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1. 发明授权

US4243812A Processes for the preparation of glyoxal-2-oxims 失效
标题翻译：乙二醛-2-氧化物的制备方法
公开(公告)号：US4243812A
公开(公告)日：1981-01-06
申请号：US67889
申请日：1979-08-20
申请人： Takaji Honna , Motoaki Tanaka , Syozo Yamada , Hidekazu Miyake
发明人： Takaji Honna , Motoaki Tanaka , Syozo Yamada , Hidekazu Miyake
IPC分类号： A61K31/42 , A61P25/04 , A61P29/00 , C07D261/08 , C07D261/12
CPC分类号： C07D261/08
摘要： Novel derivatives of glyoxal-2-oxim represented by the chemical formula ##STR1## wherein R is hydrogen or a lower alkyl or phenyl group, are provided in accordance with the present invention. These derivatives are prepared by reacting the corresponding isoxazole-5-carbaldehyde with nitromethane in the presence of a metal alkoxide, or the corresponding 5-acetylisoxazole with a nitrate. They have anti-inflammatory and/or analgesic activities.
摘要翻译：根据本发明提供了由化学式 [I]表示的乙二醛-2-肟基的新型衍生物，其中R是氢或低级烷基或苯基。这些衍生物通过在金属醇盐或相应的5-乙酰异恶唑与硝酸盐存在下使相应的异恶唑-5-甲醛与硝基甲烷反应来制备。它们具有抗炎和/或止痛活性。

2. 发明授权

US5114083A Method and appatatus for pulverizing material 失效
标题翻译：用于粉碎材料的方法和装置
公开(公告)号：US5114083A
公开(公告)日：1992-05-19
申请号：US465178
申请日：1990-02-12
申请人： Iwao Ikebuchi , Yoshitaka Ihara , Hisashi Takei , Syozo Yamada , Mamoru Nakano , Akira Ganse
发明人： Iwao Ikebuchi , Yoshitaka Ihara , Hisashi Takei , Syozo Yamada , Mamoru Nakano , Akira Ganse
IPC分类号： B02C17/16
CPC分类号： B02C17/16
摘要： The present invention relates to a method and apparatus for pulverizing a material to produce a fine powdery material such as silica powder as a material for a filler for sealing semiconductors. It has a shell and a screw shaft mounted in the shell. A disk having an inverted conical bottom surface is coaxially secured to the bottom of the screw shaft. The disk serves to protect the blade of the screw shaft from wear. Also owing to the inverted conical bottom surface, a centripetal force acts on the screw shaft while in rotation, thus preventing it from running out of true. By providing a plurality of screw shafts in the shell, the fluid in the shell flows in a complicated manner, thus increasing the pulverizing efficiency. A partitioning plate formed with a hole in the upper or lower part thereof may be provided between the adjacent screw shafts to minimize the possibility of shortcircuiting of the material from the inlet of the shell to its outlet. The respective screw shafts may have different revolving speeds, different heights or different screw pitches from one another to create a complicated fluid flow in the shell and thus to improve the pulverizing efficiency.
摘要翻译： PCT No.PCT / JP89 / 00584 371日期1990年2月12日 102（e）1990年2月12日PCT PCT 1989年6月7日PCT。出版物WO89 / 11911 日本1989年12月14日。本发明涉及一种粉碎材料以生产细粉末材料如二氧化硅粉末作为密封半导体填料的材料的方法和装置。它具有外壳和安装在外壳中的螺钉轴。具有倒锥形底面的盘同轴地固定在螺杆轴的底部。该盘用于保护螺杆轴的刀片免受磨损。另外由于倒锥形底面，向心力在旋转时作用在螺杆轴上，从而防止其脱离真实状态。通过在壳体中设置多个螺杆轴，壳体中的流体以复杂的方式流动，从而提高了粉碎效率。在其相邻的螺杆轴之间可以设置在其上部或下部形成有孔的分隔板，以最小化材料从壳的入口到其出口的短路的可能性。相应的螺杆轴可以具有不同的转速，不同的高度或不同的螺距，从而在壳体中产生复杂的流体流动，从而提高粉碎效率。

3. 发明授权

US4224450A Process for the preparation of glyoxal-2-oximes 失效
标题翻译：乙二醛2-肟的制备方法
公开(公告)号：US4224450A
公开(公告)日：1980-09-23
申请号：US67888
申请日：1979-08-20
申请人： Takaji Honna , Motoaki Tanaka , Syozo Yamada , Hidekazu Miyake
发明人： Takaji Honna , Motoaki Tanaka , Syozo Yamada , Hidekazu Miyake
IPC分类号： A61K31/42 , A61P25/04 , A61P29/00 , C07D261/08 , C07D261/14
CPC分类号： C07D261/08
摘要： Novel derivatives of glyoxal-2-oxim represented by the chemical formula ##STR1## wherein R is hydrogen or a lower alkyl or phenyl group, are provided in accordance with the present invention. These derivatives are prepared by reacting the corresponding isoxazole-5-carbaldehyde with nitromethane in the presence of a metal alkoxide, or the corresponding 5-acetylisoxazole with a nitrite. They have anti-inflammatory and/or analgesic activities.
摘要翻译：根据本发明提供了由化学式 [I]表示的乙二醛-2-肟基的新型衍生物，其中R是氢或低级烷基或苯基。这些衍生物通过在金属醇盐或相应的5-乙酰异恶唑与亚硝酸盐存在下使相应的异恶唑-5-甲醛与硝基甲烷反应来制备。它们具有抗炎和/或止痛活性。

4. 发明授权

US4212874A Glyoxal-2-oxim derivatives and a process for relieving pain/or inflammation therewith 失效
标题翻译：乙二醛-2-肟衍生物及其缓解疼痛或炎症的方法
公开(公告)号：US4212874A
公开(公告)日：1980-07-15
申请号：US16821
申请日：1979-03-02
申请人： Takaji Honna , Motoaki Tanaka , Syozo Yamada , Hidekazu Miyake
发明人： Takaji Honna , Motoaki Tanaka , Syozo Yamada , Hidekazu Miyake
IPC分类号： A61K31/42 , A61P25/04 , A61P29/00 , C07D261/08
CPC分类号： C07D261/08
摘要： Novel derivatives of glyoxal-2-oxim represented by the chemical formula ##STR1## wherein R is hydrogen or a lower alkyl or phenyl group, are provided in accordance with the present invention. These derivatives are prepared by reacting the corresponding isoxazole-5-carbaldehyde with nitromethane in the presence of a metal alkoxide, or the corresponding 5-acetylisoxazole with a nitrite. They have anti-inflammatory and/or analgesic activities.
摘要翻译：根据本发明提供了由化学式 [I]表示的乙二醛-2-肟基的新型衍生物，其中R是氢或低级烷基或苯基。这些衍生物通过在金属醇盐或相应的5-乙酰异恶唑与亚硝酸盐存在下使相应的异恶唑-5-甲醛与硝基甲烷反应来制备。它们具有抗炎和/或止痛活性。

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