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1. 发明授权

US06524989B2 Tetraorganophosponium dicyclic tetraorganoborate catalyst 有权
标题翻译：四有机磷鎓二环四硼酸盐催化剂
公开(公告)号：US06524989B2
公开(公告)日：2003-02-25
申请号：US09833585
申请日：2001-04-13
申请人： Sumiya Miyake , Akiko Okubo , Hiromi Honda , Yoshiyuki Go , Hiroshi Nagata , Minoru Kobayashi
发明人： Sumiya Miyake , Akiko Okubo , Hiromi Honda , Yoshiyuki Go , Hiroshi Nagata , Minoru Kobayashi
IPC分类号： B01J3120
CPC分类号： H01L23/293 , B01J31/0268 , B01J31/06 , B01J31/146 , C08G59/245 , C08G59/68 , C08G59/688 , C08G73/121 , C08L63/00 , H01L2924/0002 , Y10T428/31511 , C08L61/04 , H01L2924/00
摘要： This invention provides a latent catalyst having a structure of phosphonium borate consisting of a monovalent cation portion in which four specific groups are bonded to the phosphorus atom and a monovalent anion portion in which four specific groups are bonded to the boron atom, and a latent catalyst having a structure wherein the above phosphonium borate is the recurring unit and at least two of said recurring unit are connected through at least one of the four specific groups bonded to the boron atom. This invention also provides a thermosetting resin composition comprising such a latent catalyst and an epoxy resin molding material comprising such a latent catalyst and further provides a semiconductor device in which a semiconductor is encapsulated with said epoxy resin molding material.
摘要翻译：本发明提供一种潜在催化剂，其具有由一个阳离子部分组成的硼酸鏻结构，其中四个特定基团与磷原子键合，其中四个特定基团与硼原子键合的一价阴离子部分，潜在催化剂具有其中上述硼酸鏻是重复单元的结构，并且所述重复单元中的至少两个通过键合到硼原子的四个特定基团中的至少一个连接。本发明还提供一种包含这种潜催化剂和包含这种潜催化剂的环氧树脂模制材料的热固性树脂组合物，并且还提供半导体器件，其中半导体被所述环氧树脂模制材料封装。

2. 发明授权

US06180695B2 Flame-retardant resin composition and semiconductor sealant using the same 失效
标题翻译：阻燃树脂组合物和使用其的半导体密封剂
公开(公告)号：US06180695B2
公开(公告)日：2001-01-30
申请号：US09069832
申请日：1998-04-30
申请人： Mikio Ito , Sumiya Miyake
发明人： Mikio Ito , Sumiya Miyake
IPC分类号： C08K332
CPC分类号： C09K21/14 , C08K5/53 , C08L61/06 , C08L63/00 , C09K21/12 , Y10T428/31518 , Y10T428/31522 , C08L2666/22
摘要： The present invention provides a flame-retardant resin composition comprising: (A) an epoxy resin other than halogenated epoxy resins, having at least two epoxy groups in the molecule, (B) a curing agent, and (C) a product obtained by reacting (C1) a phosphorus compound having at least one P-H linkage in the molecule, with (C2) a compound having, in the molecule, at least one functional group selected from the group consisting of C—C double bond, epoxy group, alcoholic hydroxyl group and carbonyl group, and at least one functional group selected from the group consisting of epoxy group, phenolic hydroxyl group, amino group, cyanate ester group and isocyanate group, and having a phosphorus content of 0.3% by weight to 8% by weight. This resin composition has high flame retardancy without using any halogen compound and does not impair the properties of an article to which the composition is applied.
摘要翻译：本发明提供一种阻燃性树脂组合物，其包含：（A）除了分子内具有至少两个环氧基的卤代环氧树脂以外的环氧树脂，（B）固化剂，和（C）通过使（C1）分子中具有至少一个PH键的磷化合物，（C2）在分子中具有至少一个选自CC双键，环氧基，醇羟基和羰基，以及选自环氧基，酚羟基，氨基，氰酸酯基和异氰酸酯基中的至少一种官能团，磷含量为0.3重量％〜8重量％。该树脂组合物在不使用任何卤素化合物的情况下具有高阻燃性，并且不损害施用组合物的制品的性质。

3. 发明授权

US5932637A Flame retardant resin composition and laminate using the same 失效
标题翻译：阻燃树脂组合物和使用其的层压材料
公开(公告)号：US5932637A
公开(公告)日：1999-08-03
申请号：US979540
申请日：1997-11-26
申请人： Mikio Ito , Sumiya Miyake , Kazuhiko Shibata , Akihiko Tobisawa
发明人： Mikio Ito , Sumiya Miyake , Kazuhiko Shibata , Akihiko Tobisawa
IPC分类号： B32B27/38 , C08G59/22 , C08G59/40 , C08G59/50 , C08G59/56 , C08K5/00 , C08K5/3417 , C08K5/49 , C08L63/00 , C09D163/00 , H05K1/03 , C08K5/521
CPC分类号： C08L63/00 , C08G59/4042 , C08G59/56 , C08K5/3417 , C08K5/49 , H05K1/0373
摘要： A flame-retardant resin composition which comprises (A) 100 parts by weight of an unhalogenated epoxy resin having at least two epoxy groups in one molecule, (B) 20 to 205 parts by weight of a maleimide compound having at least one maleimido group in one molecule, (C) 20 to 65 parts by weight of a curing agent having an amino group and (D) a phosphorus compound in a proportion of 0.5 to 4.5 parts by weight in terms of phosphorus element per 100 parts by weight of a total of the components (A), (B) and (C), provided that the proportion of nitrogen element contained in the composition is 2.0 to 10.0 parts by weight per 100 parts by weight of the total composition. The above flame-retardant resin composition has a high flame retardance without adding a halogen compound and does not deteriorate the characteristics of commercial products.
摘要翻译：一种阻燃树脂组合物，其包含（A）100重量份在一分子中具有至少两个环氧基的未卤化环氧树脂，（B）20至205重量份的具有至少一个马来酰亚胺基的马来酰亚胺化合物一分子，（C）20〜65重量份的具有氨基的固化剂和（D）磷化合物，按磷元素计为0.5〜4.5重量份/ 100重量份的组分（A），（B）和（C），条件是组合物中所含的氮元素的比例为每100重量份总组合物2.0至10.0重量份。上述阻燃树脂组合物在不添加卤素化合物的情况下具有高阻燃性，并且不劣化商品的特性。

4. 发明授权

US08188154B2 Decomposition reaction apparatus, system for producing raw material for recycled resin composition, method for producing raw material for recycled resin composition, raw material for recycled resin composition, and formed article 有权
标题翻译：分解反应装置，再生树脂组合物原料的制造系统，再生树脂组合物的原料的制造方法，再生树脂组合物的原料，成形体
公开(公告)号：US08188154B2
公开(公告)日：2012-05-29
申请号：US11667107
申请日：2005-10-07
申请人： Junya Goto , Sumiya Miyake , Masaki Ishikawa , Kazunori Shimoyachi
发明人： Junya Goto , Sumiya Miyake , Masaki Ishikawa , Kazunori Shimoyachi
IPC分类号： C08J11/04 , B01J8/00
CPC分类号： C08J11/18 , B01J3/00 , B01J3/008 , B01J4/008 , B01J19/20 , B01J19/243 , B01J2219/00033 , B01J2219/0009 , B01J2219/00135 , B01J2219/00162 , B01J2219/00164 , B01J2219/00166 , B01J2219/00168 , B01J2219/00184 , B01J2219/00252 , B01J2219/185 , B01J2219/1944 , Y02P20/544 , Y02P20/582 , Y02W30/706
摘要： A decomposition reaction apparatus for the decomposition treatment of a thermosetting resin, which comprises a reaction apparatus comprising an introduction section for introducing a resin composition containing the thermosetting resin and a solvent containing a monomer component of the thermosetting resin or a component similar to the monomer component, a decomposition reaction section for heating and pressuring the resin composition and the above solvent so as for the solvent to have a supercritical state or a subcritical state, to thereby prepare a treated and recovered product containing a recycled resin formed by the reduction of the molecular weight of the above thermosetting resin, and a discharge section for discharging the treated and recovered product. In the above reaction apparatus, the introduction of the resin composition and the solvent, the decomposition treatment of the thermosetting resin in the decomposition reaction section and the discharge of the treated and recovered product from the discharge section are all carried out continuously, and therefore, a raw material for a recycled resin composition using an industrial or general waste containing a thermosetting resin as the above resin composition can be produced continuously.
摘要翻译：一种用于热固性树脂的分解处理的分解反应装置，其包括反应装置，该反应装置包括用于引入含有热固性树脂的树脂组合物的引入部分和含有热固性树脂的单体组分的溶剂或类似于单体组分的组分，用于对树脂组合物和上述溶剂进行加压和加压以使溶剂具有超临界状态或亚临界状态的分解反应部分，从而制备含有通过还原分子形成的再循环树脂的处理和回收产物上述热固性树脂的重量，以及用于排出经处理和回收的产品的排出部分。在上述反应装置中，引入树脂组合物和溶剂，分解反应部中的热固性树脂的分解处理和从排出部排出的处理回收产物全部连续进行，可以连续生产使用含有热固性树脂的工业或一般废物作为上述树脂组合物的回收树脂组合物的原料。

5. 发明申请

US20090215912A1 Decomposition Reaction Apparatus, System For Producing Raw Material For Recycled Resin Composition, Method For Producing Raw Material For Recycled Resin Composition, Raw Material For Recycled Resin Composition, And Formed Article 有权
标题翻译：分解反应装置，用于生产用于再循环树脂组合物的原料的系统，用于生产用于再循环树脂组合物的原料的方法，用于再循环树脂组合物的原料和成型品
公开(公告)号：US20090215912A1
公开(公告)日：2009-08-27
申请号：US11667107
申请日：2005-10-07
申请人： Junya Goto , Sumiya Miyake , Masaki Ishikawa , Kazunori Shimoyachi
发明人： Junya Goto , Sumiya Miyake , Masaki Ishikawa , Kazunori Shimoyachi
IPC分类号： C08J11/10 , B09B3/00 , B01J19/18 , C07C37/86 , C07D301/32
CPC分类号： C08J11/18 , B01J3/00 , B01J3/008 , B01J4/008 , B01J19/20 , B01J19/243 , B01J2219/00033 , B01J2219/0009 , B01J2219/00135 , B01J2219/00162 , B01J2219/00164 , B01J2219/00166 , B01J2219/00168 , B01J2219/00184 , B01J2219/00252 , B01J2219/185 , B01J2219/1944 , Y02P20/544 , Y02P20/582 , Y02W30/706
摘要： A decomposition reaction apparatus for the decomposition treatment of a thermosetting resin, which comprises a reaction apparatus comprising an introduction section for introducing a resin composition containing the thermosetting resin and a solvent containing a monomer component of the thermosetting resin or a component similar to the monomer component, a decomposition reaction section for heating and pressuring the resin composition and the above solvent so as for the solvent to have a supercritical state or a subcritical state, to thereby prepare a treated and recovered product containing a recycled resin formed by the reduction of the molecular weight of the above thermosetting resin, and a discharge section for discharging the treated and recovered product. In the above reaction apparatus, the introduction of the resin composition and the solvent, the decomposition treatment of the thermosetting resin in the decomposition reaction section and the discharge of the treated and recovered product from the discharge section are all carried out continuously, and therefore, a raw material for a recycled resin composition using an industrial or general waste containing a thermosetting resin as the above resin composition can be produced continuously.
摘要翻译：一种用于热固性树脂的分解处理的分解反应装置，其包括反应装置，该反应装置包括用于引入含有热固性树脂的树脂组合物的引入部分和含有热固性树脂的单体组分的溶剂或类似于单体组分的组分，用于对树脂组合物和上述溶剂进行加压和加压以使溶剂具有超临界状态或亚临界状态的分解反应部分，从而制备含有通过还原分子形成的再循环树脂的处理和回收产物上述热固性树脂的重量，以及用于排出经处理和回收的产品的排出部分。在上述反应装置中，引入树脂组合物和溶剂，分解反应部中的热固性树脂的分解处理和从排出部排出的处理回收产物全部连续进行，可以连续生产使用含有热固性树脂的工业或一般废物作为上述树脂组合物的回收树脂组合物的原料。

6. 发明授权

US06946421B2 Latent catalyst 失效
标题翻译：潜在催化剂
公开(公告)号：US06946421B2
公开(公告)日：2005-09-20
申请号：US10320474
申请日：2002-12-17
申请人： Sumiya Miyake , Akiko Okubo , Hiromi Honda , Yoshiyuki Go , Hiroshi Nagata , Minoru Kobayashi
发明人： Sumiya Miyake , Akiko Okubo , Hiromi Honda , Yoshiyuki Go , Hiroshi Nagata , Minoru Kobayashi
IPC分类号： B01J31/02 , B01J31/14 , C08G59/24 , C08G59/68 , C08G73/12 , C08L63/00 , H01L23/29 , B01J31/20 , B01J31/22 , C08K63/04
CPC分类号： H01L23/293 , B01J31/0268 , B01J31/06 , B01J31/146 , C08G59/245 , C08G59/68 , C08G59/688 , C08G73/121 , C08L63/00 , H01L2924/0002 , Y10T428/31511 , C08L61/04 , H01L2924/00
摘要： This invention provides a latent catalyst having a structure of phosphonium borate consisting of a monovalent cation portion in which four specific groups are bonded to the phosphorus atom and a monovalent anion portion in which four specific groups are bonded to the boron atom, and a latent catalyst having a structure wherein the above phosphonium borate is the recurring unit and at least two of said recurring unit are connected through at least one of the four specific groups bonded to the boron atom. This invention also provides a thermo-setting resin composition comprising such a latent catalyst and an epoxy resin molding material comprising such a latent catalyst and further provides a semiconductor device in which a semiconductor is encapsulated with said epoxy resin molding material.
摘要翻译：本发明提供一种潜在催化剂，其具有由一个阳离子部分组成的硼酸鏻结构，其中四个特定基团与磷原子键合，其中四个特定基团与硼原子键合的一价阴离子部分，潜在催化剂具有其中上述硼酸鏻是重复单元的结构，并且所述重复单元中的至少两个通过键合到硼原子的四个特定基团中的至少一个连接。本发明还提供一种包含这种潜催化剂和包含这种潜催化剂的环氧树脂模制材料的热固性树脂组合物，并且还提供半导体装置，其中半导体被所述环氧树脂模制材料包封。

7. 发明授权

US06296940B1 Laminate comprising a flame-retardant resin composition 失效
标题翻译：包含阻燃树脂组合物的层压材料
公开(公告)号：US06296940B1
公开(公告)日：2001-10-02
申请号：US09603961
申请日：2000-06-26
申请人： Mikio Ito , Sumiya Miyake
发明人： Mikio Ito , Sumiya Miyake
IPC分类号： B32B1508
CPC分类号： C09K21/14 , C08K5/53 , C08L61/06 , C08L63/00 , C09K21/12 , Y10T428/31518 , Y10T428/31522 , C08L2666/22
摘要： The present invention provides a flame-retardant resin composition comprising: (A) an epoxy resin other than halogenated epoxy resins, having at least two epoxy groups in the molecule, (B) a curing agent, and (C) a product obtained by reacting (C1) a phosphorus compound having at least one P-H linkage in the molecule, with (C2) a compound having, in the molecule, at least one functional group selected from the group consisting of C—C double bond, epoxy group, alcoholic hydroxyl group and carbonyl group, and at least one functional group selected from the group consisting of epoxy group, phenolic hydroxyl group, amino group, cyanate ester group and isocyanate group, and having a phosphorus content of 0.3% by weight to 8% by weight. This resin composition has high flame retardancy without using any halogen compound and does not impair the properties of an article to which the composition is applied.
摘要翻译：本发明提供一种阻燃性树脂组合物，其包含：（A）除了分子内具有至少两个环氧基的卤代环氧树脂以外的环氧树脂，（B）固化剂，和（C）通过使（C1）分子中具有至少一个PH键的磷化合物，（C2）在分子中具有至少一个选自CC双键，环氧基，醇羟基和羰基，以及选自环氧基，酚羟基，氨基，氰酸酯基和异氰酸酯基中的至少一种官能团，磷含量为0.3重量％〜8重量％。该树脂组合物在不使用任何卤素化合物的情况下具有高阻燃性，并且不损害施用组合物的制品的性质。

8. 发明授权

US06881812B2 Thermosetting resin and tetraorganophosphonium dicyclic tetraorganoborane catalyst 失效
标题翻译：热固性树脂和四有机鏻二环四有机硼烷催化剂
公开(公告)号：US06881812B2
公开(公告)日：2005-04-19
申请号：US10320475
申请日：2002-12-17
申请人： Sumiya Miyake , Akiko Okubo , Hiromi Honda , Yoshiyuki Go , Hiroshi Nagata , Minoru Kobayashi
发明人： Sumiya Miyake , Akiko Okubo , Hiromi Honda , Yoshiyuki Go , Hiroshi Nagata , Minoru Kobayashi
IPC分类号： B01J31/02 , B01J31/14 , C08G59/24 , C08G59/68 , C08G73/12 , C08L63/00 , H01L23/29 , B01J31/20 , B01J31/22 , C08K63/04
CPC分类号： H01L23/293 , B01J31/0268 , B01J31/06 , B01J31/146 , C08G59/245 , C08G59/68 , C08G59/688 , C08G73/121 , C08L63/00 , H01L2924/0002 , Y10T428/31511 , C08L61/04 , H01L2924/00
摘要： This invention provides a latent catalyst having a structure of phosphonium borate consisting of a monovalent cation portion in which four specific groups are bonded to the phosphorus atom and a monovalent anion portion in which four specific groups are bonded to the boron atom, and a latent catalyst having a structure wherein the above phosphonium borate is the recurring unit and at least two of said recurring unit are connected through at least one of the four specific groups bonded to the boron atom. This invention also provides a thermosetting resin composition comprising such a latent catalyst and an epoxy resin molding material comprising such a latent catalyst and further provides a semiconductor device in which a semiconductor is encapsulated with said epoxy resin molding material.
摘要翻译：本发明提供一种潜在催化剂，其具有由一个阳离子部分组成的硼酸鏻结构，其中四个特定基团与磷原子键合，其中四个特定基团与硼原子键合的一价阴离子部分，潜在催化剂具有其中上述硼酸鏻是重复单元的结构，并且所述重复单元中的至少两个通过键合到硼原子的四个特定基团中的至少一个连接。本发明还提供一种包含这种潜催化剂和包含这种潜催化剂的环氧树脂模制材料的热固性树脂组合物，并且还提供半导体器件，其中半导体被所述环氧树脂模制材料封装。

9. 发明授权

US06664344B1 Composition of polyepoxide, phenolic co-condensate and phosphonium-polyphenolic molecular association product 有权
标题翻译：聚环氧化物，酚类共缩合物和鏻多酚分子缔合产物的组成
公开(公告)号：US06664344B1
公开(公告)日：2003-12-16
申请号：US09762950
申请日：2001-02-15
申请人： Hiromi Oki , Yoshiyuki Go , Sumiya Miyake , Yoshihito Akiyama
发明人： Hiromi Oki , Yoshiyuki Go , Sumiya Miyake , Yoshihito Akiyama
IPC分类号： C08L6300
CPC分类号： H01L23/293 , C08G59/621 , C08G59/688 , H01L2924/0002 , H01L2924/00
摘要： The present invention provides an epoxy resin composition that has both a rapidly-curability and an excellent storage stability and is useful in the field of electronic and electric materials. That is, the present invention is an epoxy resin composition comprising a compound (A) having two or more epoxy groups in the molecule, a co-condensation product (B) having two or more phenolic hydroxyl groups in the molecule, and a molecular association product (C) of a tetra-substituted phosphonium (X), a compound (Y) having two or more phenolic hydroxyl groups in the molecule, and a conjugate base of the compound (Y) having two or more phenolic hydroxyl groups in the molecule, said conjugate base being a phenoxide type compound obtained by removing a hydrogen atom from the aforesaid compound (Y) having two or more phenolic hydroxyl groups in the molecule.
摘要翻译：本发明提供了具有快速固化性和优异的储存稳定性的环氧树脂组合物，并且在电子和电气材料领域中是有用的。也就是说，本发明是一种环氧树脂组合物，其包含分子中具有两个以上环氧基的化合物（A），分子中具有两个以上酚羟基的共缩合产物（B）和分子缔合四取代鏻（X）的产物（C），分子中具有两个或多个酚羟基的化合物（Y）和分子中具有两个或多个酚羟基的化合物（Y）的共轭碱所述共轭碱是通过从分子中具有两个或多个酚羟基的上述化合物（Y）除去氢原子得到的酚盐型化合物。

10. 发明授权

US06306792B1 Evaluating moisture resistance reliability of phosphonium borate catalyst 失效
标题翻译：评估硼酸铌催化剂的耐湿可靠性
公开(公告)号：US06306792B1
公开(公告)日：2001-10-23
申请号：US09201812
申请日：1998-12-01
申请人： Sumiya Miyake , Akiko Okubo , Hiromi Honda , Yoshiyuki Go , Hiroshi Nagata , Minoru Kobayashi
发明人： Sumiya Miyake , Akiko Okubo , Hiromi Honda , Yoshiyuki Go , Hiroshi Nagata , Minoru Kobayashi
IPC分类号： B01J3120
CPC分类号： H01L23/293 , B01J31/0268 , B01J31/06 , B01J31/146 , C08G59/245 , C08G59/68 , C08G59/688 , C08G73/121 , C08L63/00 , H01L2924/0002 , Y10T428/31511 , C08L61/04 , H01L2924/00
摘要： The moisture resistance reliability of a latent catalyst is evaluated for a phosphonium borate wherein at least one group pendant on the boron atom is a group formed when a proton donor having at least one proton capable of being liberated out of the molecule has liberated one or at least two protons, the evaluation comprising (1) mixing one gram of the proton donor wherefrom the latent catalyst is derived with 50 grams of purified water to obtain an aqueous mixture, (3) subjecting the aqueous mixture to pressure cooker treatment at a temperature of 125° C. for 20 hours in a pressure cooker vessel to obtain an extraction mixture, and (4) measuring the electrical conductivity of the extraction mixture wherein the acceptable electrical conductivity of the extraction mixture is no greater than 1,000 &mgr;S/cm.
摘要翻译：评估潜在催化剂的耐湿可靠性，其中硼原子上的至少一个侧基是当具有至少一个能够从分子中释放的质子的质子供体释放出一个或在至少两个质子，评估包括（1）将1克质子供体与潜在催化剂得到的溶液与50克纯净水混合以获得含水混合物，（3）在含水混合物的温度为 125℃在压力锅容器中干燥20小时以获得提取混合物，和（4）测量萃取混合物的电导率，其中提取混合物的可接受电导率不大于1,000μS/ cm。

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