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1. 发明授权

US6103029A Triazole cross-linked polymers 失效
标题翻译：三唑交联聚合物
公开(公告)号：US6103029A
公开(公告)日：2000-08-15
申请号：US880710
申请日：1997-06-23
申请人： Russell Reed, Jr.
发明人： Russell Reed, Jr.
IPC分类号： C06B45/10 , C08G65/325 , C06B33/12 , C08G63/91 , C08G73/00
CPC分类号： C08G65/325 , C06B45/105
摘要： Polyethers containing pendant azide groups are cured without a catalyst byyclo-addition with diacetylenes to form triazole cross-linked, energetic binders having improved mechanical properties and stability. The polyethers typically have three hydroxy-terminated chains each of about 5000 to about 50,000 daltons. Ideally, only one azide group per chain reacts by cyclo-addition since the diacetylene is added in a proportion of about one molecule to each two polyether chains. Repeating units of glycidal azide, azidomethylmethyloxetane, bis-azidomethyloxetane/nitratomethylmethyloxetane, and bis-azidomethyloxetane/azidomethylmethyloxetane are believed effective as polyethers when used with the diethynlbenzenes 1,4-bis(ethynl)benzene, 1,4-bis(ethynlcarbonyl)benzene, and 1,3-bis(cyanoethynl)benzene. The polyethers may be further cross-liked at the hydroxyl terminations by urethane bonds.
摘要翻译：含有叠氮化物基团的聚醚通过与二乙炔进行环加成而不用催化剂固化，形成具有改善的机械性能和稳定性的三唑交联的高能粘合剂。聚醚通常具有每个约5000至约50,000道尔顿的三个羟基封端的链。理想情况下，每个链只有一个叠氮基团通过环加成反应，因为二乙炔以每一个聚醚链约1分子的比例加入。当与二乙烯苯1,4-双（乙炔）苯，1,4-双（乙炔羰基）苯，二甲基亚氨基甲基苯，1,4-双（乙炔基）苯，二甲基甲硅烷基苯，和1,3-双（氰乙炔）苯。聚醚可以通过氨基甲酸酯键在羟基末端进一步交叉。

2. 发明授权

US5520826A Flame extinguishing pyrotechnic and explosive composition 失效
标题翻译：火焰灭火和爆炸物组成
公开(公告)号：US5520826A
公开(公告)日：1996-05-28
申请号：US249778
申请日：1994-05-16
申请人： Russell Reed, Jr. , Vicki L. Brady
发明人： Russell Reed, Jr. , Vicki L. Brady
IPC分类号： A62D1/06 , C06B45/10 , C06D5/06 , C06B45/06
CPC分类号： C06D5/06 , A62D1/06 , C06B45/105
摘要： A flame extinguishing pyrotechnic which flamelessly deflagrates to producerimarily nitrogen, carbon dioxide, and a fluoroolefin. The flame extinguishing characteristic is achieved by reducing the content of oxygen proximate the deflagration as well as through the flame suppressing properties of particular fluoroolefins. The pyrotechnic composition contains an azido binder such as glycidyl azide polymer (GAP), an azido plasticizer, a solid tetrazole, and a perfluorocarboxylic acid salt. This composition is cured to a rubbery composite by the addition of an isocyanate.
摘要翻译：一种火焰灭火烟火，无火焰地爆燃以主要产生氮气，二氧化碳和氟烯烃。灭火特性是通过降低爆燃附近的氧含量以及通过特定氟烯烃的阻燃性能来实现的。烟火组合物包含叠氮基粘合剂，例如缩水甘油基叠氮化物聚合物（GAP），叠氮增塑剂，固体四唑和全氟羧酸盐。该组合物通过加入异氰酸酯固化成橡胶状复合材料。

3. 发明授权

US5061330A Insensitive high energetic explosive formulations 失效
标题翻译：不敏感高能爆炸制剂
公开(公告)号：US5061330A
公开(公告)日：1991-10-29
申请号：US440678
申请日：1982-11-01
申请人： Russell Reed, Jr. , May L. Chan
发明人： Russell Reed, Jr. , May L. Chan
IPC分类号： C06B25/34 , C06B45/10
CPC分类号： C06B25/34 , C06B45/105
摘要： A cast cured propellant and explosive with a higher volume percentage of ymer resulting in improved mechanical and safety properties is made from glycidyl azide polymer, an energetic plasticizer and HMX or RDX. Aluminum powder can also be added.
摘要翻译：由缩水甘油基叠氮化物聚合物，高能增塑剂和HMX或RDX制成具有较高体积百分数聚合物的铸塑固化推进剂和爆炸物，从而改善机械和安全性能。也可加入铝粉。

4. 发明授权

US5042385A Inhibitor and barrier for use with high energy rocket propellants 失效
标题翻译：用于高能火箭推进剂的抑制剂和屏障
公开(公告)号：US5042385A
公开(公告)日：1991-08-27
申请号：US460682
申请日：1983-01-24
申请人： Russell Reed, Jr. , May L. Chan
发明人： Russell Reed, Jr. , May L. Chan
IPC分类号： C06B45/12 , F02K9/34
CPC分类号： F02K9/346 , C06B45/12
摘要： A flame inhibitor coating for application to those surfaces of a solid prllant grain in a rocket motor where burning is not desired such as the aft end of a perforated propellant grain which includes a barrier layer of a mixture of amine silane, a trialkoxypropylsilylamino prepolymer, and diglycidylether of polypropylene glycol, an epoxy applied to the grain surface and allowed to cure to a polysiloxane layer, and a flame inhibitor layer applied over the barrier layer consisting of a mixture of hydroxyl terminated polybutadiene and dimeryl diisocyanate with flake aluminum which is applied over the barrier layer and allowed to cure. The barrier layer prevents migration of nitrate esters from the solid propellant grain to the flame inhibitor layer thus preventing peeling and reduction of flame inhibiting properties. The polysiloxane barrier layer is also useful in itself as a flame inhibitor and can also be employed between the insulator/liner of the rocket motor and the solid propellant grain.
摘要翻译：用于火箭发动机的固体推进剂颗粒的那些表面的阻燃剂涂层，其中不需要燃烧，例如穿孔推进剂颗粒的后端，其包括胺硅烷，三烷氧基丙基甲硅烷基氨基预聚物和三烷氧基丙基甲硅烷基氨基预聚物的混合物的阻挡层和聚丙二醇的二缩水甘油醚，施加到晶粒表面并使其固化成聚硅氧烷层的环氧树脂，以及施加在由羟基封端的聚丁二烯和二聚二异氰酸酯的混合物组成的阻挡层上的阻燃层，阻挡层并允许固化。阻挡层防止硝酸酯从固体推进剂颗粒向阻燃剂层迁移，从而防止阻燃性能的剥离和降低。聚硅氧烷阻挡层本身也可用作阻燃剂，也可用于火箭发动机的绝缘体/内衬与固体推进剂颗粒之间。

5. 发明授权

US4379903A Propellant binders cure catalyst 失效
标题翻译：推进剂粘合剂固化催化剂
公开(公告)号：US4379903A
公开(公告)日：1983-04-12
申请号：US353773
申请日：1982-03-01
申请人： Russell Reed, Jr. , May L. Chan
发明人： Russell Reed, Jr. , May L. Chan
IPC分类号： C06B45/10 , C08G18/22 , C08G18/50 , C08G18/38
CPC分类号： C08G18/5021 , C06B45/10 , C06B45/105 , C08G18/22
摘要： A multiple component catalyst system for curing of energetic urethane bins for solid fuel propellants and gas generators based upon curing of glycidyl-azide polymer and isocynate curative mixtures. Void or bubble free propellant grains are obtained by employing a cure catalyst composed of a mixture of triphenyl bismuth and dibutyltin dilaurate, preferably in a respective ratio of about 10:1 by weight. The void free propellant grains have burn characteristics acceptable for missile propulsion applications.
摘要翻译：一种用于固化固体燃料推进剂和气体发生器的能量聚氨酯粘合剂的多组分催化剂体系，其基于缩水甘油基叠氮化物聚合物和异氰酸酯固化剂混合物的固化。通过使用由三苯基铋和二月桂酸二丁基锡的混合物组成的固化催化剂，优选以约10:1重量比的比例，获得无孔或无气泡的推进剂颗粒。无空隙的推进剂颗粒具有可接受的导弹推进应用的燃烧特性。

6. 发明授权

US4350542A Bonding agent for HMX (cyclotetramethylenetetranitramine) 失效
标题翻译： HMX粘合剂（环四亚甲基四胺）
公开(公告)号：US4350542A
公开(公告)日：1982-09-21
申请号：US135563
申请日：1980-03-31
申请人： John F. Kincaid , Russell Reed, Jr.
发明人： John F. Kincaid , Russell Reed, Jr.
IPC分类号： C06B21/00 , C06B45/10 , C06B45/22 , C06B25/34 , C07D251/14
CPC分类号： C06B45/10 , C06B21/0083 , C06B45/22
摘要： The present invention relates to an improved propellant or explosive and hod for making it having increased energy yet having increased toughness and hazard properties. More specifically, an HMX or RDX material is coated with a nitrocellulose, poly-hydroxyethyl acrylate or poly-hydroxymethyl acrylate for bonding hydroxyl groups that subsequently allows reaction with amine silane/s or a polymer of the type ##STR1## wherein n is an integer of 3 or 4, m is an integer of 2 or 3, and R is methyl or ethyl. Further coating of the product is then carried out with a primary hydroxyl forming material and then curing the product in the presence of an isocyanate.
摘要翻译：本发明涉及一种改进的推进剂或爆炸物以及使其具有增加的能量但具有增加的韧性和危险性质的方法。更具体地，HMX或RDX材料涂覆有硝化纤维素，丙烯酸聚羟基乙酯或聚羟基甲基丙烯酸酯，用于键合羟基，其随后允许与胺硅烷反应或者类型为“IMAGE”的聚合物，其中n是整数 3或4，m为2或3的整数，R为甲基或乙基。然后用初级羟基形成材料进行产物的进一步包覆，然后在异氰酸酯的存在下固化产物。

7. 发明授权

US4293352A Degradable binder explosives 失效
标题翻译：可降解粘结剂炸药
公开(公告)号：US4293352A
公开(公告)日：1981-10-06
申请号：US69215
申请日：1979-08-23
申请人： Benjamin Y. S. Lee , Russell Reed, Jr. , Roger L. Miller
发明人： Benjamin Y. S. Lee , Russell Reed, Jr. , Roger L. Miller
IPC分类号： C06B45/10 , C08G18/42
CPC分类号： C06B45/10 , C08G18/4244
摘要： Explosive compositions containing a polyurethane binder which will degradepon contact with dilute mineral acids or aqueous ammonia.
摘要翻译：含有聚氨酯粘合剂的爆炸性组合物在与稀无机酸或氨水接触时会降解。

8. 发明授权

US4283237A Method of making a gun propellant composition 失效
标题翻译：制作枪推进剂组合物的方法
公开(公告)号：US4283237A
公开(公告)日：1981-08-11
申请号：US565428
申请日：1975-04-03
申请人： Russell Reed, Jr. , Raymond M. Price
发明人： Russell Reed, Jr. , Raymond M. Price
IPC分类号： C06B21/00 , C06B45/10 , C08G18/48
CPC分类号： C06B21/0066 , C06B45/10 , C08G18/4837
摘要： HMX-containing gun propellants having good thermal stability and mechanical properties are made by mixing HMX with a polymerizable binder, a polyacrylate cross-linking agent and a polymerization catalyst and extruding the mixture into hot water to form cured pellets of propellant. The binder comprises a long chain acrylic monomer of 14 to 24 carbon atoms or a blend of such a long chain monomer and a shorter chain monomer having 6 to 13 carbon atoms. The molar ratio of short chain acrylic monomer to long chain monomer may vary from 0:1 to 3:1.
摘要翻译：通过将HMX与可聚合粘合剂，聚丙烯酸酯交联剂和聚合催化剂混合并将混合物挤出到热水中以形成固化的推进剂颗粒，制备具有良好热稳定性和机械性能的含HMX的枪推进剂。粘合剂包含14至24个碳原子的长链丙烯酸单体或这种长链单体和具有6至13个碳原子的较短链单体的共混物。短链丙烯酸单体与长链单体的摩尔比可以在0:1至3:1之间变化。

9. 发明授权

US4272480A Device for reducing the sensitivity of an ethylene oxide leak detector 失效
标题翻译：用于降低环氧乙烷泄漏检测器灵敏度的装置
公开(公告)号：US4272480A
公开(公告)日：1981-06-09
申请号：US124369
申请日：1980-02-25
申请人： Bertram O. Stull , Russell Reed, Jr.
发明人： Bertram O. Stull , Russell Reed, Jr.
IPC分类号： G01M3/20 , G01N31/22 , G01N33/00 , G01N21/01
CPC分类号： G01M3/20 , G01N31/224 , G01N33/0047
摘要： A device for monitoring for the presence of ethylene oxide gas comprising indicator which undergoes color change in the presence of ethylene oxide and a scrubber system to keep the device from being too sensitive. The scrubber system preferably employs activated charcoal coated with silicotungstic acid as the scrubber material.
摘要翻译：用于监测环氧乙烷气体存在的装置，包括在环氧乙烷和洗涤器系统存在下经历颜色变化的指示剂，以保持装置过于敏感。洗涤器系统优选使用涂覆有硅钨酸的活性炭作为洗涤器材料。

10. 发明授权

US4263070A Thermally stable gun and caseless cartridge propellants 失效
标题翻译：耐热稳定的枪和无内存的推进剂
公开(公告)号：US4263070A
公开(公告)日：1981-04-21
申请号：US449195
申请日：1974-03-05
申请人： Raymond M. Price , Russell Reed, Jr.
发明人： Raymond M. Price , Russell Reed, Jr.
IPC分类号： C06B25/34 , C06B45/10 , C08G18/48
CPC分类号： C08G18/4837 , C06B25/34 , C06B45/10
摘要： The water and oil resistance of caseless gun propellant compositions of the type which comprise cyclotetramethylenetetramine (HMX) as the high energy component and polyurethane as the binder are improved by preparing the binder by reaction of isocyanates with a hydroxyl-terminated block copolymer of ethylene oxide and propylene oxide or mixture of the block copolymer with other hydroxyl-terminated polyalkylene oxides. The block copolymer preferably contains from 40% to 60% by weight of ethylene oxide units and comprises at least 15% by weight of the binder.
摘要翻译：通过异氰酸酯与环氧乙烷的羟基封端的嵌段共聚物的反应制备粘合剂，改善了包含作为高能组分的环四亚甲基四胺（HMX）和聚氨酯作为粘合剂的无机枪推进剂组合物的耐水耐油性，环氧丙烷或嵌段共聚物与其它羟基封端的聚环氧烷的混合物。嵌段共聚物优选含有40重量％至60重量％的环氧乙烷单元，并且包含至少15重量％的粘合剂。

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