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1. 发明授权

US06262142B1 Translucent wear resistant dental enamel material and method 有权
标题翻译：半透明耐磨牙釉质材料及方法
公开(公告)号：US06262142B1
公开(公告)日：2001-07-17
申请号：US09351532
申请日：1999-07-12
申请人： Xiuling Wang , John C. Subelka , Steven R. Jefferies , Paul D. Hammesfahr , Paul A. Silver
发明人： Xiuling Wang , John C. Subelka , Steven R. Jefferies , Paul D. Hammesfahr , Paul A. Silver
IPC分类号： A61K608
CPC分类号： A61K6/083 , A61C2202/01 , C08L33/00
摘要： A method and material for forming translucent wear resistant dental enamel and the dental enamel material formed which has an opacity less than 50 percent and a localized wear volume loss of less than 0.025 mm3. The dental enamel material is formed from a polymerizable matrix and a filler. The material for forming translucent wear resistant dental enamel having an opacity less than 50 percent, a localized wear volume loss of less than 0.025 mm3 and a localized extended wear volume loss of less than 0.04 mm3, comprises a polymerizable matrix forming liquid and inorganic filler particles. The liquid comprises polymerizable material having a first refractive index. The filler comprising a first plurality of particles having a second refractive index. The first plurality of particles being formed from a low and a high median particle size plurality of particles. The low median particle size plurality of particles having a median particle size between 0.1 and 1.0 micrometers. The high median particle size plurality of particles having a median particle size between 1 and 10 micrometers. The first refractive index being within 5 percent of said second refractive index. More preferably the low median particle size plurality of particles have a median particle size between 0.3 and 0.7 micrometers, and said high median particle size plurality of particles have a median particle size between 1 and 2 micrometers. More preferably the filler further comprises a second plurality of filler particles having an average particle size of from about 0.01 to about 0.04 micrometers.
摘要翻译：形成半透明耐磨牙釉质和形成的牙釉质材料的方法和材料，其不透明度小于50％，局部磨损体积损失小于0.025mm 3。牙釉质材料由可聚合基质和填料形成。用于形成不透明度小于50％，局部磨损体积损失小于0.025mm 3和局部延长的磨损体积损失小于0.04mm 3的半透明耐磨牙釉质的材料包括形成可聚合基质的液体和无机填料颗粒。液体包括具有第一折射率的可聚合材料。填料包括具有第二折射率的第一多个颗粒。第一多个颗粒由低和高中值粒度的多个颗粒形成。中值粒径小的多个中等粒度的中值粒径在0.1和1.0微米之间。高中值粒度的多个颗粒具有1至10微米的中值粒度。第一折射率在所述第二折射率的5％以内。更优选地，低中值粒径的多个颗粒的中值粒径在0.3和0.7微米之间，并且所述高中值粒度的多个颗粒具有在1和2微米之间的中值粒度。更优选地，填料还包含平均粒度为约0.01至约0.04微米的第二多个填料颗粒。

2. 发明授权

US06353040B1 Dental composite restorative material and method of restoring a tooth 失效
标题翻译：牙齿复合修复材料及牙齿修复方法
公开(公告)号：US06353040B1
公开(公告)日：2002-03-05
申请号：US09136320
申请日：1998-07-06
申请人： John C. Subelka , Steven R. Jefferies , Donald A. Kapperman , Paul D. Hammesfahr , Paul A. Silver
发明人： John C. Subelka , Steven R. Jefferies , Donald A. Kapperman , Paul D. Hammesfahr , Paul A. Silver
IPC分类号： A61K6083
CPC分类号： A61K6/083 , A61C2202/01 , A61K6/0088 , A61K6/0091 , Y10T428/1352 , C08L33/00 , C08L23/00 , C08L25/04
摘要： A dental composite material includes a hardenable resin matrix and a filler component. The filler component includes (a) a first plurality of preferably glass particles having an average particle size of from about 1 to about 10 micrometers; (b) a second plurality of preferably glass particles having an average particle size of from about 0.1 to about 1 micrometers; and, (c) a plurality of filler particles having an average particle size of from about 0.01 to about 0.04 micrometers. A method according to the invention includes compacting a dental composite material into a prepared tooth cavity, wherein the material has a packability index above about 300 g/mm2.
摘要翻译：牙科复合材料包括可硬化树脂基质和填充剂组分。填料组分包括（a）平均粒度为约1至约10微米的第一多个优选玻璃颗粒; （b）平均粒径为约0.1至约1微米的第二多个优选玻璃颗粒; 和（c）平均粒径为约0.01至约0.04微米的多个填料颗粒。根据本发明的方法包括将牙科复合材料压实成制备的牙齿腔，其中所述材料的包装指数高于约300g / mm 2。

3. 发明授权

US4902560A Improving the physical properties of glass composite polydicyclopentadiene by heat treatment 失效
标题翻译：通过热处理提高玻璃复合聚二聚戊二烯的物理性能
公开(公告)号：US4902560A
公开(公告)日：1990-02-20
申请号：US200889
申请日：1988-06-01
申请人： Paul A. Silver
发明人： Paul A. Silver
IPC分类号： C08G61/08 , C08J5/04 , C08J5/24 , C08L65/00
CPC分类号： C08J5/043 , C08G61/08 , C08J2365/00 , Y10T428/24636 , Y10T428/31645 , Y10T442/2992
摘要： A method of preparing a glass fiber-reinforced, crosslinked polymer structure which comprises saturating an uncoated, unsized woven glass fabric with a polymerizable liquid comprised of dicyclopentadiene and, optionally, one or more other metathesis polymerizable strained ring polycyclic cycloolefins, subjecting said saturated fabric to polymerization conditions, and, thereafter, post-curing the resultant structure at a temperature greater than about 225.degree. C., and a glass fiber-reinforced, crosslinked polymer prepared by that process, are disclosed. Post-curing at temperatures greater than 225.degree. C. enhances the physical properties of the woven fiber-reinforced, crosslinked polymer.

4. 发明授权

US5710194A Dental compounds, compositions, products and methods 失效
公开(公告)号：US5710194A
公开(公告)日：1998-01-20
申请号：US603957
申请日：1996-02-15
申请人： Paul D. Hammesfahr , Kewang Lu , Paul A. Silver
发明人： Paul D. Hammesfahr , Kewang Lu , Paul A. Silver
IPC分类号： A61C5/06 , A61K6/00 , A61K6/083 , C07C69/54 , C07C69/92 , A61K6/08 , C07C322/00
CPC分类号： C07C69/92 , A61C5/064 , A61C5/066 , A61K6/0017 , A61K6/0023 , A61K6/083 , A61K6/0835
摘要： The invention provides polymerizable dental, compounds, compositions, including the compounds and products for mixing the compositions and methods of using the compositions. Aryl acid compounds are provided in accordance with the invention. The compositions include at least one polymerizable aryl acid compound, an effective amount of a polymerization initiator, and at least 10 percent by weight of ceramic, metal and/or metal oxide filler particles having a particle size less than 500 microns. The dental products of the invention include a polymerizable composition in an enclosure having at least two chambers separated by a wall adapted to be ruptured prior to or during mixing of the composition. Compositions of the invention are preferred for use in these enclosures. Core build up material including a polymerizable acid containing compound is used to support dental crowns and adhere them to teeth in accordance with the invention.

5. 发明授权

US06696507B2 Dental composite restorative material and method of restoring a tooth 有权
标题翻译：牙齿复合修复材料及牙齿修复方法
公开(公告)号：US06696507B2
公开(公告)日：2004-02-24
申请号：US10036881
申请日：2002-01-04
申请人： John C. Subelka , Steven R. Jefferies , Donald A. Kapperman , Paul D. Hammesfahr , Paul A. Silver
发明人： John C. Subelka , Steven R. Jefferies , Donald A. Kapperman , Paul D. Hammesfahr , Paul A. Silver
IPC分类号： A61C500
CPC分类号： A61K6/083 , A61C2202/01 , A61K6/0088 , A61K6/0091 , Y10T428/1352 , C08L33/00 , C08L23/00 , C08L25/04
摘要： A dental composite material includes a hardenable resin matrix and a filler component. The filler component includes (a) a first plurality of preferably glass particles having an average particle size of from about 1 to about 10 micrometers; (b) a second plurality of preferably glass particles having an average particle size of from about 0.1 to about 1 micrometers; and, (c) a plurality of filler particles having an average particle size of from about 0.01 to about 0.04 micrometers. A method according to the invention includes compacting a dental composite material into a prepared tooth cavity, wherein the material has a packability index above about 300 g/mm2.
摘要翻译：牙科复合材料包括可硬化树脂基质和填充剂组分。填料组分包括（a）平均粒度为约1至约10微米的第一多个优选玻璃颗粒; （b）平均粒径为约0.1至约1微米的第二多个优选玻璃颗粒; 和（c）平均粒径为约0.01至约0.04微米的多个填料颗粒。根据本发明的方法包括将牙科复合材料压实成制备的牙齿腔，其中所述材料的包装指数高于约300g / mm 2。

6. 发明授权

US5981620A Dental compounds, compositions, products and methods 失效
标题翻译：牙科化合物，组合物，产品和方法
公开(公告)号：US5981620A
公开(公告)日：1999-11-09
申请号：US953705
申请日：1997-10-17
申请人： Paul D. Hammesfahr , Kewang Lu , Paul A. Silver
发明人： Paul D. Hammesfahr , Kewang Lu , Paul A. Silver
IPC分类号： A61C5/06 , A61K6/00 , A61K6/083 , C07C69/54 , C07C69/92 , A61K6/08 , C07C322/00
CPC分类号： C07C69/92 , A61C5/064 , A61C5/066 , A61K6/0017 , A61K6/0023 , A61K6/083 , A61K6/0835
摘要： The invention provides polymerizable dental, compounds, compositions, including the compounds and products for mixing the compositions and methods of using the compositions. Aryl acid compounds are provided in accordance with the invention. The compositions include at least one polymerizable aryl acid compound, an effective amount of a polymerization initiator, and at least 10 percent by weight of ceramic, metal and/or metal oxide filler particles having a particle size less than 500 microns. The dental products of the invention include a polymerizable composition in an enclosure having at least two chambers separated by a wall adapted to be ruptured prior to or during mixing of the composition. Compositions of the invention are preferred for use in these enclosures. Core build up material including a polymerizable acid containing compound is used to support dental crowns and adhere them to teeth in accordance with the invention.
摘要翻译：本发明提供可聚合的牙科，化合物，组合物，包括用于混合组合物的化合物和产品以及使用该组合物的方法。根据本发明提供了芳酸化合物。组合物包括至少一种可聚合芳基化合物，有效量的聚合引发剂和至少10重量％的具有小于500微米的粒度的陶瓷，金属和/或金属氧化物填料颗粒。本发明的牙科产品包括在外壳中的可聚合组合物，其具有至少两个由适于在组合物混合之前或混合期间被破裂的壁隔开的腔室。本发明的组合物优选用于这些外壳。根据本发明，使用包含可聚合酸的化合物的核心堆积材料来支撑牙冠并将其粘附到牙齿上。

7. 发明授权

US5096644A Process for making a filled metathesis polymer article 失效
标题翻译：制备填充复分解聚合物制品的方法
公开(公告)号：US5096644A
公开(公告)日：1992-03-17
申请号：US370532
申请日：1989-06-23
申请人： Zenichiro Endo , Shigeyoshi Hara , Paul A. Silver , Hikoichiro Yamada
发明人： Zenichiro Endo , Shigeyoshi Hara , Paul A. Silver , Hikoichiro Yamada
IPC分类号： C08G61/08 , C08K9/06 , B29C45/14 , B29C45/16 , B32B31/00
CPC分类号： C08G61/08 , C08K9/06
摘要： A molded article is produced by metathesis polymerization of a mixture containing at least one metathesis polymerizable monomer, a metathesis polymerization catalyst and an organic or inorganic filler material which has been treated with a vinyl-substituted silane coupler having at least one hydrolyzable group in addition to the vinyl group.
摘要翻译：通过使含有至少一种易位可聚合单体，易位聚合催化剂和有机或无机填充材料的混合物的复分解聚合制备模制品，所述填充材料除了具有至少一个可水解基团的乙烯基取代的硅烷偶联剂乙烯基。

8. 发明授权

US5055499A Molded polymer article filled with inorganic material and production of said article 失效
标题翻译：填充无机材料的成型聚合物制品和所述制品的生产
公开(公告)号：US5055499A
公开(公告)日：1991-10-08
申请号：US461559
申请日：1990-01-05
申请人： Zenichiro Endo , Shigeyoshi Hara , Paul A. Silver , Hikoichiro Yamada
发明人： Zenichiro Endo , Shigeyoshi Hara , Paul A. Silver , Hikoichiro Yamada
IPC分类号： C08L65/00 , C08G61/08 , C08K9/06
CPC分类号： C08G61/08 , C08K9/06
摘要： A method is disclosed for preparing filled shaped articles of metathesis polymerized poly(cycloolefins) wherein an inorganic filler material is treated with a norbornene-substituted silane coupling agent. The norbornene moiety copolymerizes with the metathesis polymerizable monomer and the silane moiety creates a bond with the filler. Products are characterized by improved physical properties.
摘要翻译：公开了一种用于制备复分解聚合的聚（环烯烃）的填充成型制品的方法，其中用降冰片烯取代的硅烷偶联剂处理无机填料。降冰片烯部分与易位可聚合单体共聚，硅烷部分与填料形成结合。产品的特征在于物理性能的改善。

9. 发明授权

US4740537A Phosphorus based flame retardant composition for reaction injection molded polydicyclopentadiene 失效
标题翻译：用于反应注射聚二聚戊二烯的磷基阻燃组合物
公开(公告)号：US4740537A
公开(公告)日：1988-04-26
申请号：US861214
申请日：1986-05-09
申请人： Paul A. Silver
发明人： Paul A. Silver
IPC分类号： C09K21/14 , C08F2/44 , C08F32/00 , C08F32/06 , C08F32/08 , C08G61/06 , C08G61/08 , C08K3/06 , C08K3/22 , C08K3/28 , C08K5/02 , C08K5/03 , C08K5/17 , C08K9/08 , C08K9/10 , C08K13/02 , C08L45/00 , C08L61/10 , C08L65/00 , C08K3/02
CPC分类号： C08G61/08
摘要： Disclosed is a composition that is polymerizable by contacting it with an olefin metathesis catalyst comprising dicyclopentadiene, red phosphorus, and a brominated aromatic compound selected from the group consisting of decabromodiphenyl oxide, N,N'-ethylene-bis-(tetrabromophthalimide), brominated polystyrene, brominated polyphenylene oxide, tetradecabromodiphenoxy benzene, tetrabromoxylene, and octabromodiphenyl oxide.

10. 发明授权

US4731395A Polydicyclopentadiene having improved odor 失效
标题翻译：具有改善气味的聚二环戊二烯
公开(公告)号：US4731395A
公开(公告)日：1988-03-15
申请号：US863214
申请日：1986-05-14
申请人： Brian Byrne , Pierre I. Croquez , Barbara C. Gebbia , Paul A. Silver
发明人： Brian Byrne , Pierre I. Croquez , Barbara C. Gebbia , Paul A. Silver
IPC分类号： C08F2/44 , C08F4/78 , C08F32/00 , C08F32/08 , C08G61/06 , C08K5/00 , C08K5/04 , C08L45/00 , C08L65/00 , A61L9/01 , C08F132/08
CPC分类号： C08K5/0008 , C08G61/06 , C08L65/00
摘要： Poly(dicyclopentadiene) having improved odor is obtained by incorporating in at least one of the parts of the two part metathesis polymerization catalyst system from about 2 to about 500 ppm (based on the weight of dicyclopentadiene) of liquid deodorant such as cyclacet, cyclaprop, .beta.-damascenone, .beta.-damascone, rose oxide, terpene C, citronellyl methyl ether, citronellyl ethyl ether, geranyl methyl ether, geranyl ethyl ether, 2,6-dimethyloctyl methyl ether, 2,6-dimethyloctyl ethyl ether, .alpha.-terpenyl methyl ether, .alpha.-terpenyl ethyl ether, methyl salicylate, methyl octin carbonate, and 1,3,5-undecatriene.

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