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1. 发明申请

US20120107599A1 Fine Carbon Fiber with Linearity and Resin Composite Material Using the Same 有权
标题翻译：具有线性的细碳纤维和使用其的树脂复合材料
公开(公告)号：US20120107599A1
公开(公告)日：2012-05-03
申请号：US13312719
申请日：2011-12-06
申请人： Koichiro YONETAKE , Tatsuhiro TAKAHASHI , Ryuji YAMAMOTO , Toshio MORITA
发明人： Koichiro YONETAKE , Tatsuhiro TAKAHASHI , Ryuji YAMAMOTO , Toshio MORITA
IPC分类号： B32B9/00 , B32B27/04 , D01F9/12
CPC分类号： B82Y30/00 , B29C70/14 , D01F9/127 , D01F9/1276 , D04H13/00 , Y10T428/249924 , Y10T428/249927 , Y10T428/24994 , Y10T428/249945 , Y10T428/2916 , Y10T428/2918 , Y10T428/2933 , Y10T428/294 , Y10T428/2958 , Y10T428/30
摘要： A fine carbon fiber having linearity, each fiber filament of the carbon fiber having a bending angle of 30° or less with respect to the longitudinal direction of the fiber filament, and including a hollow space extending along its axis, and having an outer diameter of 1 to 1,000 nm, an aspect ratio of 5 to 1,000, and a BET specific surface area of 2 to 2,000 m2/g, wherein the average interlayer distance (d002) of the carbon fiber at a (002) plane is 0.345 nm or less as measured by means of X-ray diffractometry, and the ratio of the peak height (Id) of the band at 1,341 to 1,349 cm−1 in a Raman scattering spectrum of the carbon fiber to that of the peak height (Ig) of the band at 1,570 to 1,578 cm−1 in the spectrum (Id/Ig) is 0.1 to 2. The fiber exhibits excellent dispersibility in a matrix.
摘要翻译：具有线性的细碳纤维，碳纤维的纤维长丝相对于纤维长丝的长度方向具有30°以下的弯曲角度，并且包括沿其轴线延伸的中空空间，并且具有外径 1〜1000nm，长宽比为5〜1000，BET比表面积为2〜2000m 2 / g，其中，（002）面上的碳纤维的平均层间距离（d002）为0.345nm以下如通过X射线衍射法测定的，并且在碳纤维的拉曼散射光谱中，在1,341〜1349cm -1处的条带的峰高（Id）与峰高（Ig）的峰高光谱（Id / Ig）中的1570至1,578cm -1的谱带为0.1至2.该纤维在基质中表现出优异的分散性。

2. 发明授权

US08149983B2 Method for analysis of pellet-cladding interaction 有权
标题翻译：颗粒 - 包层相互作用分析方法
公开(公告)号：US08149983B2
公开(公告)日：2012-04-03
申请号：US11447357
申请日：2006-06-06
申请人： Charles L. Beard, Jr. , Toshio Morita , R. Wade Miller
发明人： Charles L. Beard, Jr. , Toshio Morita , R. Wade Miller
IPC分类号： G21C9/00
CPC分类号： G21C17/00 , G21C2003/047 , G21D3/001 , G21Y2002/202 , G21Y2004/40 , Y02E30/39
摘要： A method is provided for evaluating pellet-cladding interaction (PCI) in a nuclear core having a reactor protection system and a plurality of elongated fuel rods each having fuel surrounded by cladding with a gap therebetween. The method includes: selecting a number of core parameters to be analyzed; evaluating the selected parameters at a plurality of statepoints; generating a model of an operating space of the core based, at least in part, upon the statepoints; selecting a subset or loci of statepoints from the model wherein each of the statepoints of the loci of statepoints, when subjected to a predetermined transient, falls within the operational limits of the reactor protection system; and evaluating the loci of statepoints for PCI in response to the transient. In this manner, the potential for PCI can be accurately determined without requiring every statepoint for every fuel rod in the core to be individually analyzed.
摘要翻译：提供了一种用于评估具有反应器保护系统的核芯中的颗粒 - 包层相互作用（PCI）的方法，以及多个细长燃料棒，每个细长的燃料棒具有围绕其间具有间隙的包层。该方法包括：选择要分析的多个核心参数; 在多个状态点评估所选择的参数; 至少部分地基于状态点生成核心的操作空间的模型; 从模型中选择状态点的子集或轨迹，其中当受到预定瞬变时，状态点的轨迹中的每个状态点落入反应堆保护系统的操作限度内; 并针对短暂性评估评估PCI的状态点位置。以这种方式，可以准确地确定PCI的潜力，而不需要对芯中的每个燃料棒进行单独分析的每个状态点。

3. 发明授权

US07879442B2 Composite of vapor grown carbon fiber and inorganic fine particle and use thereof 有权
标题翻译：气相生长碳纤维和无机细颗粒的复合物及其用途
公开(公告)号：US07879442B2
公开(公告)日：2011-02-01
申请号：US10571700
申请日：2004-09-15
申请人： Toshio Morita , Chiaki Sotowa , Ryuji Yamamoto
发明人： Toshio Morita , Chiaki Sotowa , Ryuji Yamamoto
IPC分类号： B32B5/16 , D02G3/00 , H01M4/58
CPC分类号： D06M11/36 , B82Y30/00 , C01B32/16 , C08J5/042 , C08J5/06 , C08J2377/00 , D01F9/127 , D01F11/12 , D06M11/00 , D06M11/42 , D06M11/44 , D06M11/45 , D06M11/46 , D06M11/47 , D06M11/48 , D06M11/49 , D06M11/76 , D06M11/79 , D06M23/08 , D06M2101/40 , Y10T428/2913 , Y10T428/2918 , Y10T428/2927 , Y10T428/2973 , Y10T428/2989 , Y10T428/2991
摘要： The present invention relates to a composite of vapor grown carbon fiber and inorganic fine particles comprising vapor grown carbon fiber, each fiber filament of the carbon fiber having a structure with hollow space extending along its axis, a diameter of 0.001 to 1 μm and an aspect ratio of 5 to 15,000; and inorganic fine particles having a particle size of 0.0001 to 5 μm, the particles being deposited onto the surface of the carbon fiber, wherein the ratio of the average diameter of the vapor grown carbon fiber to the average particle size of the inorganic fine particles is 1 0.01 to 1:5; the ratio by mass of the vapor grown carbon fiber to the inorganic fine particles is 1:0.005 to 1:50; and the carbon crystal structure of the carbon fiber is maintained and the surface characteristics are modified.
摘要翻译：本发明涉及气相生长碳纤维和包含气相生长碳纤维的无机细颗粒的复合物，碳纤维的每个纤维长丝具有沿其轴线延伸的中空空间的结构，直径为0.001至1μm，比例为5至15,000; 和粒径为0.0001〜5μm的无机细颗粒，将颗粒沉积在碳纤维的表面上，其中气相生长碳纤维的平均直径与无机细颗粒的平均粒径之比为 1 0.01〜1:5; 气相生长碳纤维与无机细颗粒的质量比为1:0.005〜1:50; 并且保持碳纤维的碳晶体结构并改变表面特性。

4. 发明授权

US07846415B2 Production method of vapor-grown carbon fiber and apparatus therefor 有权
标题翻译：气相生长碳纤维的生产方法及其设备
公开(公告)号：US07846415B2
公开(公告)日：2010-12-07
申请号：US11658231
申请日：2005-07-22
申请人： Eiji Kambara , Tomoaki Yoshida , Toshio Morita
发明人： Eiji Kambara , Tomoaki Yoshida , Toshio Morita
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , D01F9/127 , D01F9/1272 , D01F9/1276 , D01F9/133
摘要： The invention provides a method of producing vapor grown carbon fiber by vapor-phase reaction conducted by supplying carbon source compounds and a catalyst or a catalyst precursor into a heating zone, wherein at least one of the carbon source compound and the catalyst or the catalyst precursor is solid at room temperature and the solid compound is supplied in gas form into the heating zone from a material supplier filled with the solid material alone at a constant amount. The production method according to the invention enables efficient and stable production of vapor phase carbon fiber even by using a high-volume production equipment.
摘要翻译：本发明提供了一种通过气相反应生产气相生长碳纤维的方法，其通过将碳源化合物和催化剂或催化剂前体供给到加热区中进行，其中至少一种碳源化合物和催化剂或催化剂前体在室温下为固体，固体化合物以固体量从填充有固体材料的材料供应器以气体形式供应到加热区中。根据本发明的制造方法，即使通过使用大批量的生产设备也能够有效且稳定地生产气相碳纤维。

5. 发明授权

US07524479B2 Method for producing vapor grown carbon fiber 失效
标题翻译：生产气相生长碳纤维的方法
公开(公告)号：US07524479B2
公开(公告)日：2009-04-28
申请号：US10475777
申请日：2002-06-26
申请人： Kazuo Muramaki , Yoshihisa Sakamoto , Ryuji Yamamoto , Toshio Morita
发明人： Kazuo Muramaki , Yoshihisa Sakamoto , Ryuji Yamamoto , Toshio Morita
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , D01F9/127 , D01F9/133
摘要： A method for producing vapor grown carbon, including mixing a raw material gas containing an organic compound and an organo-transition metallic compound preliminarily heated preferably to a temperature of 100 to 450° C. with a carrier gas heated preferably to a temperature of 700 to 1,600° C., and introducing the resultant gas mixture into a carbon fiber production zone, wherein preferably a mixture of an aromatic compound and acetylene, ethylene, or butadiene is used as an organic compound. The method can include dissolving the transition metallic compound in a solvent, atomizing the resultant solution into fine droplets, evaporating the solvent in the droplets to thereby obtain fine particles of the transition metal compound, and introducing the drifting particles with an organic compound gas into the carbon fiber production zone. Vapor grown carbon fiber is thereby produced.
摘要翻译：一种生产气相生长碳的方法，包括将预先加热至100至450℃的预先加热的有机化合物的原料气体和有机过渡金属化合物与优选加热至700℃的载气混合， 1600℃，将所得气体混合物引入碳纤维生产区，其中优选使用芳香族化合物和乙炔，乙烯或丁二烯的混合物作为有机化合物。该方法可以包括将过渡金属化合物溶解在溶剂中，将所得溶液雾化成微小液滴，蒸发液滴中的溶剂，从而获得过渡金属化合物的细颗粒，并将漂移颗粒与有机化合物气体引入碳纤维生产区。由此生成气相生长的碳纤维。

6. 发明申请

US20080226537A1 Fine carbon fiber, method for producing the same and electrically conducting material comprising the fine carbon fiber 审中-公开
标题翻译：细碳纤维，其制造方法和包含细碳纤维的导电材料
公开(公告)号：US20080226537A1
公开(公告)日：2008-09-18
申请号：US12153131
申请日：2008-05-14
申请人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
发明人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , D01F9/127 , Y10T428/2913 , Y10T428/2918 , Y10T428/2924 , Y10T428/2929 , Y10T428/30
摘要： A fine carbon fiber having an outer diameter of about 1 to about 80 nm and an aspect ratio of 10 to 30,000, comprising a hollow center portion and a multi-layer sheath structure of a plurality of carbon layers, the layers forming annual rings, wherein the sheath-forming carbon layers form an incomplete sheath, i.e., the carbon layers are partially broken or disrupted in a longitudinal direction, and the outer diameter of the carbon fiber and/or the diameter of the hollow center portion are not uniform in a longitudinal direction. The carbon fiber is obtained by instantaneously reacting a carrier gas at a high temperature and an organic compound gas kept at a temperature below the decomposition temperature of the transition metal compound and has a conductivity equivalent to that of a conventional vapor phase method and is useful as a filler material in resins, rubbers, paints and the like.
摘要翻译：外径约1〜约80nm，纵横比为10〜30,000的细碳纤维，其包含多个碳层的中空中心部分和多层护套结构，所述层形成年轮，其中，鞘形成碳层形成不完整的护套，即碳层在纵向上部分断裂或破裂，并且碳纤维的外径和/或中空中心部分的直径在纵向上不均匀方向。碳纤维通过使高温下的载气和保持在低于过渡金属化合物的分解温度的温度的有机化合物气体瞬时反应而获得，并且具有与常规气相法相当的导电性，可用作树脂，橡胶，油漆等中的填充材料。

7. 发明授权

US07390593B2 Fine carbon fiber, method for producing the same and use thereof 有权
标题翻译：细碳纤维，其制造方法及其应用
公开(公告)号：US07390593B2
公开(公告)日：2008-06-24
申请号：US10494810
申请日：2002-11-06
申请人： Ryuji Yamamoto , Toshio Morita
发明人： Ryuji Yamamoto , Toshio Morita
IPC分类号： D01F9/12 , H01B1/04 , C01B31/00
CPC分类号： D01F11/12 , B01J20/20 , B01J20/28014 , B82Y30/00 , B82Y40/00 , C01B3/0021 , C01B32/15 , C08K7/06 , C08K2201/016 , D01F9/127 , H01M4/583 , H01M4/587 , H01M4/625 , Y02E60/325 , Y10S977/745 , Y10S977/843
摘要： A vapor grown fine carbon fiber, each fiber filament of the carbon fiber comprising, in its interior, a hollow space extending along the fiber filament, and having a multi-layer structure, an outer diameter of 2 to 500 nm, and an aspect ratio of 1 to 100, wherein the fiber filament comprises a cut portion on its surface along the hollow space, a production method therefor, and electrically conductive material, a secondary battery and a gas occlusion material using the carbon fiber. The fine carbon fiber of the present invention is excellent in properties such as occlusion of gases such as hydrogen and methane, smoothness, electrical conductivity and thermal conductivity, and also excellent in dispersability, wettability and adhesion with a matrix such as resin.
摘要翻译：气相生长的细碳纤维，碳纤维的每个纤维长丝在其内部包括沿着纤维长丝延伸的中空空间，并且具有多层结构，外径为2至500nm，纵横比为1〜100，其中纤维长丝在其中空空间的表面上包括切割部分，其制造方法，以及使用碳纤维的导电材料，二次电池和气体闭塞材料。本发明的细碳纤维的特性如氢气，甲烷等气体的阻塞性，平滑性，导电性和导热性，以及分散性，润湿性和与树脂等基体的粘合性优异。

8. 发明申请

US20070014522A1 Optical DVI cable system and method of laying cable 失效
标题翻译：光学DVI电缆系统及敷设电缆的方法
公开(公告)号：US20070014522A1
公开(公告)日：2007-01-18
申请号：US11486393
申请日：2006-07-14
申请人： Hideki Yamaguchi , Hideya Konda , Toshio Morita , Satoshi Koide , Nobuhiko Utagawa
发明人： Hideki Yamaguchi , Hideya Konda , Toshio Morita , Satoshi Koide , Nobuhiko Utagawa
IPC分类号： G02B6/36
CPC分类号： G02B6/3817 , G02B6/3885 , G02B6/3887 , G02B6/4292 , G02B6/4416
摘要： A composite cable 21 with a plug 22 attached thereto includes optical fibers, metal wires, a tensile strength fiber 21a, and an envelope 21b for enveloping them and the plug 22 includes a ferrule 210 of the plug for connecting the optical fiber, a cable clamp 221 and a Kevler holder 222 (first fixing mechanism) for fixing the tensile strength fiber 21a, and a gasket 223 (second fixing mechanism) for blocking a twist of the envelope 21b and further includes a joint mechanism (227) of a detachable traction cap for pulling the composite cable 21 and inserting the composite cable 21 into piping.
摘要翻译：具有安装有插头22的复合电缆21包括光纤，金属线，拉伸强度纤维21a和用于包封它们的外壳21b，插头22包括用于连接光纤的插头的套圈210，电缆夹221和用于固定拉伸强度纤维21a的凯夫勒支架222（第一固定机构）和用于阻挡外壳21b的扭曲的垫圈223（第二固定机构），还包括：接头机构用于拉动复合电缆21并将复合电缆21插入管道的可拆卸牵引盖。

9. 发明授权

US07150911B2 Electrical insulating vapor grown carbon fiber and method for producing the same, and use thereof 失效
公开(公告)号：US07150911B2
公开(公告)日：2006-12-19
申请号：US10067266
申请日：2002-02-07
申请人： Toshio Morita , Hitoshi Inoue , Ryuji Yamamoto
发明人： Toshio Morita , Hitoshi Inoue , Ryuji Yamamoto
IPC分类号： B32B9/00 , D01F9/12
CPC分类号： C30B23/007 , B82Y30/00 , C30B29/02 , C30B29/605 , C30B33/00 , D01F9/127 , Y10T428/249924 , Y10T428/2918 , Y10T428/292 , Y10T428/2933 , Y10T428/30
摘要： An electrical insulating vapor grown carbon fiber containing a vapor grown carbon fiber having a fiber diameter of 0.01 to 0.5 μm, wherein the surface thereof is partially or entirely coated with an electrical insulating material and a method of producing thereof is disclosed.

10. 发明申请

US20060235135A1 Resin crystallization promoter and resin composition 审中-公开
标题翻译：树脂结晶促进剂和树脂组合物
公开(公告)号：US20060235135A1
公开(公告)日：2006-10-19
申请号：US10554063
申请日：2004-04-23
申请人： Tatsuhiro Takahashi , Toshio Morita
发明人： Tatsuhiro Takahashi , Toshio Morita
IPC分类号： C08K3/04
CPC分类号： C08K7/06 , C08K2201/016
摘要： The present invention relates to a thermoplastic resin crystallization promoter comprising fine carbon fiber consisting of fiber filaments having a diameter of 0.001 μm to 5 μm and an aspect ratio of 5 to 15,000, a thermoplastic resin composition consisting of the fine carbon fiber and thermoplastic resin and comprising crystallized resin, and a production method thereof. The crystallization promoter comprising the fine carbon fiber of the present invention enables to crystallize even an amorphous resin, which has an irregular molecular structure and therefore is not crystallized, or which exhibits low crystallization degree and therefore is difficult to crystallize by means of a conventional crystallization promoter. The crystallization promoter provides a thermoplastic resin composition, which, when molded, exhibits improved strength and tribological characteristics and is further reinforced when mixed with a filler.
摘要翻译：本发明涉及一种热塑性树脂结晶促进剂，其包含由直径为0.001〜5μm的纤维长丝和5〜15000的纵横比构成的细碳纤维，由细碳纤维和热塑性树脂构成的热塑性树脂组合物和包括结晶树脂及其制备方法。包含本发明的细碳纤维的结晶促进剂甚至能够使具有不规则分子结构的非晶性树脂结晶，因此不结晶，或者结晶度低，因此难以通过常规结晶结晶启动子。结晶促进剂提供了一种热塑性树脂组合物，其在模制时表现出改进的强度和摩擦学特性，并且当与填料混合时进一步增强。

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