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1. 发明申请

US20130065054A1 Process for Producing Poly(Arylene Sulfide), and Poly(Arylene Sulfide) 有权
标题翻译：生产聚（亚硫酰亚胺）和聚（亚硫酰亚胺）的方法
公开(公告)号：US20130065054A1
公开(公告)日：2013-03-14
申请号：US13698600
申请日：2011-04-21
申请人： Yoshihiro Ichinose , Masanori Kobayashi , Tomoyoshi Koizumi , Mitsuhiro Matsuzaki
发明人： Yoshihiro Ichinose , Masanori Kobayashi , Tomoyoshi Koizumi , Mitsuhiro Matsuzaki
IPC分类号： C08G75/16
CPC分类号： C08G75/0254 , C08G75/0213 , C08G75/0259 , C08G75/0281 , Y10T428/2982
摘要： Disclosed is a process for producing poly(arylene sulfide) which includes: a polymerization step of polymerizing a dihalogenated aromatic compound and at least one sulfur source selected from the group consisting of alkali metal sulfides and alkali metal hydrogen sulfides in an organic amide solvent, preferably in the presence of a phase separating agent; a separation step of separating a polymer from a reaction liquid containing a produced polymer after the polymerization step; a washing step of washing the polymer with a washing liquid that consists of water and/or an organic solvent; and a separated liquid treatment step of bringing both a separated liquid that has been recovered after the separation of the polymer in the separation step and a separated liquid containing a wash waste liquid that has been recovered after the separation of the polymer in the washing step into contact with an alkaline compound. Also disclosed is poly(arylene sulfide).
摘要翻译：公开了一种生产聚（亚芳基硫醚）的方法，其包括：在有机酰胺溶剂中聚合二卤代芳族化合物和至少一种选自碱金属硫化物和碱金属硫化氢的硫源的聚合步骤，优选在相分离剂的存在下; 在聚合步骤之后从含有生成的聚合物的反应液中分离聚合物的分离步骤; 用由水和/或有机溶剂组成的洗涤液洗涤聚合物的洗涤步骤; 以及分离液体处理步骤，在分离步骤中分离聚合物之后已经回收的分离液体和在洗涤步骤中分离聚合物之后已经回收的含有洗涤废液的分离液体进入与碱性化合物接触。还公开了聚（亚芳基硫醚）。

2. 发明授权

US06921609B2 Gradient cathode material for lithium rechargeable batteries 有权
标题翻译：用于锂可充电电池的梯度阴极材料
公开(公告)号：US06921609B2
公开(公告)日：2005-07-26
申请号：US10073674
申请日：2002-02-11
申请人： Christina Lampe-Onnerud , Per Onnerud , Jie Shi , Sharon Dalton , Tomoyoshi Koizumi , Aisaku Nagai
发明人： Christina Lampe-Onnerud , Per Onnerud , Jie Shi , Sharon Dalton , Tomoyoshi Koizumi , Aisaku Nagai
IPC分类号： C01G53/00 , C01G53/04 , H01M4/02 , H01M4/36 , H01M4/48 , H01M4/485 , H01M4/50 , H01M4/505 , H01M4/52 , H01M4/525 , H01M10/052 , H01M10/24 , H01M10/36 , H01M10/44
CPC分类号： H01M4/525 , H01M4/0471 , H01M4/131 , H01M4/1391 , H01M4/366 , H01M10/052
摘要： A composition suitable for use as a cathode material of a lithium battery includes a core material having an empirical formula LixM′zNi1−yM″yO2. “x” is equal to or greater than about 0.1 and equal to or less than about 1.3. “y” is greater than about 0.0 and equal to or less than about 0.5. “z” is greater than about 0.0 and equal to or less than about 0.2. M′ is at least one member of the group consisting of sodium, potassium, nickel, calcium, magnesium and strontium. M″ is at least one member of the group consisting of cobalt, iron, manganese, chromium, vanadium, titanium, magnesium, silicon, boron, aluminum and gallium. A coating on the core has a greater ratio of cobalt to nickel than the core. The coating and, optionally, the core can be a material having an empirical formula Lix1Ax2Ni1−y1−z1Coy1Bz1Oa. “x1” is greater than about 0.1 a equal to or less than about 1.3. “x2,” “y1” and “z1” each is greater than about 0.0 and equal to or less than about 0.2. “a” is greater than 1.5 and less than about 2.1. “A” is at least one element selected from the group consisting of barium, magnesium, calcium and strontium. “B” is at least one element selected from the group consisting of boron, aluminum, gallium, manganese, titanium, vanadium and zirconium.
摘要翻译：适合用作锂电池的阴极材料的组合物包括具有经验式Li x 1 M'z Ni 1-y的核心材料 > M“O 2 。 “x”等于或大于约0.1且等于或小于约1.3。 “y”大于约0.0且等于或小于约0.5。 “z”大于约0.0且等于或小于约0.2。 M'是由钠，钾，镍，钙，镁和锶组成的组中的至少一个成员。 M“是由钴，铁，锰，铬，钒，钛，镁，硅，硼，铝和镓组成的组中的至少一个。芯上的涂层具有比芯更大的钴与镍的比例。涂层和任选的芯可以是具有经验式的材料，例如，N 1，X 2，Ni 1-y 1-z 1， > y1 z1 。 “x1”大于等于或小于约1.3的约0.1a. “x2”，“y1”和“z1”各自大于约0.0且等于或小于约0.2。 “a”大于1.5且小于约2.1。 “A”是选自钡，镁，钙和锶中的至少一种元素。 “B”是选自硼，铝，镓，锰，钛，钒和锆中的至少一种元素。

3. 发明授权

US5326593A Surface roughening of resin molded articles for metallizing 失效
标题翻译：用于金属化的树脂模塑制品的表面粗糙化
公开(公告)号：US5326593A
公开(公告)日：1994-07-05
申请号：US897057
申请日：1992-06-11
申请人： Tomoyoshi Koizumi , Yukio Ichikawa
发明人： Tomoyoshi Koizumi , Yukio Ichikawa
IPC分类号： B32B7/04 , B32B15/08 , B32B38/00 , C08J7/02 , C08J7/14 , C23C18/22 , H05K1/03 , H05K3/18 , H05K3/38 , B05D3/10
CPC分类号： C08J7/14 , C23C18/22 , C08J2381/02 , H05K1/0333 , H05K3/181 , H05K3/381
摘要： A method for roughening the surface of a resin molded article to make it susceptible to metallizing is disclosed, including contacting a resin molded article at least the surface portion of which to be roughened mainly includes a block copolymer including 100 parts by weight of a polyarylene sulfide component block and from 100 to 200 parts by weight of a polyarylene sulfide ketone component block with a solvent capable of dissolving a polyarylene sulfide ketone more than a polyarylene sulfide.
摘要翻译：公开了一种使树脂模制品的表面粗糙化以使其易于金属化的方法，包括至少使树脂模塑制品的表面部分与粗糙化物接触，主要包括嵌段共聚物，该嵌段共聚物包括100重量份的聚芳硫醚 100重量份〜200重量份的聚芳硫醚酮组分嵌段，其中可溶于聚亚芳基硫醚酮的溶剂多于聚亚芳基硫醚。

4. 发明授权

US09339778B2 Column-type solid-liquid countercurrent contact apparatus, solid particle washing apparatus, and method 有权
标题翻译：柱式固液逆流接触装置，固体颗粒洗涤装置及方法
公开(公告)号：US09339778B2
公开(公告)日：2016-05-17
申请号：US13581946
申请日：2011-02-23
申请人： Tomoyoshi Koizumi , Kimihiko Kikuchi
发明人： Tomoyoshi Koizumi , Kimihiko Kikuchi
IPC分类号： B01F7/16 , B01F7/00 , B01F7/18 , B01J8/00 , B01J8/10 , B01J8/12 , C07C319/14 , C08G75/02 , C08L71/00 , C08L81/06
CPC分类号： B01F7/169 , B01F7/00633 , B01F7/18 , B01F2215/0431 , B01J8/008 , B01J8/10 , B01J8/12 , B01J2208/0084 , B01J2208/00867 , C07C319/14 , C08G75/02 , C08G2650/40 , C08L71/00 , C08L81/06 , C08L2205/02 , C07C321/30
摘要： A column-type solid-liquid countercurrent contact apparatus, a washing apparatus for solid particles such as poly(arylene sulfide) (PAS) particles, a PAS manufacturing apparatus, a method of solid-liquid countercurrent contact, a method of washing solid particles such as PAS particles, and a method of manufacturing PAS, wherein a column top part, a column body part, and a column bottom part are included, the column body part is provided with a plurality of stirring chambers connected in the vertical direction and mutually divided by a ring-shaped partitioning plate, a paddle blade (a blade diameter/a diameter of the stirring chamber≧0.65 and the blade diameter/the diameter of the stirring chamber≦0.10) and a baffle are disposed at each of the plurality of stirring chambers, and a disc having a size covering at least a part of a communication opening positioned below the paddle blade is attached to a rotating shaft or to the paddle blade.
摘要翻译：柱型固液逆流接触装置，固体颗粒如聚（亚芳基硫醚）（PAS）颗粒的洗涤装置，PAS制造装置，固液逆流接触的方法，固体颗粒的洗涤方法作为PAS颗粒，以及制造PAS的方法，其中包括塔顶部分，柱体部分和塔底部，柱体部分设置有沿竖直方向连接并相互分开的多个搅拌室通过环形分隔板，在多个搅拌中的每一个处设置有桨叶（叶片直径/搅拌室直径= 0.65，叶片直径/搅拌室直径，0.10）和挡板室和具有覆盖位于桨叶下方的连通开口的至少一部分的尺寸的盘被附接到旋转轴或桨叶。

5. 发明申请

US20120322972A1 Column-Type Solid-Liquid Countercurrent Contact Apparatus, Solid Particle Washing Apparatus, and Method 有权
标题翻译：柱式固液逆流接触装置，固体颗粒洗涤装置及方法
公开(公告)号：US20120322972A1
公开(公告)日：2012-12-20
申请号：US13581946
申请日：2011-02-23
申请人： Tomoyoshi Koizumi , Kimihiko Kikuchi
发明人： Tomoyoshi Koizumi , Kimihiko Kikuchi
IPC分类号： B01F7/18 , C08G75/14 , B08B3/00 , B01J19/18
CPC分类号： B01F7/169 , B01F7/00633 , B01F7/18 , B01F2215/0431 , B01J8/008 , B01J8/10 , B01J8/12 , B01J2208/0084 , B01J2208/00867 , C07C319/14 , C08G75/02 , C08G2650/40 , C08L71/00 , C08L81/06 , C08L2205/02 , C07C321/30
摘要： A column-type solid-liquid countercurrent contact apparatus, a washing apparatus for solid particles such as poly(arylene sulfide) (PAS) particles, a PAS manufacturing apparatus, a method of solid-liquid countercurrent contact, a method of washing solid particles such as PAS particles, and a method of manufacturing PAS, wherein a column top part, a column body part, and a column bottom part are included, the column body part is provided with a plurality of stirring chambers connected in the vertical direction and mutually divided by a ring-shaped partitioning plate, a paddle blade (a blade diameter/a diameter of the stirring chamber≧0.65 and the blade diameter/the diameter of the stirring chamber≦0.10) and a baffle are disposed at each of the plurality of stirring chambers, and a disc having a size covering at least a part of a communication opening positioned below the paddle blade is attached to a rotating shaft or to the paddle blade.
摘要翻译：柱型固液逆流接触装置，固体颗粒如聚（亚芳基硫醚）（PAS）颗粒的洗涤装置，PAS制造装置，固液逆流接触的方法，固体颗粒的洗涤方法作为PAS颗粒，以及制造PAS的方法，其中包括塔顶部分，柱体部分和塔底部，柱体部分设置有沿竖直方向连接并相互分开的多个搅拌室通过环形分隔板，在多个搅拌中的每一个处设置有桨叶（叶片直径/搅拌室直径= 0.65，叶片直径/搅拌室直径，0.10）和挡板室和具有覆盖位于桨叶下方的连通开口的至少一部分的尺寸的盘被附接到旋转轴或桨叶。

6. 发明授权

US09068047B2 Process for producing poly(arylene sulfide), and poly(arylene sulfide) comprising contacting a wash liquid with an alkaline compound 有权
标题翻译：包括使洗涤液与碱性化合物接触的制备聚（亚芳基硫醚）和聚（亚芳基硫醚）的方法
公开(公告)号：US09068047B2
公开(公告)日：2015-06-30
申请号：US13698600
申请日：2011-04-21
申请人： Yoshihiro Ichinose , Masanori Kobayashi , Tomoyoshi Koizumi , Mitsuhiro Matsuzaki
发明人： Yoshihiro Ichinose , Masanori Kobayashi , Tomoyoshi Koizumi , Mitsuhiro Matsuzaki
IPC分类号： C08G75/02 , C08G75/14
CPC分类号： C08G75/0254 , C08G75/0213 , C08G75/0259 , C08G75/0281 , Y10T428/2982
摘要： Disclosed is a process for producing poly(arylene sulfide) which includes: a polymerization step of polymerizing a dihalogenated aromatic compound and at least one sulfur source selected from the group consisting of alkali metal sulfides and alkali metal hydrogen sulfides in an organic amide solvent, preferably in the presence of a phase separating agent; a separation step of separating a polymer from a reaction liquid containing a produced polymer after the polymerization step; a washing step of washing the polymer with a washing liquid that consists of water and/or an organic solvent; and a separated liquid treatment step of bringing both a separated liquid that has been recovered after the separation of the polymer in the separation step and a separated liquid containing a wash waste liquid that has been recovered after the separation of the polymer in the washing step into contact with an alkaline compound. Also disclosed is poly(arylene sulfide).
摘要翻译：公开了一种生产聚（亚芳基硫醚）的方法，其包括：在有机酰胺溶剂中聚合二卤代芳族化合物和至少一种选自碱金属硫化物和碱金属硫化氢的硫源的聚合步骤，优选在相分离剂的存在下; 在聚合步骤之后从含有生成的聚合物的反应液中分离聚合物的分离步骤; 用由水和/或有机溶剂组成的洗涤液洗涤聚合物的洗涤步骤; 以及分离液体处理步骤，在分离步骤中分离聚合物之后已经回收的分离液体和在洗涤步骤中分离聚合物之后已经回收的含有洗涤废液的分离液体进入与碱性化合物接触。还公开了聚（亚芳基硫醚）。

7. 发明申请

US20130116401A1 Production Process of Poly(Arylene Sulfide) and Production Apparatus Thereof 有权
标题翻译：聚（亚硫酰基）生产工艺及其生产设备
公开(公告)号：US20130116401A1
公开(公告)日：2013-05-09
申请号：US13809505
申请日：2011-07-06
申请人： Takayuki Kimura , Tomoyoshi Koizumi , Mitsuhiro Matsuzaki
发明人： Takayuki Kimura , Tomoyoshi Koizumi , Mitsuhiro Matsuzaki
IPC分类号： C08G75/14
CPC分类号： C08G75/14 , C08G75/0213 , C08G75/0254 , C08G75/0259 , C08G75/0281
摘要： A production process of a poly(arylene sulfide) (PAS), including a polymerization step of forming a PAS from a sulfur source that is an alkali metal (hydro)sulfides and a dihalo-aromatic compound in an organic amide solvent; a separation step of PAS particles; a countercurrent washing step that is a step of washing the PAS particles with water and/or an organic solvent, wherein a downward current of a PAS particle-containing aqueous slurry is continuously brought into countercurrent contact with an upward current of a washing liquid; a PAS particle re-separation step of capturing a washing waste liquid by a PAS particle re-separating unit, in which a micro-slit filter has been installed, and then re-separating the PAS particles from the micro-slit filter, preferably using a backwashing unit, to discharge them; and a collecting step of the PAS particles discharged, and a production apparatus of a poly(arylene sulfide).
摘要翻译：一种聚（亚芳基硫醚）（PAS）的生产方法，包括在有机酰胺溶剂中由作为碱金属（氢）硫化物的硫源和二卤代芳族化合物形成PAS的聚合步骤; PAS颗粒的分离步骤; 逆流洗涤步骤，其是用水和/或有机溶剂洗涤PAS颗粒的步骤，其中含有PAS颗粒的含水浆料的向下电流连续地与洗涤液的向上流动接触; PAS粒子重新分离步骤，其中已经安装了微缝隙过滤器的PAS粒子重新分离单元捕获洗涤废液，然后从微缝隙过滤器重新分离PAS颗粒，优选使用反冲洗单元，以排放它们; 以及排出的PAS颗粒的收集步骤和聚（亚芳基硫醚）的生产装置。

8. 发明申请

US20110178268A1 Production Process of Granular Poly(Arylene Sulfide) 有权
标题翻译：颗粒聚（亚硫酰）的生产工艺
公开(公告)号：US20110178268A1
公开(公告)日：2011-07-21
申请号：US13056433
申请日：2009-06-10
申请人： Kenji Suzuki , Tomoyoshi Koizumi , Yoshinori Shiojiri
发明人： Kenji Suzuki , Tomoyoshi Koizumi , Yoshinori Shiojiri
IPC分类号： C08G75/16
CPC分类号： C08G75/0245 , C08G75/0213 , C08G75/025 , C08G75/0254 , C08G75/0281
摘要： The invention provides a production process of a granular poly(arylene sulfide) by polymerizing a sulfur source and a dihalo-aromatic compound in an organic amide solvent by a polymerization process containing a phase-separation polymerization step, wherein the production process contains a step I of adding an aromatic compound in a proportion of 0.01 to 20 mol per 100 mol of the organic amide solvent into the liquid phase containing the organic amide solvent and a formed polymer within the polymerization reaction system, said liquid phase being in the phase-separated state, after the phase-separation polymerization step; a step II of cooling the liquid phase within the polymerization reaction system; and a step III of collecting the formed polymer from the liquid phase.
摘要翻译：本发明通过含有相分离聚合步骤的聚合方法在有机酰胺溶剂中聚合硫源和二卤代芳族化合物来提供粒状聚（亚芳基硫醚）的制备方法，其中制备方法包含步骤I 将相对于每100摩尔有机酰胺溶剂为0.01-20摩尔的芳族化合物加入含有有机酰胺溶剂的液相和聚合反应体系内形成的聚合物，所述液相处于相分离状态在分相聚合步骤之后; 在聚合反应体系内冷却液相的步骤II; 以及从液相中收集形成的聚合物的步骤III。

9. 发明授权

US06855461B2 Cathode material for lithium rechargeable batteries 有权
标题翻译：锂可充电电池的阴极材料
公开(公告)号：US06855461B2
公开(公告)日：2005-02-15
申请号：US10073678
申请日：2002-02-11
申请人： Christina Lampe-Onnerud , Per Onnerud , Dmitri Novikov , Jie Shi , Richard Chamberlain , Tomoyoshi Koizumi , Aisaku Nagai
发明人： Christina Lampe-Onnerud , Per Onnerud , Dmitri Novikov , Jie Shi , Richard Chamberlain , Tomoyoshi Koizumi , Aisaku Nagai
IPC分类号： C01G53/00 , C01B35/10 , C01G23/04 , C01G31/02 , C01G45/12 , C01G49/02 , C01G51/04 , C01G53/04 , H01M2/02 , H01M4/131 , H01M4/525 , H01M10/052 , H01M4/58
CPC分类号： C01G53/50 , C01G53/66 , C01P2002/77 , C01P2006/40 , H01M4/131 , H01M4/525 , H01M4/622 , H01M4/625 , H01M10/052
摘要： A crystal which can be employed as the active material of a lithium-based battery has an empirical formula of Lix1A2Ni1-y-zCoyBzOa, wherein “x1” is greater than about 0.1 and equal to or less than about 1.3, “x2,” “y” and “z” each is greater than about 0.0 and equal to or less than about 0.2, “a” is greater than about 1.5 and less than about 2.1, “A” is at least one element selected from the group consisting of barium, magnesium, calcium and strontium and “B” is at least one element selected from the group consisting of boron, aluminum, gallium, manganese, titanium, vanadium and zirconium. A method includes combining lithium, nickel, cobalt and at least one element “A” selected from the group consisting of barium, magnesium, calcium and strontium, has at least one element “B” selected from the group consisting of boron, aluminum, gallium, manganese, titanium, vanadium and zirconium, in the presence of oxygen, wherein the combined components have the relative ratio of Lix1:Ax2:Ni1-y-z:Coy:Bz, wherein “x1,” “x2,” “y” and “z” have the values given for the empirical formula shown above.
摘要翻译：可以用作锂基电池的活性材料的晶体具有Lix1A2Ni1-y-zCoyBzOa的经验式，其中“x1”大于约0.1且等于或小于约1.3，“x2”，“ y“和”z“各自大于约0.0且等于或小于约0.2，”a“大于约1.5且小于约2.1，”A“是选自由以下组成的组中的至少一种元素：钡，镁，钙和锶，“B”是选自硼，铝，镓，锰，钛，钒和锆中的至少一种元素。一种方法包括组合锂，镍，钴和至少一种选自钡，镁，钙和锶的元素“A”，具有至少一种选自硼，铝，镓的元素“B” ，锰，钛，钒和锆，其中组合成分具有Lix1：Ax2:Ni1-yz:Coy:Bz的相对比例，其中“x1”，“x2”，“y”和“ z“具有上述经验公式给出的值。

10. 发明授权

US08981041B2 Production process of poly(arylene sulfide) and production apparatus thereof 有权
标题翻译：聚（亚芳基硫醚）的生产工艺及其生产设备
公开(公告)号：US08981041B2
公开(公告)日：2015-03-17
申请号：US13809505
申请日：2011-07-06
申请人： Takayuki Kimura , Tomoyoshi Koizumi , Mitsuhiro Matsuzaki
发明人： Takayuki Kimura , Tomoyoshi Koizumi , Mitsuhiro Matsuzaki
IPC分类号： C08G75/14 , C08G75/02
CPC分类号： C08G75/14 , C08G75/0213 , C08G75/0254 , C08G75/0259 , C08G75/0281
摘要： A production process of a poly(arylene sulfide) (PAS), including a polymerization step of forming a PAS from a sulfur source that is an alkali metal (hydro)sulfides and a dihalo-aromatic compound in an organic amide solvent; a separation step of PAS particles; a countercurrent washing step that is a step of washing the PAS particles with water and/or an organic solvent, wherein a downward current of a PAS particle-containing aqueous slurry is continuously brought into countercurrent contact with an upward current of a washing liquid; a PAS particle re-separation step of capturing a washing waste liquid by a PAS particle re-separating unit, in which a micro-slit filter has been installed, and then re-separating the PAS particles from the micro-slit filter, preferably using a backwashing unit, to discharge them; and a collecting step of the PAS particles discharged, and a production apparatus of a poly(arylene sulfide).
摘要翻译：一种聚（亚芳基硫醚）（PAS）的生产方法，包括在有机酰胺溶剂中由作为碱金属（氢）硫化物的硫源和二卤代芳族化合物形成PAS的聚合步骤; PAS颗粒的分离步骤; 逆流洗涤步骤，其是用水和/或有机溶剂洗涤PAS颗粒的步骤，其中含有PAS颗粒的含水浆料的向下电流连续地与洗涤液的向上流动接触; PAS粒子重新分离步骤，其中已经安装了微缝隙过滤器的PAS粒子重新分离单元捕获洗涤废液，然后从微缝隙过滤器重新分离PAS颗粒，优选使用反冲洗单元，以排放它们; 以及排出的PAS颗粒的收集步骤和聚（亚芳基硫醚）的生产装置。

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