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1. 发明授权

US06225510B1 Preparation of di-t-alkyl peroxides and t-alkyl hydroperoxides from n-alkyl ethers 失效
标题翻译：从正烷基醚制备二烷基过氧化物和叔烷基氢过氧化物
公开(公告)号：US06225510B1
公开(公告)日：2001-05-01
申请号：US09459254
申请日：1999-12-10
申请人： Peter Frenkel , Ted M. Pettijohn , Lawrence R. Brecker
发明人： Peter Frenkel , Ted M. Pettijohn , Lawrence R. Brecker
IPC分类号： C07C40900
CPC分类号： C07C409/16 , C07C407/00 , C07C409/04
摘要： A process for production of a t-alkyl peroxide compound includes the steps of: a) reacting an n-alkyl t-alkyl ether with a reactant mixture comprising an acid catalyst and a compound of the formula RO2H (I) where R is H or t-alkyl, provided that if R is t-alkyl the t-alkyl peroxide compound product is a di-t-alkyl peroxide, and b) isolating a reaction product comprising said t-alkyl peroxide compound from the mixture resulting from step a). The process can be used to prepare t-butyl hydroperoxide or di-t-butyl peroxide from methyl t-butyl ether. Sulfuric acid may be used as the acid catalyst.
摘要翻译：一种生产叔烷基过氧化物的方法包括以下步骤：a）使正烷基叔烷基醚与包含酸催化剂和下式化合物的反应混合物反应，其中R是H或叔烷基，条件是如果R是叔烷基，则叔烷基过氧化物产物是二叔烷基过氧化物，和b）从由步骤a）得到的混合物中分离出包含所述叔烷基过氧化物化合物的反应产物。用于从甲基叔丁基醚制备叔丁基过氧化氢或二叔丁基过氧化物。硫酸可用作酸催化剂。

2. 发明授权

US06180832B2 Preparation of peroxyketals 失效
标题翻译：过氧缩酮的制备
公开(公告)号：US06180832B2
公开(公告)日：2001-01-30
申请号：US09321288
申请日：1999-05-27
申请人： Peter Frenkel , Ted M. Pettijohn
发明人： Peter Frenkel , Ted M. Pettijohn
IPC分类号： C07C40916
CPC分类号： C07C409/22 , C07C407/00
摘要： The process of preparing peroxyketals which comprises reacting a composition comprising ketone with hydroperoxide in the presence of heteropolyacid.
摘要翻译：制备过氧缩酮的方法，其包括在杂多酸存在下使包含酮与氢过氧化物的组合物反应。

3. 发明授权

US6001767A Heteropoly acid peroxide promoter 失效
标题翻译：杂多酸过氧化物启动子
公开(公告)号：US6001767A
公开(公告)日：1999-12-14
申请号：US905593
申请日：1997-08-04
申请人： Peter Frenkel , Ted M. Pettijohn
发明人： Peter Frenkel , Ted M. Pettijohn
IPC分类号： C08F4/28 , C08F4/32 , C08F4/38 , B01J31/00 , C08L33/06
CPC分类号： C08F4/32
摘要： The invention disclosed involves the use of heteropoly acids as promoters to decompose organic peroxides.
摘要翻译：所公开的发明涉及使用杂多酸作为促进剂来分解有机过氧化物。

4. 发明授权

US5260244A Transition metal/rare earth catalyst, olefin polymeration process, and polymer produced 失效
标题翻译：过渡金属/稀土催化剂，烯烃聚合方法和生产的聚合物
公开(公告)号：US5260244A
公开(公告)日：1993-11-09
申请号：US955606
申请日：1992-10-01
申请人： Ted M. Pettijohn
发明人： Ted M. Pettijohn
IPC分类号： C08F4/646 , C08F10/00
CPC分类号： C08F10/00 , Y10S526/943
摘要： A polymerization catalyst system is formed by combining an organometal compound and a transition metal compound to produce a catalyst A; and combining catalyst A and a catalyst B comprising a rare earth complex having a formula Cp.sub.n MX.sub.4-n.M'L.sub.x, wherein Cp is cyclopentadienyl or cyclopentadienyl substituted with an alkyl or alkyl silyl radical, M is yttrium, scandium or a rare earth metal having an atomic number in the range of 57 to 71, M' is an alkali metal, L is a suitable electron donor ligand, X is a halogen, n is 1 or 2, and x is a number corresponding to the value needed to form a stable complex.Optionally catalyst A is contacted with a rare earth metal halide.Optionally catalyst B is contacted with an alkali or alkaline earth metal alkyl.Optionally a hydrocarbyl aluminum compound can be contacted with catalyst B or with the catalyst system.
摘要翻译：通过组合有机金属化合物和过渡金属化合物以形成催化剂A形成聚合催化剂体系; 并且将催化剂A和包含具有式CpnMX4-n.M'Lx的稀土络合物的催化剂B组合，其中Cp是环烷基或被烷基或烷基甲硅烷基取代的环戊二烯基，M是钇，钪或稀土金属，其具有 57至71的范围内的原子序数，M'是碱金属，L是合适的电子给体配体，X是卤素，n是1或2，x是与形成稳定复杂。任选地，催化剂A与稀土金属卤化物接触。任选地，催化剂B与碱金属或碱土金属烷基接触。任选地，烃基铝化合物可以与催化剂B或催化剂体系接触。

5. 发明授权

US5232999A Olefin polymerization catalyst and process 失效
标题翻译：烯烃聚合催化剂和工艺
公开(公告)号：US5232999A
公开(公告)日：1993-08-03
申请号：US826549
申请日：1992-01-27
申请人： Brian K. Conroy , Kenneth R. Farmer , Ted M. Pettijohn
发明人： Brian K. Conroy , Kenneth R. Farmer , Ted M. Pettijohn
IPC分类号： C08F4/54 , C08F10/00
CPC分类号： C08F4/54 , C08F10/00
摘要： The compound (Cp*.sub.2 YCl).sub.2 wherein Cp* is pentamethylcyclopentadienyl and its preparation and use for the polymerization of olefins is disclosed.
摘要翻译：公开了其中Cp *是五甲基环戊二烯基的化合物（Cp * 2YCl）2及其制备和用于烯烃聚合的用途。

6. 发明授权

US06379711B1 Phosphomolybdic acid stabilizer for hydrogen peroxide 失效
标题翻译：用于过氧化氢的磷钼酸稳定剂
公开(公告)号：US06379711B1
公开(公告)日：2002-04-30
申请号：US09493163
申请日：2000-01-27
申请人： Peter Frenkel , Ted M. Pettijohn
发明人： Peter Frenkel , Ted M. Pettijohn
IPC分类号： A01N5900
CPC分类号： C01B15/037 , Y10S514/97
摘要： Phosphomolybdic acid and partial alkali salts of phosphomolybdic acid are used as stabilizers for aqueous hydrogen peroxide.
摘要翻译：磷钼酸和磷钼酸的部分碱金属盐用作过氧化氢水溶液的稳定剂。

7. 发明授权

US5814575A Chromium compounds and uses thereof 失效
公开(公告)号：US5814575A
公开(公告)日：1998-09-29
申请号：US485344
申请日：1995-06-07
申请人： William K. Reagen , Ted M. Pettijohn , Jeffrey W. Freeman
发明人： William K. Reagen , Ted M. Pettijohn , Jeffrey W. Freeman
IPC分类号： B01J23/26 , B01J31/14 , B01J31/16 , B01J31/18 , B01J31/22 , B01J37/02 , C07C2/32 , C07F11/00 , C08F4/69 , C08F4/78 , C08F10/00
CPC分类号： B01J31/2208 , B01J23/26 , B01J31/1616 , B01J31/181 , B01J31/2213 , B01J37/0203 , C07C2/32 , C07F11/005 , C08F10/00 , B01J2231/20 , B01J2531/0205 , B01J2531/62 , B01J31/143 , B01J31/2234 , C07C2531/12 , C07C2531/22 , Y02P20/588
摘要： Novel chromium-containing compounds, such as, for example, chromium pyrrolides, are prepared by forming a mixture of a chromium salt, a metal amide, and an electron pair donor solvent, such as, for example, an ether. These novel chromium-containing, or chromium pyrrolide, compounds can be used either unsupported or supported on an inorganic oxide support, with a metal alkyl and an unsaturated hydrocarbon, to trimerize, oligomerize, and/or polymerize olefins.

8. 发明授权

US5763723A Chromium compounds and uses thereof 失效
标题翻译：铬化合物及其用途
公开(公告)号：US5763723A
公开(公告)日：1998-06-09
申请号：US485544
申请日：1995-06-07
申请人： William K. Reagen , Ted M. Pettijohn , Jeffrey W. Freeman
发明人： William K. Reagen , Ted M. Pettijohn , Jeffrey W. Freeman
IPC分类号： B01J23/26 , B01J31/14 , B01J31/16 , B01J31/18 , B01J31/22 , B01J37/02 , C07C2/32 , C07F11/00 , C08F4/69 , C08F4/78 , C08F10/00
CPC分类号： B01J31/2208 , B01J23/26 , B01J31/1616 , B01J31/181 , B01J31/2213 , B01J37/0203 , C07C2/32 , C07F11/005 , C08F10/00 , B01J2231/20 , B01J2531/0205 , B01J2531/62 , B01J31/143 , B01J31/2234 , C07C2531/12 , C07C2531/22 , Y02P20/588
摘要： Novel chromium-containing compounds, such as, for example, chromium pyrrolides, are prepared by forming a mixture of a chromium salt, a metal amide, and an electron pair donor solvent, such as, for example, an ether. These novel chromium-containing, or chromium pyrrolide, compounds can be used either unsupported or supported on an inorganic oxide support, with a metal alkyl and an unsaturated hydrocarbon, to trimerize, oligomerize, and/or polymerize olefins.
摘要翻译：通过形成铬盐，金属酰胺和电子对供体溶剂（例如醚）的混合物来制备新的含铬化合物，例如吡咯化铬。这些新颖的含铬或铬吡咯化合物可以无支撑或负载在无机氧化物载体上，与金属烷基和不饱和烃一起使用以使烯烃三聚，低聚和/或聚合。

9. 发明授权

US5705725A Aromatic alkali metal alkene addition process 失效
标题翻译：芳香碱金属烯烃加成工艺
公开(公告)号：US5705725A
公开(公告)日：1998-01-06
申请号：US770004
申请日：1991-10-02
申请人： Ted M. Pettijohn , Mark E. Lashier , Henry L. Hsieh
发明人： Ted M. Pettijohn , Mark E. Lashier , Henry L. Hsieh
IPC分类号： C07C2/30 , C07C2/72 , C07C2/66 , C07C2/34 , C07C2/68
CPC分类号： C07C2/30 , C07C2/72 , C07C2531/12
摘要： A process is provided comprising: (a) contacting a hydrocarbyl lithium with an alkali metal hydrocarbyloxide in the presence of an aromatic compound; and thereafter (b) recovering an aromatic alkali metal compound; and thereafter (c) contacting said aromatic alkali metal compound with an alpha-olefin. Optionally, a catalytic support is also present during steps a, b, and c.
摘要翻译：提供了一种方法，其包括：（a）在芳族化合物的存在下使烃基锂与碱金属烃氧化物接触; （b）回收芳族碱金属化合物; 然后（c）使所述芳族碱金属化合物与α-烯烃接触。任选地，在步骤a，b和c期间也存在催化载体。

10. 发明授权

US5523507A Process of trimerizing and oligomerizing olefins using chromium compounds 失效
标题翻译：使用铬化合物使烯烃三聚和低聚的方法
公开(公告)号：US5523507A
公开(公告)日：1996-06-04
申请号：US290048
申请日：1994-07-29
申请人： William K. Reagen , Ted M. Pettijohn , Jeffrey W. Freeman
发明人： William K. Reagen , Ted M. Pettijohn , Jeffrey W. Freeman
IPC分类号： B01J23/26 , B01J31/14 , B01J31/16 , B01J31/18 , B01J31/22 , B01J37/02 , C07C2/32 , C07F11/00 , C08F4/69 , C08F4/78 , C08F10/00 , C07C2/30
CPC分类号： B01J31/2208 , B01J23/26 , B01J31/1616 , B01J31/181 , B01J31/2213 , B01J37/0203 , C07C2/32 , C07F11/005 , C08F10/00 , B01J2231/20 , B01J2531/0205 , B01J2531/62 , B01J31/143 , B01J31/2234 , C07C2531/12 , C07C2531/22 , Y02P20/588
摘要： Novel chromium-containing compounds, such as, for example, chromium pyrrolides, are prepared by forming a mixture of a chromium salt, a metal amide, and an electron pair donor solvent, such as, for example, an ether. These novel chromium-containing, or chromium pyrrolide, compounds can be used either unsupported or supported on an inorganic oxide support, with a metal alkyl and an unsaturated hydrocarbon, to trimerize, oligomerize, and/or polymerize olefins.
摘要翻译：通过形成铬盐，金属酰胺和电子对供体溶剂（例如醚）的混合物来制备新的含铬化合物，例如吡咯化铬。这些新颖的含铬或铬吡咯化合物可以无支撑或负载在无机氧化物载体上，与金属烷基和不饱和烃一起使用以使烯烃三聚，低聚和/或聚合。

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