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1. 发明授权

US08193119B2 Acid combination one step reaction process for agricultural use products and associated methods 有权
标题翻译：酸性组合农业用途一步反应过程及相关方法
公开(公告)号：US08193119B2
公开(公告)日：2012-06-05
申请号：US13035779
申请日：2011-02-25
申请人： Carl J. Fabry , Vaughn Astley
发明人： Carl J. Fabry , Vaughn Astley
IPC分类号： C05D1/00 , C01B25/163
CPC分类号： A01N59/26 , C05B13/00 , C05B17/00 , C05G3/02
摘要： A process for the manufacture of an aqueous composition that is a combination of a fungicide and fertilizer comprising the following steps: (1) dissolving phosphorous acid in phosphoric acid to form a solution of an acid mixture; (2) reacting the acid mixture of step (1) with an aqueous potassium hydroxide solution at a temperature of about 65° C. to about 260° C. in a continuous reactor while maintaining the ratio of potassium to phosphorous in various mole ratios thereby forming a reaction mixture comprising potassium phosphates, potassium polyphosphates, potassium phosphites, and potassium polyphosphites and potassium phosphate phosphite copolymers; and, (3) cooling the reaction mixture rapidly at least 1° C. to 60° C., to below about 35° C. to about 65° C. Using a similar process a composition having fungicidal properties is prepared by reaction phosphoric acid with potassium hydroxide.The reaction mixtures prepared according to each of the above processes are also part of this invention.
摘要翻译：一种制备杀真菌剂和肥料的组合的水性组合物的方法，包括以下步骤：（1）将磷酸溶解在磷酸中以形成酸混合物的溶液; （2）在连续反应器中，在约65℃至约260℃的温度下使步骤（1）的酸混合物与氢氧化钾水溶液反应，同时保持钾与磷的摩尔比的比例形成包含磷酸钾，多磷酸钾，亚磷酸钾和多磷酸钾和磷酸亚磷酸钾共聚物的反应混合物; 和（3）将反应混合物快速冷却至少1℃至60℃，至约35℃至约65℃。使用类似方法，通过反应磷酸制备具有杀真菌性质的组合物与氢氧化钾。根据上述方法制备的反应混合物也是本发明的一部分。

2. 发明申请

US20110183843A1 ACID COMBINATION ONE STEP REACTION PROCESS FOR AGRICULTURAL USE PRODUCTS AND ASSOCIATED METHODS 有权
标题翻译：酸化组合农用产品及相关方法的一步反应方法
公开(公告)号：US20110183843A1
公开(公告)日：2011-07-28
申请号：US13035779
申请日：2011-02-25
申请人： Carl J. Fabry , Vaughn Astley
发明人： Carl J. Fabry , Vaughn Astley
IPC分类号： A01N59/26
CPC分类号： A01N59/26 , C05B13/00 , C05B17/00 , C05G3/02
摘要： A process for the manufacture of an aqueous composition that is a combination of a fungicide and fertilizer comprising the following steps: (1) dissolving phosphorous acid in phosphoric acid to form a solution of an acid mixture; (2) reacting the acid mixture of step (1) with an aqueous potassium hydroxide solution at a temperature of about 65° C. to about 260° C. in a continuous reactor while maintaining the ratio of potassium to phosphorous in various mole ratios thereby forming a reaction mixture comprising potassium phosphates, potassium polyphosphates, potassium phosphites, and potassium polyphosphites and potassium phosphate phosphite copolymers; and, (3) cooling the reaction mixture rapidly at least 1° C. to 60° C., to below about 35° C. to about 65° C. Using a similar process a composition having fungicidal properties is prepared by reaction phosphoric acid with potassium hydroxide.The reaction mixtures prepared according to each of the above processes are also part of this invention.
摘要翻译：一种制备杀真菌剂和肥料的组合的水性组合物的方法，包括以下步骤：（1）将磷酸溶解在磷酸中以形成酸混合物的溶液; （2）在连续反应器中，在约65℃至约260℃的温度下使步骤（1）的酸混合物与氢氧化钾水溶液反应，同时保持钾与磷的摩尔比的比例形成包含磷酸钾，多磷酸钾，亚磷酸钾和多磷酸钾和磷酸亚磷酸钾共聚物的反应混合物; 和（3）将反应混合物快速冷却至少1℃至60℃，至约35℃至约65℃。使用类似方法，通过反应磷酸制备具有杀真菌性质的组合物与氢氧化钾。根据上述方法制备的反应混合物也是本发明的一部分。

3. 发明授权

US08216972B1 Acid combination one step reaction process for agricultural use products and associated methods 有权
标题翻译：酸性组合农业用途一步反应过程及相关方法
公开(公告)号：US08216972B1
公开(公告)日：2012-07-10
申请号：US13094932
申请日：2011-04-27
申请人： Carl J. Fabry , Vaughn Astley
发明人： Carl J. Fabry , Vaughn Astley
IPC分类号： C05D1/00 , C01B25/163
CPC分类号： C05B13/00 , A01N25/02 , A01N37/40 , A01N59/26 , C05B17/00 , C05C3/00 , C05D1/00 , C05D5/00 , C05G3/0064 , C05G3/02 , C05D9/02 , A01N2300/00
摘要： A process for the manufacture of an aqueous composition that is a combination of a fungicide and fertilizer comprising the following steps: (1) dissolving phosphorous acid in phosphoric acid to form a solution of an acid mixture; (2) reacting the acid mixture of step (1) with an aqueous hydroxide solution creating an exothermic reaction under pressure; and, (3) cooling the reaction product to between about 35° C. to about 65° C. The reaction product prepared according to the above process can also be used as a bactericide.
摘要翻译：一种制备杀真菌剂和肥料的组合的水性组合物的方法，包括以下步骤：（1）将磷酸溶解在磷酸中以形成酸混合物的溶液; （2）使步骤（1）的酸混合物与氢氧化水溶液反应，在压力下产生放热反应; 和（3）将反应产物冷却至约35℃至约65℃。根据上述方法制备的反应产物也可用作杀菌剂。

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