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1. 发明申请

US20070039522A1 Reducing agent for the soluble chromate content of cement and methods for the production thereof 审中-公开
标题翻译：水泥可溶性铬酸盐含量的还原剂及其生产方法
公开(公告)号：US20070039522A1
公开(公告)日：2007-02-22
申请号：US10564651
申请日：2004-07-16
申请人： Michael Vossing , Gerhard Auer , Benno Laubach , Detlef Klein , Werner Schuy , Klaus Kollisch , Erwin Weiss , Werner Bahl , Philip Reese
发明人： Michael Vossing , Gerhard Auer , Benno Laubach , Detlef Klein , Werner Schuy , Klaus Kollisch , Erwin Weiss , Werner Bahl , Philip Reese
IPC分类号： C01G49/14 , C01G49/00 , C04B28/26 , C04B40/00
CPC分类号： C01B17/901 , C01G23/0532 , C01G49/14 , C01P2004/61 , C01P2004/62 , C04B22/149 , C04B28/02 , C04B2111/1081 , C22B7/04 , Y02P10/212 , C04B22/142
摘要： The invention relates to a reducing agent for the soluble chromate content of cement and to methods for the production thereof, which comprise concentrating an used sulfuric acid, containing iron(II) sulfate, and separating the sulfuric acid from the obtained precipitate which contains iron(II) sulfate.
摘要翻译：本发明涉及一种用于水泥的可溶性铬酸盐含量的还原剂及其制备方法，其包括浓缩含硫酸铁（II）的硫酸，并将硫酸与所得到的含铁沉淀物 II）硫酸盐。

2. 发明授权

US06673963B2 Process for preparing sorbic acid by thermal cleavage 失效
标题翻译：通过热裂解制备山梨酸的方法
公开(公告)号：US06673963B2
公开(公告)日：2004-01-06
申请号：US10237336
申请日：2002-09-09
申请人： Daniel Decker , Guenter Roscher , Christoph Mollenkopf , Erwin Weiss , Stefan Purps
发明人： Daniel Decker , Guenter Roscher , Christoph Mollenkopf , Erwin Weiss , Stefan Purps
IPC分类号： C07C5710
CPC分类号： C07C51/09 , C07C57/10
摘要： The invention relates to a process for preparing sorbic acid by thermal cleavage in a solvent of the polyester prepared from crotonaldehyde and ketene, the cleavage of the polyester being carried out in the presence of 20 to 100% by weight of a secondary or tertiary aliphatic, alicyclic nitrogen- and/or oxygen-containing amine, or aliphatic-aromatic substituted amine, as catalyst.
摘要翻译：本发明涉及通过在由巴豆醛和乙烯酮制备的聚酯的溶剂中热裂解制备山梨酸的方法，该聚酯在20至100重量％的仲或叔脂族，脂环族氮和/或含氧胺或脂族 - 芳族取代的胺作为催化剂。

3. 发明授权

US4847419A Process for the preparation of bifunctional tertiary aromatic phosphine sulfides, and also several specific representatives of this class of compounds 失效
标题翻译：双官能叔芳基硫化膦的制备方法，以及这类化合物的几个具体代表
公开(公告)号：US4847419A
公开(公告)日：1989-07-11
申请号：US004167
申请日：1987-01-15
申请人： Erwin Weiss , Hans-Jerg Kleiner
发明人： Erwin Weiss , Hans-Jerg Kleiner
IPC分类号： C07F9/53 , C08G65/40
CPC分类号： C07F9/5325
摘要： A compound of the formula I, ##STR1## in which X is F, Cl or Br,R is alkyl having from 1 to 5 carbon atoms, aryl, aryloxy or aralkyl andn is an integer from 1 to 5, a plurality of R representing equal or different of said substituents and a process for preparing them.
摘要翻译：式I化合物，其中X为F，Cl或Br，R为具有1至5个碳原子的烷基，芳基，芳氧基或芳烷基，n为1至5的整数，多个R表示相同或不同的所述取代基，以及其制备方法。

4. 发明授权

US08808451B2 Reducing agent for the soluble chromate content of cement and methods for production thereof 有权
标题翻译：水泥可溶性铬酸盐含量的还原剂及其生产方法
公开(公告)号：US08808451B2
公开(公告)日：2014-08-19
申请号：US13371783
申请日：2012-02-13
申请人： Michael Vössing , Auer Gerhard , Benno Laubach , Detlef Klein , Werner Schuy , Klaus Köllisch , Erwin Weiss , Werner Bahl , Philip Reese
发明人： Michael Vössing , Auer Gerhard , Benno Laubach , Detlef Klein , Werner Schuy , Klaus Köllisch , Erwin Weiss , Werner Bahl , Philip Reese
IPC分类号： C04B22/08 , C04B14/00
CPC分类号： C01B17/901 , C01G23/0532 , C01G49/14 , C01P2004/61 , C01P2004/62 , C04B22/149 , C04B28/02 , C04B2111/1081 , C22B7/04 , Y02P10/212 , C04B22/142
摘要： The invention relates to a reducing agent for the soluble chromate content of cement and to methods for the production thereof, which comprise concentrating an used sulfuric acid, containing iron (II) sulfate, and separating the sulfuric acid from the obtained precipitate which contains iron (II) sulfate.
摘要翻译：本发明涉及一种用于水泥的可溶性铬酸盐含量的还原剂及其制备方法，其包括浓缩含硫酸铁（II）的硫酸，并将硫酸与所得到的含铁沉淀物 II）硫酸盐。

5. 发明授权

US4526728A 2-Acrylamido- and 2-methacrylamido-2-methyl propanephosphonic acids and their salts, process for the preparation thereof, and use thereof for the manufacture of copolymers 失效
标题翻译： 2-丙烯酰氨基 - 和2-甲基丙烯酰胺基-2-甲基丙膦酸及其盐，其制备方法及其在制备共聚物中的用途
公开(公告)号：US4526728A
公开(公告)日：1985-07-02
申请号：US596895
申请日：1984-04-05
申请人： Manfred Finke , Walter Rupp , Erwin Weiss
发明人： Manfred Finke , Walter Rupp , Erwin Weiss
IPC分类号： C07F9/38 , C08F30/02 , C08G63/00 , C08G63/44
CPC分类号： C08F30/02 , C07F9/3808
摘要： 2-(Meth)acrylamido-2-methylpropanephosphonic acid is prepared by reaction of 2-methylprop-1-ene-1-phosphonic acid or 2-methylpro-2-ene-1-phosphonic acid with (meth)acrylonitrile in the presence of an equimolar amount of a strong acid. The compounds are suitable as such or in the form of their salts as comonomer for the manufacture of copolymers, which are used inter alia as dyeing auxiliaries and as scale inhibitors.
摘要翻译： 2-（甲基）丙烯酰氨基-2-甲基丙烷膦酸通过2-甲基丙-1-烯-1-膦酸或2-甲基丙-2-烯-1-膦酸与（甲基）丙烯腈在存在下反应制备等摩尔量的强酸。化合物本身或其盐的形式是共聚单体的形式，用于制备共聚物，其尤其用作染色助剂和作为阻垢剂。

6. 发明授权

US4806691A Process for the preparation of tertiary phosphine oxides 失效
标题翻译：制备叔氧化膦的方法
公开(公告)号：US4806691A
公开(公告)日：1989-02-21
申请号：US905170
申请日：1986-09-09
申请人： Erwin Weiss
发明人： Erwin Weiss
IPC分类号： C07F9/53
CPC分类号： C07F9/53
摘要： Tertiary phosphine oxides are prepared by oxidation of tertiary phosphine sulfides using H.sub.2 O.sub.2 in a solvent comprising about 2-20% by weight of optionally halogenated lower aliphatic carboxylic acids and the remainder of mono- or polyhydric aliphatic or cycloaliphatic alcohols--if appropriate in mixtures with other inert solvents which are miscible with the carboxylic acid/alcohol mixture. Preferred solvents comprise acetic acid/methanol and acetic acid/ethanol mixtures.The reaction products are final products and intermediates products in various specialized fields such as, for example, the plant protection sector and the polymers sector.
摘要翻译：通过使用H 2 O 2在包含约2-20重量％的任选卤代的低级脂族羧酸的溶剂中氧化叔膦硫化物并且其余的一元或多元脂族或脂环族醇 - 如果合适地与其它物质的混合物与羧酸/醇混合物可混溶的惰性溶剂。优选的溶剂包括乙酸/甲醇和乙酸/乙醇混合物。反应产物是各种专业领域的最终产品和中间体产品，例如植物保护部门和聚合物部门。

7. 发明授权

US4675446A Process for the preparation of tertiary phosphine oxides 失效
标题翻译：制备叔氧化膦的方法
公开(公告)号：US4675446A
公开(公告)日：1987-06-23
申请号：US756323
申请日：1985-07-18
申请人： Erwin Weiss
发明人： Erwin Weiss
IPC分类号： C07F9/53
CPC分类号： C07F9/53
摘要： Tertiary phosphine oxides are prepared by the oxidation of tertiary phosphine sulfides with H.sub.2 O.sub.2 in a solvent composed of at least about 20% by weight, preferably at least about 50% by weight, of optionally halogenated, lower aliphatic carboxylic acids and/or their anhydrides; it is particularly preferred if the solvent is composed only of acetic acid.The reaction products are end products and intermediates in a variety of areas such as, for example, the sectors of plant protection and polymers.
摘要翻译：叔膦氧化物是通过在由至少约20重量％，优选至少约50重量％的任选卤代的低级脂族羧酸和/或其酸酐的至少约50重量％的溶剂中用H 2 O 2氧化叔膦硫化物来制备的。特别优选的是，溶剂仅由乙酸组成。反应产物是各种领域的终产物和中间体，例如植物保护和聚合物领域。

8. 发明授权

US4761252A Process for the preparation of vinylphosphonic dichloride 失效
标题翻译：乙烯基膦酸二氯化物的制备方法
公开(公告)号：US4761252A
公开(公告)日：1988-08-02
申请号：US90229
申请日：1987-08-27
申请人： Herbert Siegel , Erwin Weiss , Harald Berger
发明人： Herbert Siegel , Erwin Weiss , Harald Berger
IPC分类号： B01J27/08 , B01J27/138 , B01J31/00 , B01J31/02 , C07B61/00 , C07F9/42
CPC分类号： C07F9/42
摘要： The invention relates to a process for the preparation of vinylphosphonic dichloride, in which a 2-chloroethanephosphonate of the formula ##STR1## or a mixture of the two esters, is reacted with thionyl chloride at a temperature of 60.degree. to 160.degree. C. in the presence of a catalyst which contains tertiary phosphines, quaternary ammonium or phosphonium salts or alkali metal or alkaline-earth metal halides.During this reaction, any thionyl chloride which may be present is removed by distillation subsequent to this reaction, the mixture remaining is heated to 140.degree. to 200.degree. C., and the vinylphosphonic dichloride produced during this is removed by distillation.
摘要翻译：本发明涉及一种制备乙烯基膦酸二氯化物的方法，其中将式（II）的2-氯乙基膦酸盐或两种酯的混合物与亚硫酰氯在60至160℃的温度下反应。在含有叔膦，季铵或鏻盐或碱金属或碱土金属卤化物的催化剂的存在下。在该反应中，在该反应之后，通过蒸馏除去可能存在的任何亚硫酰氯，将剩余的混合物加热至140℃至200℃，并通过蒸馏除去其中产生的乙烯基膦酰氯。

9. 发明授权

US4761251A Process for the preparation of vinylphosphonic dichloride 失效
标题翻译：乙烯基膦酸二氯化物的制备方法
公开(公告)号：US4761251A
公开(公告)日：1988-08-02
申请号：US089964
申请日：1987-08-27
申请人： Herbert Siegel , Erwin Weiss , Harald Berger
发明人： Herbert Siegel , Erwin Weiss , Harald Berger
IPC分类号： B01J31/00 , C07B61/00 , C07F9/42
CPC分类号： C07F9/42
摘要： The invention relates to a process for the preparation of vinylphosphonic dichloride through elimination of hydrogen chloride from 2-chloroethanephosphonic dichloride in the presence of catalysts. The catalysts used are tertiary phosphines, quaternary ammonium or phosphonium salts or alkali metal or alkaline-earth metal halides. When triphenyl phosphine is used as the catalyst, the reaction is carried out under reduced pressure at a temperature of 130.degree. to 166.degree. C. and the vinylphosphonic dichloride produced is simultaneously removed by distillation under reduced pressure. When the other catalysts are used, the process can be carried out at atmospheric pressure or reduced pressure and at temperatures of about 130.degree. to 220.degree. C. and the vinylphosphonic dichloride produced can be removed by distillation simultaneously with or subsequent to the reaction.
摘要翻译：本发明涉及通过在催化剂存在下从2-氯乙烷膦酸二氯中除去氯化氢来制备乙烯基膦酸二氯化物的方法。所用的催化剂是叔膦，季铵或鏻盐或碱金属或碱土金属卤化物。当使用三苯基膦作为催化剂时，反应在130〜166℃的温度下进行减压蒸馏，同时通过减压蒸馏同时除去生成的乙烯基膦酸二氯。当使用其它催化剂时，该方法可以在大气压或低压下和在约130℃至220℃的温度下进行，并且所产生的乙烯基膦酸二氯化物可以在反应或反应后同时通过蒸馏除去。

10. 发明授权

US4749524A Process for the preparation of 2-chloroethanephosphonic dichloride 失效
标题翻译： 2-氯乙烷膦酸二氯化物的制备方法
公开(公告)号：US4749524A
公开(公告)日：1988-06-07
申请号：US89827
申请日：1987-08-27
申请人： Herbert Siegel , Erwin Weiss , Harald Berger
发明人： Herbert Siegel , Erwin Weiss , Harald Berger
IPC分类号： B01J27/00 , B01J27/08 , B01J27/138 , B01J31/00 , B01J31/02 , C07B61/00 , C07F9/42
CPC分类号： C07F9/42
摘要： The invention relates to a process for the preparation of 2-chloroethanephosphonic dichloride through reaction of a 2-chloroethanephosphonate of the formula ##STR1## or a mixture of the two esters, with thionyl chloride at a temperature of 60.degree. to 160.degree. C. In this reaction, tertiary phosphines, quaternary ammonium or phosphonium salts or alkali metal or alkaline-earth metal halides are employed as catalysts. The thionyl chloride is introduced into the initially introduced ester.
摘要翻译：本发明涉及一种制备2-氯乙烷膦酸二氯化物的方法，该方法是将式（Ⅱ）所示的2-氯乙基膦酸酯与式（Ⅱ）的混合物与亚硫酰氯反应，温度为60℃至 160℃。在该反应中，使用叔膦，季铵或鏻盐或碱金属或碱土金属卤化物作为催化剂。将亚硫酰氯引入初始引入的酯中。

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