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1. 发明授权

US08268037B2 Recovery of molybdenum from molybdenum bearing sulfide materials by bioleaching in the presence of iron 失效
标题翻译：在铁存在下通过生物浸出从含钼硫化物材料中回收钼
公开(公告)号：US08268037B2
公开(公告)日：2012-09-18
申请号：US12375955
申请日：2007-07-19
申请人： Wolfgang Kummer , Wilfried Gutknecht , James Gregory Olson , Thomas R. Clark
发明人： Wolfgang Kummer , Wilfried Gutknecht , James Gregory Olson , Thomas R. Clark
IPC分类号： C22B3/18 , C22B3/06
CPC分类号： C22B3/18 , C22B3/08 , C22B34/34 , Y02P10/234
摘要： The invention relates to a method of recovering molybdenum from a molybdenum bearing sulfide material. The material is contacted with a leaching solution in the presence of iron compounds and mesophilic or thermophilic iron oxidizing microorganisms and subsequently, a leaching process is performed by controlling the molar ratio of dissolved ferric iron to dissolved molybdenum. Preferably, a high amount and molar excess of dissolved iron is used. The presence of high concentrations of ferric iron in bioleach solutions allows iron-oxidizing microorganisms to grow and oxidize iron and bioleach molybdenite at dissolved Mo concentrations as high as 4.4 g/L. Organic metabolites were not required for protecting cells from Mo toxicity. Maximum dissolution rates depend on reactor configuration, with agglomerated material simulating heap leaching of almost 1% Mo/day, but up to 10.2% Mo/day in suspension/stirred reactor configurations, with rate highly dependent on temperature within the range of 25° C. to 40° C. The ultimate extent of Mo removal from the molybdenum bearing sulfide material is 89%. Finally, molybdenum is recovered from a leach residue of the leaching process.
摘要翻译：本发明涉及从含钼硫化物材料中回收钼的方法。在铁化合物和嗜温或嗜热铁氧化微生物的存在下，将材料与浸出溶液接触，随后，通过控制溶解的三价铁与溶解的钼的摩尔比来进行浸出过程。优选地，使用高量和摩尔过量的溶解铁。在生物浸出溶液中存在高浓度的三价铁可使铁氧化微生物在溶解的Mo浓度高达4.4g / L时生长并氧化铁和生物漂白辉钼矿。不需要有机代谢物来保护细胞免受Mo毒性。最大溶解速率取决于反应器构型，其中模拟堆浸浸出量为1％Mo /天的聚集材料，但在悬浮/搅拌反应器构型中高达10.2％Mo /天，速率高度依赖于25℃范围内的温度至40℃。从含钼硫化物材料除去Mo的最终程度为89％。最后，从浸出过程的浸出残渣中回收钼。

2. 发明授权

US07175791B2 Process for producing dish-shaped moldings of thermoplastic material 有权
标题翻译：用于生产热塑性材料的碟形模制品的方法
公开(公告)号：US07175791B2
公开(公告)日：2007-02-13
申请号：US10361541
申请日：2003-02-10
申请人： Michael Pappert , Alfred Jira , Andreas Hollweg , Wolfgang Kummer , Peter Klusener
发明人： Michael Pappert , Alfred Jira , Andreas Hollweg , Wolfgang Kummer , Peter Klusener
IPC分类号： B29C47/00
CPC分类号： B29C47/0066 , B29C47/0023 , B29C47/0026 , B29C47/0054 , B29C49/0047 , B29C49/02 , B29C49/04 , B29C49/22 , B29C49/4205 , B29C51/02 , B29C51/08 , B29C51/10 , B29C51/105 , B29C51/267 , B29C2049/0057 , B29C2791/007 , B29C2793/0063 , B29K2995/0082
摘要： A process for the production of dish-shaped moldings or hollow bodies of thermoplastic material comprises the step of producing an at least approximately tubular preform by the extrusion of thermoplastic material. The preform is axially divided to form at least one single-layer web of material which is removed from the extrusion head by being engaged by means of a manipulator which spreads and/or straightens the web transversely with respect to the extrusion direction. The web is then transferred to a molding tool by a manipulator for it to be put into its final form in its first heat in the molding tool.
摘要翻译：用于生产碟形模制品或热塑性材料的中空体的方法包括通过挤出热塑性材料制造至少近似管状的预成型件的步骤。预成型件被轴向分开以形成至少一个单层材料纤维网，其通过借助于相对于挤出方向横向扩展和/或拉伸织物的操纵器而从挤压头移除。然后将纸幅通过操纵器转移到模制工具中，使其在模制工具中的第一次加热中被放入其最终形式。

3. 发明申请

US20060001197A1 Process for producing hollow bodies of thermoplastic material and apparatus for same 有权
标题翻译：用于制造热塑性材料的空心体的方法及其装置
公开(公告)号：US20060001197A1
公开(公告)日：2006-01-05
申请号：US11173123
申请日：2005-07-01
申请人： Wolfgang Kummer
发明人： Wolfgang Kummer
IPC分类号： B29C49/70
CPC分类号： B29C49/4247 , B26D3/001 , B26D3/163 , B29C49/04 , B29C2793/009
摘要： The invention concerns a process and an apparatus for producing hollow bodies of thermoplastic material by means of extrusion blow molding. A tubular preform of plasticised material is expanded beyond parts of a blow molding mold enclosing it, by means of increased external pressure, wherein the preform, prior to closure of the mold halves, is spread transversely with respect to the extrusion direction and in a separation plane of the blow molding mold, in such a way that it extends between the lateral edges of the mold cavity of the blow molding mold. Prior to removal of the article from the blow molding mold, the bulge portion produced after closure of the blow molding mold is cut open along its length at each of the two sides of the mold at the respective edges extending in the extrusion direction.
摘要翻译：本发明涉及通过挤压吹塑成型制造热塑性材料的中空体的方法和装置。通过增加的外部压力将塑化材料的管状预成型件扩展到包围其的吹塑模具的部分之外，其中在关闭半模之前，预成型件相对于挤出方向横向扩展，并且在分离吹塑模具的平面，使得其在吹塑模具的模腔的侧边缘之间延伸。在从吹塑模具移除物品之前，在吹塑模具关闭之后产生的凸起部分沿着在挤出方向上延伸的相应边缘处的模具两侧的每一侧沿其长度被切割。

4. 发明授权

US06447739B1 Method for producing lithium transition metallates 失效
标题翻译：锂过渡金属化合物的制备方法
公开(公告)号：US06447739B1
公开(公告)日：2002-09-10
申请号：US09367809
申请日：1999-08-19
申请人： Ulrich Krynitz , Wolfgang Kummer , Mathias Benz , Juliane Meese-Marktscheffel , Evelyn Pross , Viktor Stoller
发明人： Ulrich Krynitz , Wolfgang Kummer , Mathias Benz , Juliane Meese-Marktscheffel , Evelyn Pross , Viktor Stoller
IPC分类号： C01D1500
CPC分类号： H01M4/485 , C01G45/1221 , C01G51/42 , C01G53/42 , C01P2002/72 , C01P2006/80 , H01M4/131 , H01M4/1391 , H01M4/505 , H01M4/525
摘要： The invention relates to a method for producing lithium transition metalates of the general formula (I): Lix(M1yM21−y)nOnz, where M1 represents lithium, cobalt or manganese; M2 represents cobalt, iron, manganese or aluminium and is not equal to M1; n is equal to 2 if M1=M, and 1 in all other cases; x is a number between 0.9 and 1.2; y is a number between 0.5 and 1.0; and z is a number between 1.9 and 2.1. According to the method, an intimate solid mixture is produced of oxygen-containing compounds of the transition metals and oxygen-containing lithium compounds and this mixture calcinated in a reactor, whereby calcination takes place at least partly at an absolute pressure of less than 0.5 bar.
摘要翻译：本发明涉及一种制备通式（I）的锂过渡金属盐的方法：Lix（M1yM21-y）nOnz，其中M1表示锂，钴或锰; M2表示钴，铁，锰或铝，不等于M1; 如果M1 = M，则n等于2，在其他情况下，n等于1; x是0.9和1.2之间的数字; y是0.5到1.0之间的数字; z是1.9和2.1之间的数字。根据该方法，产生过渡金属和含氧锂化合物的含氧化合物的紧密固体混合物，并将该混合物在反应器中煅烧，由此煅烧至少部分地发生在小于0.5巴的绝对压力。

5. 发明授权

US5037705A Oxygen-containing molybdenum metal powder and processes for its preparation 失效
标题翻译：含氧钼金属粉末及其制备方法
公开(公告)号：US5037705A
公开(公告)日：1991-08-06
申请号：US585802
申请日：1990-09-20
申请人： Theodor A. Weber , Wolfgang Kummer
发明人： Theodor A. Weber , Wolfgang Kummer
IPC分类号： C01G39/00 , B22F1/00 , B22F1/02 , C23C4/04 , C23C4/06
CPC分类号： C23C4/06 , B22F1/0088 , Y10T428/12181 , Y10T428/2991 , Y10T428/2993
摘要： A molybdenum metal powder having an outer shell coating of MoO.sub.2 is useful in flame spray or plasma spray processes and is prepared by partially oxidizing molybdenum powder in a carbon dioxide atmosphere at temperatures of up to 1200.degree. C.

6. 发明授权

US4976779A Oxygen-containing molybdenum metal powder and processes for its preparation 失效
标题翻译：含氧钼金属粉末及其制备方法
公开(公告)号：US4976779A
公开(公告)日：1990-12-11
申请号：US427582
申请日：1989-10-27
申请人： Theodor A. Webwer , Wolfgang Kummer
发明人： Theodor A. Webwer , Wolfgang Kummer
IPC分类号： C01G39/00 , B22F1/00 , B22F1/02 , C23C4/04 , C23C4/06
CPC分类号： C23C4/06 , B22F1/0088 , Y10T428/12181 , Y10T428/2991 , Y10T428/2993
摘要： A molybdenum metal powder having an outer shell coating of MoO.sub.2 is useful in flame spray or plasma spray processes and is prepared by partially oxidizing molybdenum powder in a carbon dioxide atmosphere at temperatures of up to 1200.degree. C.
摘要翻译：具有MoO2外壳涂层的钼金属粉末可用于火焰喷涂或等离子喷涂工艺，并且通过在二氧化碳气氛中在高达1200℃的温度下部分氧化钼粉而制备。

7. 发明授权

US06875416B1 Method for producing lithium-transition metal mixtures 有权
标题翻译：锂 - 过渡金属混合物的制备方法
公开(公告)号：US06875416B1
公开(公告)日：2005-04-05
申请号：US09601946
申请日：1998-08-13
申请人： Mathias Benz , Wolfgang Kummer , Evelyn Pross , Josef Schmoll , Wolfgang Schweda , Daniel Duff , Ricarda Leiberich , Christoph Schild , Ulrich Krynitz , Juliane Meese-Marktscheffel , Viktor Stoller
发明人： Mathias Benz , Wolfgang Kummer , Evelyn Pross , Josef Schmoll , Wolfgang Schweda , Daniel Duff , Ricarda Leiberich , Christoph Schild , Ulrich Krynitz , Juliane Meese-Marktscheffel , Viktor Stoller
IPC分类号： C01G53/00 , H01M4/48 , H01M4/485 , H01M4/50 , H01M4/505 , H01M4/52 , H01M4/525 , H01M10/0525 , H01M10/36 , C01D1/02 , C01F7/04 , C01G37/02 , C01G45/02
CPC分类号： C01G45/1228 , C01G51/42 , C01G51/44 , C01G53/42 , C01G53/44 , C01G53/50 , C01P2002/52 , C01P2002/74 , C01P2004/50 , C01P2004/61 , C01P2006/12 , H01M4/485 , H01M4/505 , H01M4/525 , H01M10/0525
摘要： The invention relates to a method for producing lithium-transition metal mixtures of general formula Lix(M1yM21-y)nOnz, wherein M1 represents nickel, cobalt or manganese, M2 represents chromium, cobalt, iron, manganese, molybdenum or aluminium, and is different from M1, n is 2 if M1 represents manganese and is 1 otherwise, x is comprised between 0.9 and 1.2, y is comprised between 0.5 and 1.0 and z is comprised between 1.9 and 2.1. According to the inventive method, an intimate mixture composed of transition metal compounds containing oxygen and of a lithium compound containing oxygen is calcinated, said mixture being obtained by processing a solid powder transition metal compound with a solution of said lithium compound, and then drying. At least the M1 compound is used in powder form having a specific surface of at least 20 m2/g (BET) and calcination is carried out in a fluidised bed.
摘要翻译：本发明涉及一种制备通式为Lix（M 1 yM 2-y）n O n z的锂 - 过渡金属混合物的方法，其中M 1表示镍，钴或锰，M 2表示铬，钴，铁，锰，钼或铝，并且不同于M 1，如果M 1表示锰，则n为2，否则为1，x为0.9至1.2，y为0.5至1.0 z在1.9和2.1之间。根据本发明的方法，煅烧由含有氧的过渡金属化合物和含氧化合物的锂化合物组成的紧密混合物，所述混合物通过用所述锂化合物的溶液处理固体粉末过渡金属化合物，然后干燥而获得。至少M 1化合物以比表面积至少为20m 2 / g（BET）的粉末形式使用，并且在流化床中进行煅烧。

8. 发明申请

US20050019247A1 Production of pure molybdenum oxide from low grade molybdenite concentrates 审中-公开
标题翻译：从低品位辉钼矿精矿生产纯氧化钼
公开(公告)号：US20050019247A1
公开(公告)日：2005-01-27
申请号：US10477080
申请日：2001-09-26
申请人： Robert Balliett , Wolfgang Kummer , John Litz , Lawrence MHugh , Harry Nauta , Paul Queneau , Rong-Chien Wu
发明人： Robert Balliett , Wolfgang Kummer , John Litz , Lawrence MHugh , Harry Nauta , Paul Queneau , Rong-Chien Wu
IPC分类号： C01G39/00 , C01G39/02 , C22B3/14 , C22B3/26 , C22B3/44 , C22B34/34
CPC分类号： C22B3/14 , C01G39/003 , C01G39/02 , C01P2006/80 , C22B3/0005 , C22B3/44 , C22B34/34 , Y02P10/234
摘要： High purity ammonium dimolybdate or molybdenum oxide is produced by the pressure oxidation of low grade molybdenite concentrates or molybdenum intermediates. The process entails nearly complete oxidation of the sulfide minerals while optimizing the process chemistry and autoclave conditions to solubilize as little of the molybdenum values as possible. The autoclave discharge 12 is then subjected to a leaching step, either an alkaline leach 50, 400 or ammonium leach 250 process, before or after a liquid/solid separation step 20, 220, 410. The solution is then subjected to (a) filtration 60, 410, solvent extraction 70, 440, crystallization 90, 450, and calcination 120, 480 or (b) filtration 260, 280, crystallization 290, and calcination 320 to produce a product suitable for chemical-grade molybdenum oxide 125, 325, 485.
摘要翻译：通过低品位辉钼矿浓缩物或钼中间体的压力氧化产生高纯度的二钼酸铵或氧化钼。该过程需要几乎完全硫化矿物氧化，同时优化工艺化学和高压釜条件以溶解尽可能少的钼值。然后在液体/固体分离步骤20,220,410之前或之后对高压釜排出口12进行浸出步骤，碱浸液50,400或铵浸出250处理。然后将溶液进行（a）过滤 60,410，溶剂萃取70,440，结晶90,450和煅烧120,480或（b）过滤260,280，结晶290和煅烧320以产生适合于化学级氧化钼125,325的产物， 485。

9. 发明申请

US20090320648A1 RECOVERY OF MOLYBDENUM FROM MOLYBDENUM BEARING SULFIDE MATERIALS BY BIOLEACHING IN THE PRESENCE OF IRON 失效
标题翻译：通过在铁存在下通过生物柴油回收莫来石轴承硫化物材料
公开(公告)号：US20090320648A1
公开(公告)日：2009-12-31
申请号：US12375955
申请日：2007-07-19
申请人： Wolfgang Kummer , Wilfried Gutknecht , James Gregory Olson , Thomas R. Clark
发明人： Wolfgang Kummer , Wilfried Gutknecht , James Gregory Olson , Thomas R. Clark
IPC分类号： C22B34/34 , E21B43/28
CPC分类号： C22B3/18 , C22B3/08 , C22B34/34 , Y02P10/234
摘要： The invention relates to a method of recovering molybdenum from a molybdenum bearing sulfide material. The material is contacted with a leaching solution in the presence of iron compounds and mesophilic or thermophilic iron oxidizing microorganisms and subsequently, a leaching process is performed by controlling the molar ratio of dissolved ferric iron to dissolved molybdenum. Preferably, a high amount and molar excess of dissolved iron is used. The presence of high concentrations of ferric iron in bioleach solutions allows iron-oxidizing microorganisms to grow and oxidize iron and bioleach molybdenite at dissolved Mo concentrations as high as 4.4 g/L. Organic metabolites were not required for protecting cells from Mo toxicity. Maximum dissolution rates depend on reactor configuration, with agglomerated material simulating heap leaching of almost 1% Mo/day, but up to 10.2% Mo/day in suspension/stirred reactor configurations, with rate highly dependent on temperature within the range of 25° C. to 40° C. The ultimate extent of Mo removal from the molybdenum bearing sulfide material is 89%. Finally, molybdenum is recovered from a leach residue of the leaching process.
摘要翻译：本发明涉及从含钼硫化物材料中回收钼的方法。在铁化合物和嗜温或嗜热铁氧化微生物的存在下，将材料与浸出溶液接触，随后，通过控制溶解的三价铁与溶解的钼的摩尔比来进行浸出过程。优选地，使用高量和摩尔过量的溶解铁。在生物浸出溶液中存在高浓度的三价铁可使铁氧化微生物在溶解的Mo浓度高达4.4g / L时生长并氧化铁和生物漂白辉钼矿。不需要有机代谢物来保护细胞免受Mo毒性。最大溶解速率取决于反应器构型，其中模拟堆浸浸出量为1％Mo /天的聚集材料，但在悬浮/搅拌反应器构型中高达10.2％Mo /天，速率高度依赖于25℃范围内的温度至40℃。从含钼硫化物材料除去Mo的最终程度为89％。最后，从浸出过程的浸出残渣中回收钼。

10. 发明授权

US07393969B2 Particular calixarenes method for production and use thereof 失效
标题翻译：特殊的杯芳烃方法用于生产和使用
公开(公告)号：US07393969B2
公开(公告)日：2008-07-01
申请号：US11574144
申请日：2005-08-16
申请人： Michael Traving , Wilfried Gutknecht , Werner Bäcker , Wolfgang Kummer , Rainer Ludwig
发明人： Michael Traving , Wilfried Gutknecht , Werner Bäcker , Wolfgang Kummer , Rainer Ludwig
IPC分类号： C07C69/76 , B01D15/00
CPC分类号： C22B3/002 , C07C69/712 , C07C2603/92 , C22B26/10 , Y02P10/234
摘要： The present invention relates to calix[4]arenes which effectively bind alkali metal ions (Na+, K+) and transport them over phase boundaries, their preparation and use.
摘要翻译：本发明涉及有效结合碱金属离子（Na +），K + +和/或它们在相界面上运输的杯[4]芳烃，其制备和用途。

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