyl ether derivative composition characterized by comprising 30-90 mol. % of (B1) (poly)alkylene glycol higher alkyl ether derivative and 70-10 mol. % of (B2) (poly)alkylene glycol higher alkyl ether derivative, respectively having a methyl group for R1 and an alkyl group of not less than two carbon atoms for R1 in the general formula (1) representing the derivatives: (wherein R1 and R2 represent alkyl groups whose total number of carbon atoms is in the range of 7-29, the number of carbon atoms of R2 is larger than the number of carbon atoms of R1, A represents a lower alkylene group, n represents a real number in the range of 1-300 on average, x represents 0 or 1, y represents a real number in the range of 1-10 on average, and R3 represents an optionally substituted organic residue of 1-60 carbon atoms [excluding the carbon atoms of the substituent]) and a deterging agent, a lubricating agent, or a dermatological medicine for external use containing the (poly)alkylene glycol higher alkyl ether derivative composition. The composition possesses such characteristic features as containing no oil-soluble component of low molecular weight, emitting odor sparingly, exhibiting a low stimulating property, having no foaming property, abounding in penetrating force, allowing thorough separation of the foam from a deterged article, and enjoying such low viscosity as to allow great ease of handling.
摘要翻译：（聚）亚烷基二醇高级烷基醚衍生物组合物，其特征在于包含30-90mol。（B1）（聚）亚烷基二醇高级烷基醚衍生物的百分比和70-10摩尔。％的（B2）（聚）亚烷基二醇高级烷基醚衍生物，在通式（1）中分别具有R1的甲基和不少于2个碳原子的烷基，其中R1和 R2表示碳原子数为7〜29的烷基，R2的碳原子数大于R1的碳原子数，A表示低级亚烷基，n表示实数平均1-300的范围，x表示0或1，y表示平均1-10个范围内的实数，R3表示1-60个碳原子的任选取代的有机残基[不包括取代基]）和含有（聚）亚烷基二醇高级烷基醚衍生物组合物的洗涤剂，润滑剂或外用皮肤病学药剂。该组合物具有如下特征：不含低分子量油溶性成分，少量发臭，表现出低刺激性，无起泡性，渗透力大，允许泡沫与洗涤物品彻底分离，享受这样的低粘度以使得易于处理。

3. 发明授权

US5026880A Method for production of 1,3-dioxolanes 失效
标题翻译： 1,3-二氧戊环的制备方法
公开(公告)号：US5026880A
公开(公告)日：1991-06-25
申请号：US564742
申请日：1990-08-09
申请人： Yoshiaki Urano , Yukio Kadono
发明人： Yoshiaki Urano , Yukio Kadono
IPC分类号： B01J27/08 , B01J27/138 , C07B61/00 , C07D317/12
CPC分类号： B01J27/08 , C07D317/12
摘要： A method for the production of a 1,3-dioxolane represented by the general formula III: ##STR1## wherein R.sup.1 is hydrogen atom or an alkyl group of 1 to 5 carbon atoms and R.sup.2 is hydrogen atom or an alkyl group of 1 to 2 carbon atoms or a phenyl group, which method comprises reacting an aldehyde represented by the general formula I ##STR2## wherein R.sup.1 has the same meaning as defined above, with an alkylene oxide represented by the general formul II: ##STR3## wherein R.sup.2 has the same meaning as defined above, in an alkylene glycol solvent corresponding to said alkylene oxide in the presence of at least one catalyst selected from the group consisting of bromides of alkali metals, iodides of alkali metals, bromides of alkaline earth metals, and iodides of alkaline earth metals.

4. 发明授权

US4741745A Process for separation of carbon dioxide from other gases 失效
标题翻译：二氧化碳与其他气体分离的方法
公开(公告)号：US4741745A
公开(公告)日：1988-05-03
申请号：US43013
申请日：1987-04-27
申请人： Yukio Kadono , Minoru Miyagawa , Takahiko Nakai , Minoru Saotome
发明人： Yukio Kadono , Minoru Miyagawa , Takahiko Nakai , Minoru Saotome
IPC分类号： B01D53/40 , B01D53/14 , B01D53/34 , B01D53/77 , C01B3/52 , C10K1/16 , C10L3/10 , B01D47/00
CPC分类号： C10K1/165 , B01D53/1456 , B01D53/1493 , C01B3/52 , C01B2203/0415 , C01B2203/0475 , C01B2203/048 , C01B2203/0485 , Y02C10/06 , Y02P20/152
摘要： Diisopropyl ethers of oligomers of ethylene glycol having between 2 and 8 ethylene glycol moieties and an average molecular weight between 190 and 300, are more useful physical absorption solvents for the separation of acid gases than are dimethyl, diethyl, ethyl butyl, propyl butyl, dibutyl, or higher alkyl ethers of the same ethylene glycol oligomers, because of a combination of high solution capacity, high separation efficiencies, low viscosity, low gas pressure, and resistance to hydrolysis during use. The diisopropyl ether of diethylene glycol is especially advantageous for use at absorber temperatures below 0.degree. C. Because of low viscosity, the diisopropyl ethers can often be substituted in separation equipment designed for use with chemical rather than physical solvents, thereby realizing the lower operating costs associated with physical solvents without requiring new capital investment.
摘要翻译：具有2至8个乙二醇部分和平均分子量在190和300之间的乙二醇低聚物的二异丙基醚比二甲基，二乙基，乙基丁基，丙基丁基，二丁基等更有用的分离酸性气体的物理吸收溶剂，或相应的乙二醇低聚物的高级烷基醚，因为在使用过程中组合了高溶液容量，高分离效率，低粘度，低气体压力和耐水解性。二乙二醇的二异丙醚特别有利于在低于0℃的吸收器温度下使用。由于低粘度，二异丙醚通常可以在设计用于化学而不是物理溶剂的分离设备中进行取代，从而实现较低的操作成本与物理溶剂相关，而不需要新的资本投资。

5. 发明授权

US06346509B1 Higher secondary alcohol alkoxylate compound composition, method for production thereof, and detergent and emulsifier using the composition 失效
标题翻译：高级仲醇烷氧基化合物组合物，其制备方法，以及使用该组合物的洗涤剂和乳化剂
公开(公告)号：US06346509B1
公开(公告)日：2002-02-12
申请号：US09834777
申请日：2001-04-12
申请人： Yukio Kadono , Kunihiko Kimata , Kenji Rakutani , Yoshiyuki Onda
发明人： Yukio Kadono , Kunihiko Kimata , Kenji Rakutani , Yoshiyuki Onda
IPC分类号： C11D100
CPC分类号： C07C41/03 , C07C41/06 , C11D1/72 , C07C43/13 , C07C43/11 , C07C43/10
摘要： A higher secondary alcohol alkoxylate compound composition represented by the general formula (1): [wherein R1 and R2 represent an alkyl group provided that the total number of carbon atoms of R1 and R2 is in the range of 7 to 29 and the number of carbon atom of R2 is not less than that of R1 (the number of carbon atom of R1
摘要翻译：由通式（1）表示的高级仲醇烷氧基化合物组合物：[其中R1和R2表示烷基，条件是R1和R2的碳原子总数在7-29范围内，碳数 R2的原子不小于R1（R1的碳原子数，R2的碳原子数），A表示低级亚烷基，n表示平均为1〜50的数字。假设当n不小于2时，由AO表示的氧化烯基的种类数可以是一个或两个或更多个，并且当氧烷基具有两个或更多个物质时，所有氧化烯基团存在于平均值的n，B表示氢原子或SO 3 M（其中M表示碱金属原子，碱土金属原子，铵基或取代的铵基）]，其中，所述组合物含有30〜90摩尔％ R 1具有甲基的醇烷氧基化合物（X）和R 1具有碳原子数2以上的烷基的高级仲醇烷氧基化合物（Y）70〜10摩尔％，其制造方法和洗涤剂和使用该组合物的乳化剂。

6. 发明授权

US06255275B1 Higher secondary alcohol alkoxylate compound composition, method for production thereof, and detergent and emulsifier using the composition 有权
标题翻译：高级仲醇烷氧基化合物组合物，其制备方法，以及使用该组合物的洗涤剂和乳化剂
公开(公告)号：US06255275B1
公开(公告)日：2001-07-03
申请号：US09464995
申请日：1999-12-16
申请人： Yukio Kadono , Kunihiko Kimata , Kenji Rakutani , Yoshiyuki Onda
发明人： Yukio Kadono , Kunihiko Kimata , Kenji Rakutani , Yoshiyuki Onda
IPC分类号： C11D100
CPC分类号： C07C41/03 , B01F17/0028 , C07C41/06 , C07C43/11 , C07C305/10 , C08G65/2609 , C11D1/29 , C11D1/72 , C07C43/13
摘要： A higher secondary alcohol alkoxylate compound composition represented by the general formula (1): , wherein the composition comprises 30 to 90 mol % of the higher secondary alcohol alkoxylate compound (X) having a methyl group for R1 and 70 to 10 mol % of the higher secondary alcohol alkoxylate compound (Y) having an alkyl group of 2 or more carbon atoms for R1, a method for the production thereof, and a detergent and an emulsifier using the composition.
摘要翻译：由通式（1）表示的高级仲醇烷氧基化合物组合物：其中，组合物含有30〜90摩尔％的具有R 1的甲基的高级仲醇烷氧基化合物（X）和70〜10摩尔％对于R 1具有2个以上碳原子的烷基的高级仲醇烷氧基化合物（Y），其制造方法以及使用该组合物的洗涤剂和乳化剂。

7. 发明授权

US5994595A Production process for (poly)alkylene glycol monoalkyl ether 失效
公开(公告)号：US5994595A
公开(公告)日：1999-11-30
申请号：US980577
申请日：1997-12-01
申请人： Yoshiyuki Onda , Masaru Kirishiki , Hideaki Tsuneki , Yukio Kadono
发明人： Yoshiyuki Onda , Masaru Kirishiki , Hideaki Tsuneki , Yukio Kadono
IPC分类号： C07C41/06 , C07C41/00
CPC分类号： C07C41/06 , C07C41/42 , Y02P20/584
摘要： The present invention provides a process for producing a (poly)alkylene glycol monoalkyl ether with high selectivity and high yield. In this process, the (poly)alkylene glycol monoalkyl ether is produced by reacting an olefin and a (poly)alkylene glycol in the presence of a catalyst, wherein: 1) a crystalline metallosilicate is used as the catalyst, and at least a portion of the used catalyst is regenerated, and the regenerated catalyst is recycled as the catalyst for the reaction; or 2) the reaction between the olefin and the (poly)alkylene glycol is carried out in the presence of either or both of a (poly)alkylene glycol dialkyl ether and an alcohol.

8. 发明授权

US5220054A Process for producing aminocarboxylic acid salt 失效
标题翻译：生产氨基羧酸盐的方法
公开(公告)号：US5220054A
公开(公告)日：1993-06-15
申请号：US915803
申请日：1992-07-27
申请人： Yoshiaki Urano , Yukio Kadono , Takakiyo Goto
发明人： Yoshiaki Urano , Yukio Kadono , Takakiyo Goto
IPC分类号： B01J23/72 , B01J25/00 , C07B61/00 , C07C227/02 , C07C229/06 , C07C229/16
CPC分类号： C07C227/02 , B01J23/72 , C07C229/16
摘要： The present invention provides a novel process for producing an aminocarboxylic acid salt which is useful as a material for agricultural chemicals and drugs, a chelating agent, a food additive, etc. The process produces an aminocarboxylic acid salt from an aminoalcohol by subjecting the aminoalcohol to an oxidative dehydrogenation reaction in the coexistence of an alkali metal hydroxide and/or an alkaline earth metal hydroxide, a copper-containing catalyst and water, and is characterized by performing the reaction while maintaining the nickel concentration in the reaction mixture at 40 ppm or less.
摘要翻译： PCT No.PCT / JP91 / 01616 Sec。 371日期：1992年7月27日 102（e）日期1992年7月27日PCT 1991年11月26日PCT PCT。第WO92 / 09559号公报日本1992年6月11日。本发明提供了用作农药和药物材料，螯合剂，食品添加剂等的氨基羧酸盐的新方法。该方法从通过在碱金属氢氧化物和/或碱土金属氢氧化物，含铜催化剂和水的共存下使氨基醇进行氧化脱氢反应，得到氨基醇，其特征在于进行反应同时保持镍浓度在反应混合物在40ppm以下。

9. 发明授权

US06573406B2 High-purity alkanolamines and their production process 有权
公开(公告)号：US06573406B2
公开(公告)日：2003-06-03
申请号：US10053911
申请日：2002-01-24
申请人： Kenji Muraoka , Toshiaki Saito , Yukio Kadono
发明人： Kenji Muraoka , Toshiaki Saito , Yukio Kadono
IPC分类号： C07C20984
CPC分类号： C07C215/08
摘要： High-purity alkanolamines, whose iron content is less than 50 ppb, are provided. Said high-purity alkanolamines can be produced by covering with an alkanolamine-resistant material at least a part of the inner wall of equipment that contacts alkanolamines from the top of the distillation tower to the storage tank in producing a high-purity alkanolamine from a crude alkanolamine by using distillation towers.

10. 发明授权

US06417408B2 Production process for (poly)alkylene glycol monoalkyl ether 失效
标题翻译：（聚）亚烷基二醇单烷基醚的制备方法
公开(公告)号：US06417408B2
公开(公告)日：2002-07-09
申请号：US09790053
申请日：2001-02-21
申请人： Yoshiyuki Onda , Masaru Kirishiki , Hideaki Tsuneki , Yukio Kadono
发明人： Yoshiyuki Onda , Masaru Kirishiki , Hideaki Tsuneki , Yukio Kadono
IPC分类号： C07C4106
CPC分类号： C07C41/06 , C07C41/42 , Y02P20/584 , C07C43/13 , C07C43/11
摘要： The present invention provides a process for producing a (poly)alkylene glycol monoalkyl ether with high selectivity and high yield. In this process, the (poly)alkylene glycol monoalkyl ether is produced by reacting an olefin and a (poly)alkylene glycol in the presence of a catalyst, wherein: 1) a crystalline metallosilicate is used as the catalyst, and at least a portion of the used catalyst is regenerated, and the regenerated catalyst is recycled as the catalyst for the reaction; or 2) the reaction between the olefin and the (poly)alkylene glycol is carried out in the presence of either or both of a (poly)alkylene glycol dialkyl ether and an alcohol.
摘要翻译：本发明提供了以高选择性和高收率制备（聚）亚烷基二醇单烷基醚的方法。在该方法中，（聚）亚烷基二醇单烷基醚是通过在催化剂存在下使烯烃和（聚）亚烷基二醇反应制备的，其中：1）使用结晶金属硅酸盐作为催化剂，并且至少一部分的再生催化剂再生，再生催化剂作为反应催化剂再循环使用; 或2）烯烃和（聚）亚烷基二醇之间的反应在（聚）亚烷基二醇二烷基醚和醇中的任一种或两者的存在下进行。

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