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1. 发明授权

US4522725A Process for separating plasma albumin 失效
标题翻译：分离血浆白蛋白的方法
公开(公告)号：US4522725A
公开(公告)日：1985-06-11
申请号：US204717
申请日：1980-11-06
申请人： Kenji Koyama , Syotaro Ohno , Mitsutoshi Fukuda
发明人： Kenji Koyama , Syotaro Ohno , Mitsutoshi Fukuda
IPC分类号： C07K14/76 , A61K35/14 , A61K35/16 , A61K38/00 , A61K38/16 , C07K14/435 , C07K14/765 , B01D13/00
CPC分类号： C07K14/765 , B01D61/145 , B01D61/18 , B01D63/00 , A61K38/00
摘要： Plasma albumin is separated by a crude albumin fraction from blood plasma by a rough fractional separation and then separating plasma albumin through an ultrafiltration membrane. The ultrafiltration membrane is a membrane made of a polysulfone resin having the formula ##STR1## (n=50 to 250).
摘要翻译：血浆白蛋白通过粗略的分级分离由血浆中的粗白蛋白部分分离，然后通过超滤膜分离血浆白蛋白。超滤膜是由具有式（IMAGE）（n = 50〜250）的聚砜树脂制成的膜。

2. 发明授权

US5223376A Method for producing fine patterns utilizing specific polymeric diazonium salt, or diazonium salt/sulfone group containing polymer, as photobleachable agent 失效
标题翻译：使用特定的聚合重氮盐或含重氮盐/砜基的聚合物生产精细图案的方法，作为光可漂白剂
公开(公告)号：US5223376A
公开(公告)日：1993-06-29
申请号：US815885
申请日：1992-01-06
申请人： Masazumi Hasegawa , Masaaki Todoko , Mitsutoshi Fukuda
发明人： Masazumi Hasegawa , Masaaki Todoko , Mitsutoshi Fukuda
IPC分类号： G03F7/09
CPC分类号： G03F7/091
摘要： A method for producing fine patterns is disclosed, comprising spin-coating a photosensitive resin solution as an upper layer, which comprises a diazonium salt as a photobleachable agent, water and/or an organic solvent, and a polymer, on a photoresist layer as a lower layer and then light-exposing both the upper layer and the lower layer, wherein the polymer in the upper layer has a structural unit shown by formula (I): ##STR1## wherein R.sub.1, R.sub.2, and R.sub.3 each represents a hydrogen atom, an alkyl group having from 1 to 4 carbon atoms, a halogen atom, or a nitrile group; R.sub.4 represents a hydrogen atom, an alkyl group having from 1 to 4 carbon atoms, a halogen atom, a hydroxyl group, or a carboxyl group; and X represents a hydrogen atom, an alkali metal, an alkaline earth metal, or an ammonium group.According to another embodiment of this invention, a method for producing fine patterns is disclosed, comprising spin-coating a photosensitive resin solution as an upper layer, which comprises a diazonium salt as a photobleachable agent, water and/or an organic solvent, and a polymer, on a photoresist layer as a lower layer, wherein a counter anion of the diazonium salt is a functional group of the polymer in the photosensitive resin.According to this invention, a light of low contrast can be increased to one of high contrast without requiring complicated steps, and patterns of less than 1 .mu.m can be produced with good precision.
摘要翻译：公开了一种生产精细图案的方法，包括在作为上层的光致抗蚀剂层上旋涂作为上光层的感光性树脂溶液，其包含作为光可漂白剂的重氮盐，水和/或有机溶剂和聚合物，下层，然后对上层和下层进行曝光，其中上层中的聚合物具有式（I）所示的结构单元：其中R 1，R 2和R 3各自表示氢原子，具有1至4个碳原子的烷基，卤素原子或腈基; R4表示氢原子，具有1至4个碳原子的烷基，卤素原子，羟基或羧基; X表示氢原子，碱金属，碱土金属或铵基。根据本发明的另一个实施方案，公开了一种制造精细图案的方法，其包括旋涂作为上层的感光性树脂溶液，其包含重氮盐作为光漂白剂，水和/或有机溶剂，以及聚合物，作为下层的光致抗蚀剂层，其中重氮盐的抗衡阴离子是感光性树脂中的聚合物的官能团。根据本发明，可以将低对比度的光增加到高对比度之一而不需要复杂的步骤，并且可以以高精度产生小于1μm的图案。

3. 发明授权

US4690887A Method for forming micro-patterns by development 失效
标题翻译：通过开发形成微观图案的方法
公开(公告)号：US4690887A
公开(公告)日：1987-09-01
申请号：US800100
申请日：1985-11-22
申请人： Mitsutoshi Fukuda , Makoto Fukutomi , Osamu Kogure , Kazunori Miyoshi
发明人： Mitsutoshi Fukuda , Makoto Fukutomi , Osamu Kogure , Kazunori Miyoshi
IPC分类号： G03F7/26 , G03F7/016 , G03F7/038 , G03F7/32 , G03C5/00
CPC分类号： G03F7/038 , G03F7/325
摘要： Disclosed is a method for forming micro-patterns on base plates such as for semiconductor integrated circuits, particularly by development, wherein a radiation sensitive negative resist film is formed on the base plate and irradiated according to pattern designs, and the non-irradiated portions of the film is dissolved by a liquid developer comprising a mixture of a good solvent selected from the group of alkyl esters of acetic acid, having an alkyl group containing 1 to 5 carbon atoms, and a poor solvent selected from the group consisting of alicyclic compounds and alkyl ethers of ethyleneglycol having an alkyl group containing 1 to 5 carbon atoms. The method can minimize swelling of irradiated portions of the resist film and can accelerate dissolution of non-irradiated portions of the resist film, so that desired micro-patterns with excellent edge shape quality can be obtained.
摘要翻译：公开了一种在半导体集成电路，特别是用于半导体集成电路的基板上形成微图形的方法，其中在基板上形成辐射敏感的负型抗蚀剂膜并根据图案设计照射，并且未照射部分该膜由液体显影剂溶解，该液体显影剂包括选自乙酸的烷基酯，具有1至5个碳原子的烷基的良溶剂和选自脂环族化合物和具有1〜5个碳原子的烷基的乙二醇的烷基醚。该方法可以使抗蚀剂膜的照射部分的溶胀最小化，并且可以加速抗蚀剂膜的未照射部分的溶解，从而可以获得具有优异的边缘形状质量的期望的微图案。

4. 发明授权

US4515886A Photosensitive compositions 失效
标题翻译：感光组合物
公开(公告)号：US4515886A
公开(公告)日：1985-05-07
申请号：US579872
申请日：1984-02-13
申请人： Tsuguo Yamaoka , Mitsutoshi Fukuda
发明人： Tsuguo Yamaoka , Mitsutoshi Fukuda
IPC分类号： G03F7/038 , G03C1/71 , G03C1/72
CPC分类号： G03F7/038 , Y10S430/12 , Y10S430/121 , Y10S430/124 , Y10S430/127 , Y10S522/904
摘要： Photosensitive compositions useful as resists for transistors, ICs, etc. comprising a solution of a photosensitive high polymer of a polymer or a copolymer which contains a unit expressed by the following general formula: ##STR1## (where X.sub.1 is an atom of hydrogen or halogen, a halogenated alkyl group of 1 to 4 carbon atoms or an alkyl group having 1 to 4 carbon atoms, X.sub.2 is a halogen atom or a halogenated alkyl group having 1 to 4 carbon atoms and R is an aromatic ring or a heterocyclic ring), and a photosensitizing agent dissolved in organic solvents. The photosensitive compositions show marked improvement in photosensitivity and gamma value.
摘要翻译：用作晶体管，IC等的抗蚀剂的光敏性组合物，其包含聚合物或共聚物的感光性高分子的溶液，所述聚合物或共聚物含有由以下通式表示的单元：其中X1是氢原子或卤素，1〜4个碳原子的卤代烷基或碳原子数1〜4的烷基，X 2为卤素原子或碳原子数1〜4的卤代烷基，R为芳香环或杂环）和溶于有机溶剂的光敏剂。光敏组合物在光敏性和γ值方面显示出显着的改善。

5. 发明授权

US4420257A Laser light scattering photometer 失效
标题翻译：激光散射光度计
公开(公告)号：US4420257A
公开(公告)日：1983-12-13
申请号：US121314
申请日：1980-02-14
申请人： Mitsutoshi Fukuda , Nobuyuki Baba , Kenji Arichika
发明人： Mitsutoshi Fukuda , Nobuyuki Baba , Kenji Arichika
IPC分类号： G01N21/53 , G01N21/00
CPC分类号： G01N21/532
摘要： A laser light beam is projected through a fluid measuring cell having a fluid accommodating chamber and inlet and outlet pathways for the fluid. The light is separated into transmitted light and scattered light. Separate light detectors sense the transmitted light and scattered light. An electric control circuit uses the variations of the intensity of the transmitted light to compensate for fluctuations in the intensity of the scattered light to provide an output related to the intensity of the scattered light.
摘要翻译：激光束通过具有流体容纳室的流体测量池和用于流体的入口和出口路径投射。光被分离成透射光和散射光。独立的光检测器感测透射光和散射光。电气控制电路使用透射光的强度的变化来补偿散射光的强度的波动，以提供与散射光的强度相关的输出。

6. 发明授权

US4333870A Process for separating .gamma.-globulin aggregate by polysulfone membrane 失效
标题翻译：通过聚砜膜分离γ-球蛋白骨架的方法
公开(公告)号：US4333870A
公开(公告)日：1982-06-08
申请号：US188118
申请日：1980-09-17
申请人： Kenji Koyama , Syotaro Ohno , Mitsutoshi Fukuda
发明人： Kenji Koyama , Syotaro Ohno , Mitsutoshi Fukuda
IPC分类号： C07K16/00 , A61K38/16 , A61K38/21 , A61K39/395 , B01D61/14 , B01D61/16 , C07K14/435 , C07K16/06 , C07G7/00
CPC分类号： C07K16/06
摘要： .gamma.-Globulin aggregate is separated by a membrane from an aqueous solution of .gamma.-globulin through an ultrafiltration membrane. The ultrafiltration membrane is a membrane made of a polysulfone resin having the formula ##STR1##
摘要翻译： γ-球蛋白聚集体通过膜通过超滤膜从γ-球蛋白水溶液中分离。超滤膜是由具有式 + TR 的聚砜树脂制成的膜

7. 发明授权

US4347138A Method of separating serum albumin and gamma-globulin from each other 失效
标题翻译：血清白蛋白和γ-球蛋白相互分离的方法
公开(公告)号：US4347138A
公开(公告)日：1982-08-31
申请号：US212746
申请日：1980-12-03
申请人： Shotaro Ohno , Kenji Koyama , Mitsutoshi Fukuda
发明人： Shotaro Ohno , Kenji Koyama , Mitsutoshi Fukuda
IPC分类号： C07K14/435 , A61K38/00 , A61K38/16 , A61K38/21 , A61K39/395 , B01D61/14 , B01D61/16 , C07K1/34 , C07K14/76 , C07K14/765 , C07K16/00 , C07K16/06 , B01D13/00
CPC分类号： C07K14/765 , C07K16/065 , A61K38/00
摘要： Serum albumin and a serum .gamma.-globulin are separated by filtration from each other in a solution of a mixture thereof by using an ultrafiltration membrane. The ultrafiltration membrane has a fractionation molecular weight of about 100,000. The total protein concentration and salt concentration in the mixture solution to be forced through the membrane are adjusted to not more than 4 g/dl and not more than 0.6 mole/l, respectively. Also, the pH of the solution is adjusted to a value of from about 3.8 to about 4.7.
摘要翻译：通过使用超滤膜在其混合物的溶液中通过过滤彼此分离血清白蛋白和血清γ-球蛋白。超滤膜的分馏分子量约为100,000。要强制通过膜的混合溶液中的总蛋白质浓度和盐浓度分别调节至不超过4g / dl且不大于0.6mol / l。此外，将溶液的pH调节至约3.8至约4.7的值。

8. 发明授权

US4252925A Anionic polymerization process 失效
标题翻译：阴离子聚合工艺
公开(公告)号：US4252925A
公开(公告)日：1981-02-24
申请号：US18748
申请日：1979-03-08
申请人： Mitsutoshi Fukuda , Kazuo Tago , Akihiko Shimizu
发明人： Mitsutoshi Fukuda , Kazuo Tago , Akihiko Shimizu
IPC分类号： C08G65/00 , C08F2/00 , C08F2/04 , C08F4/46 , C08F4/50 , C08G65/02 , C08G65/12 , C08G75/08 , C08F4/48
CPC分类号： C08G65/12 , C08F4/46 , C08F4/50 , C08G75/08
摘要： An anionic polymerization is carried out by polymerizing a monomer for anionic polymerization in a solvent in the presence of a polymerization initiator after preparing a polymerization system by an operation (I) adding a solution of an organometallic compound in a polymerization system of a solvent or a combination of a solvent and an inert gas and an operation (II) removing excess of the unreacted organometallic compound, before charging the monomer and the polymerization initiator.
摘要翻译：阴离子聚合通过在制备聚合体系之后在聚合引发剂存在下在溶剂中聚合用于阴离子聚合的单体进行阴离子聚合，操作（I）在溶剂的聚合体系中加入有机金属化合物的溶液或溶剂和惰性气体的组合以及在将单体和聚合引发剂加料之前，除去过量的未反应的有机金属化合物的操作（II）。

9. 发明授权

US5139922A Method of making resist pattern 失效
标题翻译：抗蚀剂图案制作方法
公开(公告)号：US5139922A
公开(公告)日：1992-08-18
申请号：US602930
申请日：1990-10-25
申请人： Hisashi Watanabe , Yoshihiro Todokoro , Masazumi Hasegawa , Mitsutoshi Fukuda
发明人： Hisashi Watanabe , Yoshihiro Todokoro , Masazumi Hasegawa , Mitsutoshi Fukuda
IPC分类号： G03F7/09 , G03F7/20
CPC分类号： G03F7/7045 , G03F7/094 , Y10S430/143
摘要： A thin film of conductive high molecular compound is formed on a substrate such as Si followed by a heat treatment, and thereafter an electron beam exposure and subsequent development are made, to form pattern of the thin film of conductive high molecular compound; this method can eliminate forming of metal film to prevent the electron charge, can prevent charging of resist in electron-beam exposure or further prevent proximity effect when combined with deep ultraviolet light exposure.
摘要翻译：在Si等基板上形成导电性高分子化合物的薄膜，进行热处理，然后进行电子束曝光和随后的显影，形成导电性高分子化合物的薄膜的图案。该方法可以消除金属膜的形成以防止电子电荷，可以防止电子束曝光中的抗蚀剂充电，或进一步防止与深紫外光照射结合时的接近效应。

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