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1. 发明申请

US20130317252A1 STABILIZED ISOCYANATE GROUP-CONTAINING ETHYLENICALLY UNSATURATED COMPOUND 审中-公开
标题翻译：稳定的含异氰酸酯基的亚乙基不饱和化合物
公开(公告)号：US20130317252A1
公开(公告)日：2013-11-28
申请号：US13984381
申请日：2012-02-02
申请人： Norihito Nishimura , Shinichi Yorozuya , Katsutoshi Ohno
发明人： Norihito Nishimura , Shinichi Yorozuya , Katsutoshi Ohno
IPC分类号： C07C263/18 , C07C265/04
CPC分类号： C07C263/18 , C07C265/04
摘要： An object of the present invention is to improve the stability of an ethylenically unsaturated compound having an isocyanate group in the molecule by preventing a polymerization, a multimerization reaction and a discoloration reaction of the ethylenically unsaturated compound. The present invention relates to a stabilizing composition for an isocyanate group-containing ethylenically unsaturated compound, comprising: an isocyanate group-containing ethylenically unsaturated compound (A) which comprises one or more isocyanate groups and one or more ethylenically unsaturated groups in the molecule; and a stabilizing agent (B) which is a compound in which at least one of the ethylenically unsaturated groups in the compound (A) is replaced with an alkyl halide group or an amino alkyl group which may have a substituent.
摘要翻译：本发明的目的是通过防止烯键式不饱和化合物的聚合，多聚反应和变色反应来提高分子中具有异氰酸酯基的烯属不饱和化合物的稳定性。本发明涉及含有异氰酸酯基的烯属不饱和化合物的稳定组合物，其包含：含有异氰酸酯基的烯属不饱和化合物（A），其在分子中包含一个或多个异氰酸酯基和一个或多个烯属不饱和基团; 和稳定剂（B），其中化合物（A）中的至少一个烯属不饱和基团被烷基卤基团或可以具有取代基的氨基烷基取代的化合物。

2. 发明申请

US20110137066A1 PROCESS OF INHIBITING POLYMERIZATION OF ISOCYANATE GROUP-CONTAINING, ETHYLENICALLY UNSATURATED CARBOXYLATE COMPOUNDS, AND PROCESS FOR PRODUCING THE COMPOUNDS 审中-公开
标题翻译：抑制含异氰酸酯基的聚合，乙烯基不饱和羧酸酯化合物的方法及其制备方法
公开(公告)号：US20110137066A1
公开(公告)日：2011-06-09
申请号：US13057707
申请日：2009-08-06
申请人： Norihito Nishimura , Shinichi Yorozuya
发明人： Norihito Nishimura , Shinichi Yorozuya
IPC分类号： C07C67/62
CPC分类号： C07C263/10 , C07C263/16 , C07C263/18 , C07C265/04
摘要： It is an object of the invention to provide a process of inhibiting polymerization of isocyanate group-containing, ethylenically unsaturated carboxylate compounds, and a process for producing isocyanate group-containing, ethylenically unsaturated carboxylate compounds which involves the polymerization inhibition process. The process of inhibiting polymerization of isocyanate group-containing, ethylenically unsaturated carboxylate compounds of the invention includes controlling the oxygen gas (O2) concentration in a liquid phase containing an isocyanate group-containing, ethylenically unsaturated carboxylate compound to not less than 0.5 mg/L. In a preferred embodiment, a gas containing oxygen gas (O2) is introduced to the liquid phase. In another preferred embodiment, the oxygen gas (O2) concentration in the liquid phase is measured with an electrode that is immersed in the liquid phase.
摘要翻译：本发明的目的是提供一种抑制含异氰酸酯基的烯键式不饱和羧酸酯化合物聚合的方法，以及涉及聚合抑制过程的含异氰酸酯基的烯属不饱和羧酸酯化合物的制备方法。抑制本发明的含异氰酸酯基的烯属不饱和羧酸酯化合物的聚合的方法包括将含有异氰酸酯基的烯属不饱和羧酸酯化合物的液相中的氧气（O 2）浓度控制在不小于0.5mg / L 。在优选的实施方案中，将含有氧气（O 2）的气体引入液相。在另一个优选实施方案中，用浸入液相的电极测量液相中的氧气（O 2）浓度。

3. 发明授权

US08066977B2 Agent for permanent hair waving containing heterocyclic mercapto compound 有权
标题翻译：含有杂环巯基化合物的永久性头发挥发剂
公开(公告)号：US08066977B2
公开(公告)日：2011-11-29
申请号：US11884413
申请日：2006-05-25
申请人： Akira Shibuya , Shinichi Yorozuya , Makoto Saito
发明人： Akira Shibuya , Shinichi Yorozuya , Makoto Saito
IPC分类号： A61Q5/04
CPC分类号： A61Q5/04 , A61K8/4933
摘要： Disclosed is an agent for permanent hair waving that can realize permanent hair waving even in the neutral to weakly acidic pH range in which irritation particularly to the skin is not significant. The agent for permanent hair waving includes at least one heterocyclic mercapto compound represented by formula (1): wherein R1 and R2 each independently represent a hydrogen atom or an optionally substituted alkyl group having 1 to 5 carbon atoms; X represents —O—, —S—, —NH—, or —NR3—; R3 represents an alkyl group having 1 to 5 carbon atoms; n is an integer of 0 to 2; and, when n is 2, group SH may be attached to any carbon atom of an alkylene group having 2 carbon atoms.
摘要翻译：公开了即使在特别是对皮肤的刺激不显着的中性至弱酸性pH范围内也能实现永久性头发挥发的药剂。永久性头发挥发剂包括至少一种由式（1）表示的杂环巯基化合物：其中R 1和R 2各自独立地表示氢原子或任选取代的具有1至5个碳原子的烷基; X表示-O - ， - S - ， - NH-或-NR 3 - ; R3表示碳原子数1〜5的烷基。 n为0〜2的整数，并且当n为2时，基团SH可以连接到具有2个碳原子的亚烷基的任何碳原子上。

4. 发明申请

US20090208439A1 Agent for Permanent Hair Waving Containing Heterocyclic Mercapto Compound 有权
标题翻译：含有杂环巯基化合物的永久性头发挥发剂
公开(公告)号：US20090208439A1
公开(公告)日：2009-08-20
申请号：US11884413
申请日：2006-05-25
申请人： Akira Shibuya , Shinichi Yorozuya , Makoto Saito
发明人： Akira Shibuya , Shinichi Yorozuya , Makoto Saito
IPC分类号： A61K8/49 , C07D233/40 , A61Q5/04
CPC分类号： A61Q5/04 , A61K8/4933
摘要： Disclosed is an agent for permanent hair waving that can realize permanent hair waving even in the neutral to weakly acidic pH range in which irritation particularly to the skin is not significant. The agent for permanent hair waving includes at least one heterocyclic mercapto compound represented by formula (1): wherein R1 and R2 each independently represent a hydrogen atom or an optionally substituted alkyl group having 1 to 5 carbon atoms; X represents —O—, —S—, —NH—, or —NR3—; R3 represents an alkyl group having 1 to 5 carbon atoms; n is an integer of 0 to 2; and, when n is 2, group SH may be attached to any carbon atom of an alkylene group having 2 carbon atoms.
摘要翻译：公开了即使在特别是对皮肤的刺激不显着的中性至弱酸性pH范围内也能实现永久性头发挥发的药剂。永久性头发挥发剂包括至少一种由式（1）表示的杂环巯基化合物：其中R 1和R 2各自独立地表示氢原子或任选取代的具有1至5个碳原子的烷基; X表示-O - ， - S - ， - NH-或-NR 3 - ; R3表示碳原子数1〜5的烷基。 n为0〜2的整数，并且当n为2时，基团SH可以连接到具有2个碳原子的亚烷基的任何碳原子上。

5. 发明授权

US09040736B2 Stabilized isocyanate group-containing ethylenically unsaturated compound 有权
标题翻译：含有稳定的含异氰酸酯基团的烯属不饱和化合物
公开(公告)号：US09040736B2
公开(公告)日：2015-05-26
申请号：US13984391
申请日：2012-02-02
申请人： Norihito Nishimura , Shinichi Yorozuya
发明人： Norihito Nishimura , Shinichi Yorozuya
IPC分类号： C07C69/00 , C07C263/18 , C07C265/04
CPC分类号： C07C263/18 , C07C265/04
摘要： An object of the present invention is to improve the stability of an ethylenically unsaturated compound having an isocyanate group in the molecule by preventing a polymerization of the ethylenically unsaturated compound. The present invention relates to a stabilizing composition for an isocyanate group-containing ethylenically unsaturated compound, comprising: an isocyanate group-containing ethylenically unsaturated compound (A) which comprises one or more isocyanate groups and one or more ethylenically unsaturated groups in the molecule; and a stabilizing agent (B) which is a compound in which at least one of the ethylenically unsaturated groups in the compound (A) is replaced with an alkyl group which may have a substituent.
摘要翻译：本发明的目的是通过防止烯键式不饱和化合物的聚合来提高分子中具有异氰酸酯基团的烯属不饱和化合物的稳定性。本发明涉及含有异氰酸酯基的烯属不饱和化合物的稳定组合物，其包含：含有异氰酸酯基的烯属不饱和化合物（A），其在分子中包含一个或多个异氰酸酯基和一个或多个烯属不饱和基团; 和稳定剂（B），其中化合物（A）中的至少一个烯属不饱和基团被可以具有取代基的烷基取代的化合物。

6. 发明申请

US20130317248A1 STABILIZED ISOCYANATE GROUP-CONTAINING ETHYLENICALLY UNSATURATED COMPOUND 有权
标题翻译：稳定的含异氰酸酯基的亚乙基不饱和化合物
公开(公告)号：US20130317248A1
公开(公告)日：2013-11-28
申请号：US13984391
申请日：2012-02-02
申请人： Norihito Nishimura , Shinichi Yorozuya
发明人： Norihito Nishimura , Shinichi Yorozuya
IPC分类号： C07C263/18 , C07C265/04
CPC分类号： C07C263/18 , C07C265/04
摘要： An object of the present invention is to improve the stability of an ethylenically unsaturated compound having an isocyanate group in the molecule by preventing a polymerization of the ethylenically unsaturated compound. The present invention relates to a stabilizing composition for an isocyanate group-containing ethylenically unsaturated compound, comprising: an isocyanate group-containing ethylenically unsaturated compound (A) which comprises one or more isocyanate groups and one or more ethylenically unsaturated groups in the molecule; and a stabilizing agent (B) which is a compound in which at least one of the ethylenically unsaturated groups in the compound (A) is replaced with an alkyl group which may have a substituent.
摘要翻译：本发明的目的是通过防止烯键式不饱和化合物的聚合来提高分子中具有异氰酸酯基团的烯属不饱和化合物的稳定性。本发明涉及含有异氰酸酯基的烯属不饱和化合物的稳定组合物，其包含：含有异氰酸酯基的烯属不饱和化合物（A），其在分子中包含一个或多个异氰酸酯基和一个或多个烯属不饱和基团; 和稳定剂（B），其中化合物（A）中的至少一个烯属不饱和基团被可以具有取代基的烷基取代的化合物。

7. 发明授权

US07902383B2 Production method of heterocyclic mercapto compound 有权
标题翻译：杂环巯基化合物的制备方法
公开(公告)号：US07902383B2
公开(公告)日：2011-03-08
申请号：US12302226
申请日：2007-05-28
申请人： Shinichi Yorozuya , Hidemasa Aoki
发明人： Shinichi Yorozuya , Hidemasa Aoki
IPC分类号： C07D307/00 , C07D309/30 , C07D213/69 , C07D207/00
CPC分类号： C07D307/30 , C07D207/273 , C07D223/10 , C07D333/34
摘要： A method of the invention industrially produces heterocyclic mercapto compounds useful as raw materials or intermediates in the synthesis of medicaments or pesticides, or as permanent wave agent, with a high yield and high productivity using easily available starting materials. A heterocyclic mercapto compound represented by Formula (1) (wherein X represents any structure of —O—, —S—, —NH—, and —NR1—; R1 represents any of an alkyl group, alkoxy group and alkoxyalkyl group each having 1 to 6 carbon atoms; Y represents an oxygen atom, a sulfur atom or —NR2—; R2 represents a hydrogen atom or alkyl group having 1 to 6 carbon atoms; and Z1 represents a divalent organic residue having at least one mercapto group) is produced by reacting a metal sulfide or a metal hydrosulfide with a compound represented by Formula (2) (wherein X and Y are as defined in Formula (1); and Z2 represents a divalent organic residue having at least one halogen group) in the presence of a solvent at a pH of 7.0 to 11.0.
摘要翻译：本发明的工业生产方法是使用容易获得的起始原料工业生产用作合成药物或农药的原料或中间体的杂环巯基化合物，或作为永久挥发剂，以高产率和高生产率。由式（1）表示的杂环巯基化合物（其中X表示-O - ， - S - ， - NH-和-NR 1 - 的任何结构; R 1表示任何烷基，烷氧基和烷氧基烷基， 6个碳原子; Y表示氧原子，硫原子或-NR 2 - ; R 2表示氢原子或碳原子数1〜6的烷基，Z1表示具有至少一个巯基的二价有机残基）通过使金属硫化物或金属氢硫化物与式（2）表示的化合物反应（其中X和Y如式（1）中所定义; Z 2表示具有至少一个卤素基团的二价有机残基） pH 7.0〜11.0的溶剂。

8. 发明申请

US20090171095A1 PRODUCTION METHOD OF HETEROCYCLIC MERCAPTO COMPOUND 有权
标题翻译：杂环化合物的生产方法
公开(公告)号：US20090171095A1
公开(公告)日：2009-07-02
申请号：US12302226
申请日：2007-05-28
申请人： Shinichi Yorozuya , Hidemasa Aoki
发明人： Shinichi Yorozuya , Hidemasa Aoki
IPC分类号： C07D213/70 , C07D307/33 , C07D207/24 , C07D309/30
CPC分类号： C07D307/30 , C07D207/273 , C07D223/10 , C07D333/34
摘要： A method of the invention industrially produces heterocyclic mercapto compounds useful as raw materials or intermediates in the synthesis of medicaments or pesticides, or as permanent wave agent, with a high yield and high productivity using easily available starting materials. A heterocyclic mercapto compound represented by Formula (1) (wherein X represents any structure of —O—, —S—, —NH—, and —NR1—; R1 represents any of an alkyl group, alkoxy group and alkoxyalkyl group each having 1 to 6 carbon atoms; Y represents an oxygen atom, a sulfur atom or —NR2—; R2 represents a hydrogen atom or alkyl group having 1 to 6 carbon atoms; and Z1 represents a divalent organic residue having at least one mercapto group) is produced by reacting a metal sulfide or a metal hydrosulfide with a compound represented by Formula (2) (wherein X and Y are as defined in Formula (1); and Z2 represents a divalent organic residue having at least one halogen group) in the presence of a solvent at a pH of 7.0 to 11.0.
摘要翻译：本发明的工业生产方法是使用容易获得的起始原料工业生产用作合成药物或农药的原料或中间体的杂环巯基化合物，或作为永久挥发剂，以高产率和高生产率。由式（1）表示的杂环巯基化合物（其中X表示-O - ， - S - ， - NH-和-NR 1 - 的任何结构; R 1表示任何烷基，烷氧基和烷氧基烷基， 6个碳原子; Y表示氧原子，硫原子或-NR 2 - ; R 2表示氢原子或碳原子数1〜6的烷基，Z1表示具有至少一个巯基的二价有机残基）通过使金属硫化物或金属氢硫化物与式（2）表示的化合物反应（其中X和Y如式（1）中所定义; Z 2表示具有至少一个卤素基团的二价有机残基） pH 7.0〜11.0的溶剂。

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