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1. 发明授权

US5055248A Process for producing stretched article of ultrahigh-molecular weight polyethylene 失效
标题翻译：生产超分子重量聚乙烯的拉伸制品的方法
公开(公告)号：US5055248A
公开(公告)日：1991-10-08
申请号：US423592
申请日：1989-10-16
申请人： Masanori Motooka , Hotishi Mantoku , Kazuo Yagi , Hiroyuki Takeda , Kazuyuki Takimoto
发明人： Masanori Motooka , Hotishi Mantoku , Kazuo Yagi , Hiroyuki Takeda , Kazuyuki Takimoto
IPC分类号： B29C47/00 , B29C55/00 , C08J5/18 , C08K5/00 , C08L23/06 , D01F6/04
CPC分类号： C08J5/18 , B29C47/0004 , C08K5/0016 , D01F6/04 , B29C47/0014 , B29C47/0021 , B29C47/0057 , B29C55/00 , B29K2023/00 , B29L2007/008 , B29L2031/731 , C08J2323/06
摘要： Stretched articles of ultrahigh-molecular-weight polyethylene are prepared by melt-kneading a mixture of ultrahigh-molecular-weight polyethylene with an aliphatic compound (b.sub.1) of at least 8 carbon atoms having a melting point of at least 10.degree. C. and a boiling point of at least 130.degree. C. in a screw extruder while maintaining the mixture at a temperature from the melting point of the mixture to 300.degree. C. The molten mixture is melt-extruded through a die at a temperature from the melting point of the mixture to 300.degree. C. and the resulting unstretched extrudate is cooled to solidify it. The unstretched solidified extrudate is then subjected to a stretching treatment at a temperature of the melting point of the aliphatic compound (b.sub.1) to a point 20.degree. C. above the melting point of the mixture at a particular stretch ratio.
摘要翻译：通过将超高分子量聚乙烯与熔点至少为10℃的至少8个碳原子的脂肪族化合物（b1）熔融捏合而制备超高分子量聚乙烯的拉伸制品，在螺杆挤出机中沸点至少为130℃，同时将混合物保持在从该混合物的熔点到300℃的温度。熔融混合物通过模头在从熔点将混合物至300℃并将所得未拉伸挤出物冷却固化。然后将未拉伸固化的挤出物在脂肪族化合物（b1）的熔点温度下以比特定拉伸比的混合物熔点高20℃的温度进行拉伸处理。

2. 发明授权

US4942087A Films of wholly aromatic polyester and processes for preparation thereof 失效
标题翻译：全芳族聚酯薄膜及其制备方法
公开(公告)号：US4942087A
公开(公告)日：1990-07-17
申请号：US285015
申请日：1988-12-16
申请人： Masanori Motooka , Kazuyuki Takimoto , Kunisuke Fukui
发明人： Masanori Motooka , Kazuyuki Takimoto , Kunisuke Fukui
IPC分类号： C08G63/60 , C08J5/18 , C08G63/02 , B32B27/36 , C08G69/08
CPC分类号： C08J5/18 , C08G63/605 , C08J2367/00 , Y10T428/26 , Y10T428/31786
摘要： Disclosed herein are (1) a film of a liquid crystalline wholly aromatic polyester which is non-oriented and transparent, which film can be prepared by dissolving a liquid crystalline wholly aromatic polyester in a solvent, casting the resulting solution to form a film and volatirizing the solvent from the film as cast and (2) a film of a liquid crystalline wholly aromatic polyester which is oriented and polarizing, which film can be prepared by orienting the above-mentioned non-oriented film by drawing or heating.

3. 发明授权

US4764583A Melt-moldable wholly aromatic polyester 失效
标题翻译：可熔融的全芳族聚酯
公开(公告)号：US4764583A
公开(公告)日：1988-08-16
申请号：US24087
申请日：1987-03-10
申请人： Kunisuke Fukui , Masanori Motooka
发明人： Kunisuke Fukui , Masanori Motooka
IPC分类号： C08G63/60 , C08G63/66
CPC分类号： C08G63/605
摘要： A melt-moldable wholly aromatic polyester comprising (A) aromatic hydroxycarboxylic acid residues, (B) aromatic diol residues, (C) 4,4'-dihydroxydiphenyl ether residues represented by the following formula ##STR1## and (D) aromatic dicarboxylic acid residues, and a melt-moldable wholly aromatic polyester comprising (A) aromatic hydroxycarboxylic acid residues, (C)' aromatic diol residues represented by the following formula--O--Ar.sup.4 --O--wherein Ar.sup.4 represents a group at least 60 mole % of which consists of a group of the following formula (a) ##STR2## or a group of the formula (a) and a group of the following formula (b) ##STR3## and (D) aromatic dicarboxylic acid residues.
摘要翻译：包含（A）芳族羟基羧酸残基的可熔融模制的全芳族聚酯，（B）芳族二醇残基，（C）由下式表示的4,4'-二羟基二苯基醚残基和（D）芳族二羧酸残基和可熔融成型的全芳族聚酯，其包含（A）芳族羟基羧酸残基，（C）由下式-O- Ar 4 -O-表示的芳族二醇残基，其中Ar 4表示至少60摩尔％的基团（a）或式（a）的基团和下述式（b）的基团和（D）芳族二羧酸残基组成的组。

4. 发明授权

US4616059A Graft-modified ultrahigh-molecular-weight polyethylene and process for producing same 失效
标题翻译：接枝改性的超高分子量聚乙烯及其制备方法
公开(公告)号：US4616059A
公开(公告)日：1986-10-07
申请号：US770058
申请日：1985-08-28
申请人： Masanori Motooka , Hitoshi Mantoku
发明人： Masanori Motooka , Hitoshi Mantoku
IPC分类号： C08F8/00 , B29C55/00 , B29K23/00 , C08F8/46 , C08F255/00 , C08F255/02 , D01F6/04 , D01F6/46 , D02J1/22 , C08K5/01
CPC分类号： C08F255/02
摘要： A graft-modified ultrahigh-molecular-weight polyethylene obtained by grafting (A) an ultrahigh-molecular-weight polyethylene having an inherent viscosity [.eta.], determined at 135.degree. C. in decalin, of at least 5 dl/g with (C) an unsaturated carboxylic acid graft-copolymerizable therewith or its graft-copolymerizable derivative, under melt-kneading condition in the presence of (B) an aliphatic compound having a melting point, determined by the DSC method, of at least 10.degree. C. and a boiling point of at least 130.degree. C., an amount of the component (C) grafted in said graft-modified ultrahigh-molecular-weight polyethylene being 0.01 to 10% by weight, and said graft-modified ultrahigh-molecular-weight polyethylene being substantially free of an insoluble gel product and having a tensile strength of at least 1.0 GPa; and a process for producing the same.
摘要翻译：接枝改性的超高分子量聚乙烯通过将（A）在十氢萘中在135℃下测定的特性粘度η至少为5dl / g的超高分子量聚乙烯（A）与（C ）可接枝共聚的不饱和羧酸或其接枝可共聚的衍生物，在熔融捏合条件下，在（B）通过DSC方法测定的熔点的脂族化合物存在下至少10℃，和沸点至少为130℃，接枝在所述接枝改性的超高分子量聚乙烯中的成分（C）的量为0.01〜10重量％，所述接枝改性的超高分子量聚乙烯基本上不含不溶性凝胶产品并具有至少1.0GPa的拉伸强度; 及其制造方法。

5. 发明授权

US06190153B1 Oriented film producing facility with thickness and orientation control means 失效
标题翻译：面向薄膜生产设备，具有厚度和方向控制手段
公开(公告)号：US06190153B1
公开(公告)日：2001-02-20
申请号：US09069732
申请日：1998-04-30
申请人： Koji Tsuzukiyama , Masanori Motooka , Toshiyuki Fujiwara , Michio Toriumi
发明人： Koji Tsuzukiyama , Masanori Motooka , Toshiyuki Fujiwara , Michio Toriumi
IPC分类号： B29C4358
CPC分类号： G01N21/23 , B29C47/0021 , B29C47/92 , B29C55/143 , B29C2037/90 , B29C2947/92152 , B29C2947/92438 , B29C2947/9259 , B29C2947/92647 , B29C2947/92704 , B29C2947/92885 , B29C2947/92904 , B29C2947/92933
摘要： A drawing system in which a thickness and degree of orientation of an oriented film or the like is maintained in a uniform manner under a condition of a high speed, shortened is a time required from a time when a molding material is charged in an extruder and drawing started until a time when a film is taken up on a take-up apparatus, and a high quality film or the like is produced at a high speed and besides, a probability for a not-oriented or oriented film or the like to be broken down during drawing is reduced. A thickness and degree of orientation of a film are independently measured in thickness gauges and a film orientation measuring apparatus in a continuous manner after longitudinal drawing or lateral drawing and measured values are input to a computer. The computer input with the measured values respectively compares preset target values with the measured thickness and degree of orientation and a control operation to change a longitudinal draw ratio is conducted if the measured values are different from respective preset values based on results of comparison processing.
摘要翻译：在高速的条件下，定向膜等的厚度和取向度被均匀地保持的拉制系统是缩短成型材料在挤出机中被填充的时间所需要的时间，绘画开始直到在卷取装置上卷取胶卷的时候，高速生产高质量的胶卷等，另外，不定向或定向胶片等的概率为绘图过程中细分下降。在纵向拉伸或横向拉伸之后，以厚度计和薄膜取向测量装置独立地测量薄膜的厚度和取向度，并将测量值输入计算机。如果基于比较处理的结果，如果测量值与各个预设值不同，则具有测量值的计算机输入分别将预设目标值与测量的厚度和取向度进行比较，并且进行改变纵向拉伸比的控制操作。

6. 发明授权

US4612148A Process for producing stretched articles of ultrahigh-molecular-weight polyethylene 失效
标题翻译：用于生产超高分子量聚乙烯拉伸制品的方法
公开(公告)号：US4612148A
公开(公告)日：1986-09-16
申请号：US755590
申请日：1985-07-16
申请人： Masanori Motooka , Hitoshi Mantoku , Takao Ohno
发明人： Masanori Motooka , Hitoshi Mantoku , Takao Ohno
IPC分类号： B29C47/00 , B29C47/86 , B29C55/00 , C08J5/18 , C08L23/06 , D01F6/46 , D01F1/10 , D01D5/088
CPC分类号： C08J5/18 , B29C47/0004 , B29C47/0014 , B29C47/0021 , B29C47/802 , B29C47/86 , B29C47/862 , B29C47/8805 , B29C47/8895 , C08F255/02 , C08L23/06 , D01F6/46 , B29C47/0057 , B29C47/02 , B29C55/00 , B29K2023/06 , B29K2023/0683 , B29K2995/0088 , B29L2007/008 , C08J2323/06
摘要： Stretched articles of ultrahigh-molecular-weight polyethylene are prepared by melt-kneading a mixture of ultrahigh-molecular-weight polyethylene with a paraffinic wax having a melting point of 40.degree. to 120.degree. C. and a weight average molecular weight of at least 230 but less than 2000 in a screw extruder while maintaining the temperature of the mixture at 180.degree. to 280.degree. C. The molten mixture is melt-extruded through a die at a temperature of 180.degree. to 300.degree. C. under a draft condition of a draft ratio of less than 2 or in the absence of a draft and the resulting unstretched extrudate is cooled to solidify it. The unstretched solidified extrudate is than subjected to a stretching treatment in a heated liquid medium which is a solvent for the paraffinic wax at a temperature of 60.degree. to 140.degree. C. at a particular stretch ratio. Stretch shaped articles of ultrahigh-molecular-weight polyethylene having high tensile strength and modulus of elasticity are produced uniformly and reproducibly. The stretched shaped articles are substantially free from stretching uneveness. Examples of the paraffinic wax include n-alkanes having at least 22 carbon atoms.

7. 发明授权

US4545950A Process for producing stretched articles of ultrahigh-molecular-weight polyethylene 失效
标题翻译：用于生产超高分子量聚乙烯拉伸制品的方法
公开(公告)号：US4545950A
公开(公告)日：1985-10-08
申请号：US566302
申请日：1983-12-28
申请人： Masanori Motooka , Hitoshi Mantoku , Takao Ohno
发明人： Masanori Motooka , Hitoshi Mantoku , Takao Ohno
IPC分类号： B29C47/00 , B29C47/86 , B29C55/00 , C08J5/18 , C08L23/06 , D01F6/46 , D01F1/10 , D01D5/092
CPC分类号： C08J5/18 , B29C47/0004 , B29C47/0014 , B29C47/0021 , B29C47/802 , B29C47/86 , B29C47/862 , B29C47/8805 , B29C47/8895 , C08F255/02 , C08L23/06 , D01F6/46 , B29C47/0057 , B29C47/02 , B29C55/00 , B29K2023/06 , B29K2023/0683 , B29K2995/0088 , B29L2007/008 , C08J2323/06
摘要： Stretched articles of ultrahigh-molecular-weight polyethylene are prepared by melt-kneading a mixture of ultrahigh-molecular-weight polyethylene with a paraffinic wax having a melting point of 40.degree. to 120.degree. C. and a weight average molecular weight of at least 230 but less than 2000 in a screw extruder while maintaining the temperature of the mixture at 180.degree. to 280.degree. C. The molten mixture is melt-extruded through a die at a temperature of 180.degree. to 300.degree. C. and the resulting unstretched extrudate is cooled to solidify it. The unstretched solidified extrudate is then subjected to a stretching treatment at a temperature of 60.degree. to 140.degree. C. at a particular stretch ratio. Stretch shaped articles of ultrahigh-molecular-weight polyethylene having high tensile strength and modulus of elasticity are produced uniformly and reproducibly. The stretched shaped articles are substantially free from stretching uneveness. Examples of the paraffinic wax include n-alkanes having at least 22 carbon atoms.
摘要翻译：超高分子量聚乙烯的拉伸制品通过将超高分子量聚乙烯与熔点为40〜120℃，重均分子量为230以上的链烷烃蜡的混合物熔融混炼，但在螺杆挤出机中小于2000，同时将混合物的温度保持在180℃至280℃。熔融混合物在180℃至300℃的温度下通过模具熔融挤出，并将得到的未拉伸挤出物冷却固化。然后将未拉伸固化的挤出物以特定的拉伸比在60至140℃的温度下进行拉伸处理。均匀且可再现地制造具有高拉伸强度和弹性模量的超高分子量聚乙烯的拉伸成型制品。拉伸的成形制品基本上没有拉伸不均匀。链烷烃蜡的实例包括具有至少22个碳原子的正烷烃。

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