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1. 发明申请

US20150045592A1 PROCESS FOR THE PRODUCTION OF CHLORINATED ALKANES 有权
标题翻译：生产氯化碱的方法
公开(公告)号：US20150045592A1
公开(公告)日：2015-02-12
申请号：US14358079
申请日：2012-11-13
申请人： Matthew L. Grandbois , William J. Kruper, JR.
发明人： Matthew L. Grandbois , William J. Kruper, JR.
IPC分类号： C07C17/013
CPC分类号： C07C17/013 , C07C17/10 , C07C19/01
摘要： Processes for the production of chlorinated alkanes are provided. The present processes comprise reacting one or more mono- and/or dichloroalkanes to form tri-, tetra- and/or pentachloroalkanes, with high regioselectivity. In those embodiments wherein a dichloroalkane is desirably utilized, it may advantageously be a vicinal dichloroalkane. Further, only one catalyst is utilized. The present processes make use of sulfuryl chloride as a chlorinating agent, rather than a gaseous chlorinating agent such as chlorine gas. Finally, the process uses lower intensity process conditions than at least some conventional processes, and thus, operating costs are saved.
摘要翻译：提供了生产氯代烷烃的方法。本方法包括使一种或多种单 - 和/或二氯烷烃反应形成具有高区域选择性的三，四和/或五氯代烷烃。在其中希望使用二氯烷烃的那些实施方案中，它可以有利地是连续的二氯烷烃。此外，仅使用一种催化剂。本方法使用磺酰氯作为氯化剂，而不是气态氯化剂如氯气。最后，该方法使用比至少一些常规方法更低强度的工艺条件，因此节省了操作成本。

2. 发明申请

US20140081055A1 PROCESS FOR THE PRODUCTION OF CHLORINATED PROPENES 有权
标题翻译：生产氯化丙烯的方法
公开(公告)号：US20140081055A1
公开(公告)日：2014-03-20
申请号：US14123139
申请日：2012-05-18
申请人： Max M. Tirtowidjojo , William J. Kruper, JR. , Barry B. Fish , David S. Laitar
发明人： Max M. Tirtowidjojo , William J. Kruper, JR. , Barry B. Fish , David S. Laitar
IPC分类号： C07C17/25
CPC分类号： C07C17/25 , C07C17/10 , C07C19/01 , C07C21/04
摘要： Processes for the production of chlorinated propenes are provided. The present processes make use of 1,2-dichloropropane, a by-product in the production of chlorohydrin, as a low cost starting material, alone or in combination with 1,2,3-trichloropropane. The present processes can also generate anhydrous HCl as a byproduct that can be removed from the process and used as a feedstock for other processes, providing further time and cost savings. Finally, the processes are advantageously conducted in the liquid phase, thereby presenting additional savings as compared to conventional, gas phase processes.
摘要翻译：提供了生产氯化丙烯的方法。本发明方法利用1,2-二氯丙烷作为生产氯代醇中的副产物，作为低成本原料，单独使用或与1,2,3-三氯丙烷组合使用。本方法还可以产生作为副产物的无水HCl，其可从该方法中除去并用作其它方法的原料，从而进一步节省时间和成本。最后，该方法有利地在液相中进行，从而与常规的气相方法相比可以节省更多的费用。

3. 发明申请

US20130066091A1 PROCESS FOR HYDROCHLORINATION OF MULTIHYDROXYLATED ALIPHATIC HYDROCARBONS 有权
标题翻译：多羟基化合物烃的氢化方法
公开(公告)号：US20130066091A1
公开(公告)日：2013-03-14
申请号：US13697038
申请日：2011-05-19
申请人： Tina L. Arrowood , William J. Kruper, JR. , John R. Briggs
发明人： Tina L. Arrowood , William J. Kruper, JR. , John R. Briggs
IPC分类号： C07C67/28 , C07B41/12 , C07C67/10 , C07C67/08 , C07C67/29
CPC分类号： C07B41/12 , C07C29/62 , C07C29/86 , C07C67/08 , C07C67/10 , C07C67/11 , C07C67/58 , C07C31/36 , C07C69/63 , C07C69/78
摘要： A process for producing a chlorohydrin, an ester of a chlorohydrin, or a mixture thereof including the steps of contacting, in a hydrochlorination reactor, a multihydroxylated aliphatic hydrocarbon, an ester of a multihydroxylated aliphatic hydrocarbon, or a mixture thereof with a source of a hydrogen chloride, in the presence of a hydrophobic or extractable carboxylic acid catalyst is provided.
摘要翻译：一种生产氯代醇，氯代醇酯或其混合物的方法，包括以下步骤：在氢氯化反应器中将多羟基化脂族烃，多羟基化脂族烃或其混合物的酯与提供了在疏水性或可提取的羧酸催化剂存在下的氯化氢。

4. 发明申请

US20110087056A1 ADIABATIC PLUG FLOW REACTORS AND PROCESSES INCORPORATING THE SAME 审中-公开
标题翻译： ADIABATIC PLUG流动反应器及其加工方法
公开(公告)号：US20110087056A1
公开(公告)日：2011-04-14
申请号：US12901383
申请日：2010-10-08
申请人： Max M. Tirtowidjojo , Hua Bai , Debashis Chakraborty , Juergen Eiffler , Heinz Groenewald , Kurt F. Hirsekorn , Manfred Kokott , William J. Kruper, JR. , Thomas U. Luebbe , Thomas J. Parsons , Avani Maulik Patel , Marcus Wobser
发明人： Max M. Tirtowidjojo , Hua Bai , Debashis Chakraborty , Juergen Eiffler , Heinz Groenewald , Kurt F. Hirsekorn , Manfred Kokott , William J. Kruper, JR. , Thomas U. Luebbe , Thomas J. Parsons , Avani Maulik Patel , Marcus Wobser
IPC分类号： C07C21/18 , B01J19/00 , C07C21/02
CPC分类号： C07C17/206 , B01J19/0013 , B01J19/0026 , B01J19/006 , B01J19/2405 , B01J19/2415 , B01J2219/00054 , B01J2219/00063 , B01J2219/00155 , B01J2219/00162 , B01J2219/00166 , B01J2219/00247 , C07C17/269 , C07C21/18 , C07C21/04
摘要： The present invention provides adiabatic plug flow reactors suitable for the production of chlorinated and/or fluorinated propene and higher alkenes from the reaction of chlorinated and/or fluorinated alkanes and chlorinated and/or fluorinated alkenes. The reactors comprise one or more designs that minimize the production of by-products at a desired conversion.
摘要翻译：本发明提供了适于从氯化和/或氟化烷烃和氯化和/或氟化烯烃的反应生产氯化和/或氟化丙烯和更高级烯烃的绝热活塞流反应器。反应器包括一种或多种在期望的转化下使副产物生产最小化的设计。

5. 发明申请

US20090149561A1 EXTRUDED POLYMER FOAMS CONTAINING BROMINATED 2-OXO-1,3,2-DIOXAPHOSPHORINANE COMPOUNDS AS FLAME RETARDANT ADDITIVES 审中-公开
标题翻译：含有作为阻燃添加剂的2-氧代-1,3-二氧杂环己烷化合物的挤出聚合物
公开(公告)号：US20090149561A1
公开(公告)日：2009-06-11
申请号：US12331856
申请日：2008-12-10
申请人： Anteneh Z. Worku , William G. Stobby , Sheila M. Tinetti , Inken Beulich , David R. Wilson , Duane R. Romer , James P. Godschalx , Nelson G. Rondan , William J. Kruper, JR. , Ted A. Morgan
发明人： Anteneh Z. Worku , William G. Stobby , Sheila M. Tinetti , Inken Beulich , David R. Wilson , Duane R. Romer , James P. Godschalx , Nelson G. Rondan , William J. Kruper, JR. , Ted A. Morgan
IPC分类号： C08J9/35
CPC分类号： C08J9/0038 , C08J9/12 , C08J2201/03 , C08J2325/04
摘要： Extruded polymer foams are prepared using 5,5-bis(bromomethyl)-2-oxo-1,3,2-dioxaphosphorinane or brominated 2-oxo-1,3,2-dioxaphosphorinane compounds. The brominated FR additives unexpectedly are stable at the extrusion temperatures, and provide excellent flame retardancy to the foams.
摘要翻译：使用5,5-双（溴甲基）-2-氧代-1,3,2-二氧杂磷杂环己烷或溴化2-氧代-1,3,2-二氧杂磷杂环己烷化合物制备挤出的聚合物泡沫体。溴化FR添加剂在挤出温度下出人意料地稳定，并且对泡沫具有优异的阻燃性。

6. 发明授权

US06387838B2 Activator composition comprising aluminum compound mixture 有权
标题翻译：包含铝化合物混合物的活化剂组合物
公开(公告)号：US06387838B2
公开(公告)日：2002-05-14
申请号：US09772592
申请日：2001-01-30
申请人： Eugene Y. Chen , Gordon R. Roof , William J. Kruper, Jr. , David J. Schwartz , Joey W. Storer
发明人： Eugene Y. Chen , Gordon R. Roof , William J. Kruper, Jr. , David J. Schwartz , Joey W. Storer
IPC分类号： B01J3100
CPC分类号： C07F5/066 , C07F7/10 , C07F17/00 , C08F10/00 , C08F110/06 , C08F210/16 , C08F4/61912 , C08F210/14 , C08F2500/12 , C08F4/65927 , C08F4/6592 , C08F4/65912
摘要： Compositions comprising: A) an aluminum compound corresponding to the formula AlArf3, where Arf is a fluorinated aromatic hydrocarbyl moiety of from 6 to 30 carbon atoms; B) an aluminum compound corresponding to the formula: AlArfQ1Q2, or a dimer, adduct, or mixture thereof; where: Arf is as previously defined; Q1 is Arf or a C1-20 hydrocarbyl group, optionally substituted with one or more cyclohydrocarbyl, hydrocarbyloxy, hydrocarbylsiloxy, hydrocarbylsilylamino, hydrocarbylsilyl, silylhydrocarbyl, di(hydrocarbylsilyl)amino, hydrocarbylamino, di(hydrocarbyl)amino, di(hydrocarbyl)phosphino, or hydrocarbylsulfido groups having from 1 to 20 atoms other than hydrogen, or, further optionally, such substituents may be covalently linked with each other to form one or more fused rings or ring systems; and Q2 is an aryloxy, arylsulfide or di(hydrocarbyl)amido group, optionally substituted with one or more hydrocarbyl, cyclohydrocarbyl, hydrocarbyloxy, hydrocarbylsiloxy, hydrocarbylsilylamino, hydrocarbylsilyl, silylhydrocarbyl, di(hydrocarbylsilyl)amino, hydrocarbylamino, di(hydrocarbyl)amino, di(hydrocarbyl)phosphino, or hydrocarbylsulfido groups having from 1 to 20 atoms other than hydrogen, or, further optionally such substituents may be covalently linked with each other to form one or more fused rings or ring systems, said Q2 having from 3 to 20 atoms other than hydrogen; and the molar ratio of A):B) in the composition being from 0.1:1 to 10:1 are useful as activators for olefin polymerizations.
摘要翻译：组合物，其包含：A）对应于式AlArf 3的铝化合物，其中Arf为6至30个碳原子的氟化芳族烃基部分; B）对应于式AlArfQ1Q2的铝化合物或其二聚物，加合物或其混合物 ; 其中：Arf如前所定义; Q 1是Arf或C 1-20烃基，任选被一个或多个环烃基，烃氧基，烃基甲硅烷氧基，烃基甲硅烷基氨基，烃基甲硅烷基，甲硅烷基烃基，二（烃基甲硅烷基）氨基，烃基氨基，二（烃基）氨基，二（烃基）膦基或具有除氢以外的1至20个原子的烃基硫基，或者进一步任选地，这些取代基可彼此共价连接以形成一个或多个稠环或环系; 环烷氧基，烃基甲硅烷氧基，烃基甲硅烷基氨基，烃基甲硅烷氧基，烃基甲硅烷基氨基，烃基甲硅烷基，甲硅烷基烃基，二（烃基甲硅烷基）氨基，烃基氨基，二（烃基）氨基，二（烃基）氨基，烃基）膦基或具有除氢之外的1至20个原子的烃基硫基，或者进一步任选地，这些取代基可以彼此共价连接以形成一个或多个稠环或环系，所述Q2具有3至20个原子的其它比氢; 并且组分中A）：B）的摩尔比为0.1:1至10:1可用作烯烃聚合的活化剂。

7. 发明授权

US06187940B1 Three coordinate aluminum catalyst activator composition 有权
标题翻译：三配位铝催化剂活化剂组成
公开(公告)号：US06187940B1
公开(公告)日：2001-02-13
申请号：US09330671
申请日：1999-06-11
申请人： Eugene Y. Chen , William J. Kruper, Jr. , Gordon R. Roof , David J. Schwartz , Joey W. Storer
发明人： Eugene Y. Chen , William J. Kruper, Jr. , Gordon R. Roof , David J. Schwartz , Joey W. Storer
IPC分类号： C07F506
CPC分类号： C08F10/00 , C07F5/062 , C07F5/066 , C08F4/6592 , C08F4/65927 , C08F110/06 , C08F210/16 , Y10S526/943 , C08F4/642 , C08F4/65912 , C08F210/14 , C08F2500/12
摘要： Compounds corresponding to the formula: AlArfQ1Q2, or a dimer, adduct, or mixture thereof and further mixtures with aluminum compounds of the formula AlArf3, where: Arf is a fluorinated aromatic hydrocarbyl moiety of from 6 to 30 carbon atoms; Q1 is Af or a C1-20 hydrocarbyl group, optionally substituted with one or more cyclohydrocarbyl, hydrocarbyloxy, hydrocarbylsiloxy, hydrocarbylsilylamino, hydrocarbylsilyl, silylhydrocarbyl, di(hydrocarbylsilyl)amino, hydrocarbylamino, di(hydrocarbyl)amino, di(hydrocarbyl)phosphino, or hydrocarbylsulfido groups having from 1 to 20 atoms other than hydrogen, or, further optionally, such substituents may be covalently linked with each other to form one or more fused rings or ring systems; and Q2 is an aryloxy, arylsulfide or di(hydrocarbyl)amido group, optionally substituted with one or more hydrocarbyl, cyclohydrocarbyl, hydrocarbyloxy, hydrocarbylsiloxy, hydrocarbylsilylamino, hydrocarbylsilyl, silylhydrocarbyl, di(hydrocarbylsilyl)amino, hydrocarbylamino, di(hydrocarbyl)amino, di(hydrocarbyl)phosphino, or hydrocarbylsulfido groups having from 1 to 20 atoms other than hydrogen, or, further optionally such substituents may be covalently linked with each other to form one or more fused rings or ring systems, said Q2 having from 3 to 20 atoms other than hydrogen are useful as activators for olefin polymerizations.
摘要翻译：对应于下式的AlArfQ1Q2或其二聚物，加合物或其混合物的化合物以及与式AlArf 3的铝化合物的进一步混合物，其中：Arf为6至30个碳原子的氟化芳族烃基部分; Q1为Af或任选被一个或多个环烃基，烃氧基，烃基甲硅烷氧基，烃基甲硅烷基氨基，烃基甲硅烷基，甲硅烷基烃基，二（烃基甲硅烷基）氨基，烃基氨基，二（烃基）氨基，二（烃基）膦基或烃基亚磺酰基取代的C 1-20烃基，至20个除氢以外的原子，或者进一步任选地，这些取代基可彼此共价连接以形成一个或多个稠环或环系; 环烷氧基，烃基甲硅烷氧基，烃基甲硅烷基氨基，烃基甲硅烷氧基，烃基甲硅烷基氨基，烃基甲硅烷基，甲硅烷基烃基，二（烃基甲硅烷基）氨基，烃基氨基，二（烃基）氨基，二（烃基）氨基，烃基）膦基或具有除氢之外的1至20个原子的烃基硫基，或者进一步任选地，这些取代基可以彼此共价连接以形成一个或多个稠环或环系，所述Q2具有3至20个原子的其它氢可用作烯烃聚合的活化剂。

8. 发明授权

US6160146A Process for preparing trifluoroarylaluminum etherates 有权
标题翻译：制备三氟芳烷基醚合物的方法
公开(公告)号：US6160146A
公开(公告)日：2000-12-12
申请号：US449508
申请日：1999-11-24
申请人： Eugene Y. Chen , Jerzy Klosin , William J. Kruper, Jr. , Robert E. LaPointe
发明人： Eugene Y. Chen , Jerzy Klosin , William J. Kruper, Jr. , Robert E. LaPointe
IPC分类号： C07F5/06
CPC分类号： C07F5/062
摘要： The monoether adduct of a tri(fluoroaryl)aluminum compound is prepared by an exchange reaction between a trihydrocarbylaluminum compound and a tri(fluororaryl)borane compound in a hydrocarbon solvent in the presence of a C.sub.1-6 aliphatic ether in an amount from 0.9 to 1.0 moles per mole of aluminum.
摘要翻译：三（氟芳基）铝化合物的单醚加合物是通过三烃基铝化合物和三（氟芳基）硼烷化合物在烃溶剂中在C 1-6脂族醚存在下的交换反应制备的，其量为0.9-1.0 每摩尔铝的摩尔数。

9. 发明授权

US5489425A Functionalized polyamine chelants 失效
标题翻译：官能化多胺螯合剂
公开(公告)号：US5489425A
公开(公告)日：1996-02-06
申请号：US31416
申请日：1993-03-15
申请人： William J. Kruper, Jr. , Douglas K. Pollock , William A. Fordyce , Machael J. Fazio , Muthiah N. Inbasekaran , Ramaiah Muthyala
发明人： William J. Kruper, Jr. , Douglas K. Pollock , William A. Fordyce , Machael J. Fazio , Muthiah N. Inbasekaran , Ramaiah Muthyala
IPC分类号： A61K47/48 , A61K49/00 , A61K51/10 , C07D257/02 , C07F15/00 , A61K51/00 , C07C211/00
CPC分类号： A61K47/48707 , A61K49/0002 , A61K51/1093 , C07D257/02 , C07F15/008 , A61K2123/00
摘要： A group of functionalized polyamine chelants that form complexes with rhodium are disclosed. The rhodium complexes can be attached to an antibody or antibody fragment and used for therapeutic or diagnostic purposes.
摘要翻译：公开了一组与铑形成络合物的官能化多胺螯合剂。铑络合物可以连接到抗体或抗体片段上，并用于治疗或诊断目的。

10. 发明授权

US5435990A Macrocyclic congugates and their use as diagnostic and therapeutic agents 失效
标题翻译：大环偶联物及其作为诊断和治疗剂的用途
公开(公告)号：US5435990A
公开(公告)日：1995-07-25
申请号：US962168
申请日：1992-10-15
申请人： Roberta C. Cheng , William A. Fordyce , William F. Goeckleler , William J. Kruper, Jr. , Richard K. Frank , Joseph R. Garlich , Garry E. Kiefer , Kenneth McMillan , Jaime Simon , David A. Wilson , Sharon Braughman
发明人： Roberta C. Cheng , William A. Fordyce , William F. Goeckleler , William J. Kruper, Jr. , Richard K. Frank , Joseph R. Garlich , Garry E. Kiefer , Kenneth McMillan , Jaime Simon , David A. Wilson , Sharon Braughman
IPC分类号： A61K9/08 , A61K9/107 , A61K31/395 , A61K39/395 , A61K51/00 , A61K51/04 , A61K51/10 , A61P35/00 , C07D257/02 , C07K16/00 , A61M36/06 , C07K16/30
CPC分类号： C07D257/02 , A61K51/0482 , A61K51/1045 , A61K51/109 , A61K2121/00 , A61K2123/00
摘要： A group of functionalized macrocyclic polyaminocarboxylate chelants that form complexes with rare earth-type metal ions are disclosed. The complexes, covalently attached to an antibody or antibody fragment, can be used for therapeutic and/or diagnostic purposes for cancer.
摘要翻译：公开了与稀土类金属离子形成络合物的一组官能化的大环多胺羧酸盐螯合剂。与抗体或抗体片段共价连接的复合物可用于癌症的治疗和/或诊断目的。

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