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1. 发明授权

US4115459A Preparation of fluorotrinitromethane 失效
标题翻译：氟硝基甲烷的制备
公开(公告)号：US4115459A
公开(公告)日：1978-09-19
申请号：US513630
申请日：1974-10-09
申请人： Louis R. Grant, Jr.
发明人： Louis R. Grant, Jr.
IPC分类号： C07C205/08 , C07C79/12
CPC分类号： C07C201/12
摘要： Fluorotrinitromethane is synthesized by reacting tetranitromethane with an adduct of an alkali metal fluoride and a fluorinated or chlorofluorinated acetone in an aprotic dipolar solvent.
摘要翻译：氟化硝基甲烷是通过在非质子偶极溶剂中使四硝基甲烷与碱金属氟化物和氟化或氯氟化丙酮的加合物反应而合成的。

2. 发明授权

US3484315A Reaction products of alane terminated beryllium hydride with b2h6,be(bh4)2 or b4h10 失效
标题翻译：具有B2H6，BE（BH4）2或B4H10的ALANE终止的BALLLIUM HYDRIDE的反应产物
公开(公告)号：US3484315A
公开(公告)日：1969-12-16
申请号：US3484315D
申请日：1967-12-07
申请人： ROSS I WAGNER , LOUIS R GRANT JR , FRANK C GUNDERLOY JR
发明人： WAGNER ROSS I , GRANT LOUIS R JR , GUNDERLOY FRANK C JR
IPC分类号： C06B47/10 , C07F5/02 , C07F5/06 , C06D5/08
CPC分类号： C07F5/066 , C06B47/10 , C07F5/027

3. 发明授权

US4673528A Solid H.sub.2 /D.sub.2 gas generators 失效
标题翻译：固体H2 / D2气体发生器
公开(公告)号：US4673528A
公开(公告)日：1987-06-16
申请号：US781820
申请日：1985-09-30
申请人： Glen D. Artz , Louis R. Grant
发明人： Glen D. Artz , Louis R. Grant
IPC分类号： C01B3/04 , C01B4/00 , C06D5/00 , C06B27/00
CPC分类号： C01B3/04 , C01B4/00 , C06D5/00 , Y02E60/364
摘要： A solid fuel for generating H.sub.2 or D.sub.2 gases, comprising magnesiumorohydride diammoniate (MBDA) or its deuterated analog as the H.sub.2 or D.sub.2 source, an oxidizer selected from LiNO.sub.3 and KNO.sub.3, and a binder of polytetrafluoroethylene is a thermally stable gas generator composition which yields greater than 12.5 weight percent H.sub.2 or D.sub.2. The MBDA weight percentages by weight ranges from 80-90, the oxidizer ranges from 5-15, and the binder ranges from 2-15.
摘要翻译：用于产生H 2或D 2气体的固体燃料包括硼氢化二铵（MBDA）或其作为H 2或D 2源的氘代类似物，选自LiNO 3和KNO 3的氧化剂和聚四氟乙烯的粘合剂的热稳定性气体发生剂组合物，其产生大于12.5重量％的H2或D2。 MBDA重量百分比重量范围为80-90，氧化剂范围为5-15，粘合剂的范围为2-15。

4. 发明授权

US4604271A Magnesium borohydride diammoniate and triammoniate 失效
标题翻译：硼氢化镁二铵和三铵
公开(公告)号：US4604271A
公开(公告)日：1986-08-05
申请号：US781819
申请日：1985-09-30
申请人： Ross I. Wagner , Louis R. Grant
发明人： Ross I. Wagner , Louis R. Grant
IPC分类号： C01B6/13 , C01B35/00
CPC分类号： C01B6/13
摘要： A direct low temperature process for the preparation of pure magnesium borohydride diammoniate or the deuterated analog thereof based on the addition of 90-95% of the stoichiometric amount of NH.sub.3 to an excess of Mg(BH.sub.4).sub.2.X(C.sub.2 H.sub.5).sub.2 O in a benzene reaction solvent in accordance with equation 1: ##STR1## wherein X is a numeral from about 2.0 to about 2.5; or when the reaction is conducted in an ether reaction solvent with the same quantities of reactants and under the same experimental conditions, the triammoniate or the deuterated analog thereof is formed in accordance with equation 2: ##STR2## wherein X is a numeral from about 2.0 to about 2.5. In either case the pure product is readily isolated by filtration, solvent washing to remove excess Mg(BH.sub.4).sub.2.X(C.sub.2 H.sub.5).sub.2 O, and vacuum drying at ambient temperature. Yields are 95-99%; purities are typically about 97%.
摘要翻译：基于在过量的Mg（BH 4）2 X（C 2 H 5）2 O中添加90-95％化学计量的NH 3与过量的Mg（BH 4）2 X（C 2 H 5）2 O）相比，制备纯的硼氢化镁二铵或其氘代类似物的直接低温方法苯反应溶剂按照方程式1： + TR Mg（BH4）2.2NH3 + X（C2H5）2O，其中X为约2.0至约2.5的数值; 或者当反应在具有相同量的反应物的醚反应溶剂中进行时，并且在相同的实验条件下进行，根据等式2形成三胺或其氘化的类似物： Mg（BH4）2.3NH3 + X（C 2 H 5）2 O，其中X为约2.0至约2.5的数字。在任一情况下，通过过滤容易地分离纯产物，用溶剂洗涤以除去过量的Mg（BH4）2.X（C2H5）2O，并在环境温度下真空干燥。产量为95-99％; 纯度通常约为97％。

5. 发明授权

US4472214A Triaminoguanidinium phosphate propellant additive 失效
标题翻译：三氨基胍磷酸盐推进剂添加剂
公开(公告)号：US4472214A
公开(公告)日：1984-09-18
申请号：US530325
申请日：1983-09-08
申请人： Joseph E. Flanagan , Louis R. Grant
发明人： Joseph E. Flanagan , Louis R. Grant
IPC分类号： C06B23/00 , C06B45/10
CPC分类号： C06B23/005
摘要： Triaminoguanidinium phosphate is used to improve the performance and flammability characteristics of low vulnerability propellants.
摘要翻译：三氨基胍磷酸盐用于改善低脆弱性推进剂的性能和可燃性。

6. 发明授权

US4937361A Glycidyl azide polymer and method of preparation 失效
标题翻译：缩水甘油基叠氮化物聚合物及其制备方法
公开(公告)号：US4937361A
公开(公告)日：1990-06-26
申请号：US305033
申请日：1989-02-02
申请人： Ross I. Wagner , Edgar R. Wilson , Louis R. Grant , Joseph E. Flanagan
发明人： Ross I. Wagner , Edgar R. Wilson , Louis R. Grant , Joseph E. Flanagan
IPC分类号： C08G65/24 , C08G65/32 , C08G65/325
CPC分类号： C08G65/325
摘要： A method of producing a hydroxy-terminated aliphatic polyether utilizing a specific catalytic interaction to enhance the solubility and resulting reactivity of an azide moiety.

7. 发明授权

US4381206A Advanced solid reactants for H.sub.2 /D.sub.2 generation 失效
标题翻译：用于H2 / D2生成的高级固体反应物
公开(公告)号：US4381206A
公开(公告)日：1983-04-26
申请号：US285163
申请日：1981-07-20
申请人： Louis R. Grant , Joseph E. Flanagan
发明人： Louis R. Grant , Joseph E. Flanagan
IPC分类号： C06D5/04 , H01S3/095 , H05H1/22 , C06B43/00
CPC分类号： G21B1/19 , C06D5/04 , H01S3/095 , Y02E30/16
摘要： Disclosed is an all amine borane gas generating system which consists of razine bis-borane or its deuterated derivative in the form of a compacted solid propellant pellet which serves as the thermal stimulus for the decomposition of itself. An all amine borane gas generating system which additionally consists of diborane diammoniate or its deuterated derivative provides a higher yield of hydrogen or deuterium with a higher purity from a self-sustaining reaction after the self-sustaining reaction is initiated by a heat source (e.g., an electrically heated nichrome wire) sufficient to initiate the reaction. This all amine borane gas generating system which consists of N.sub.2 H.sub.4.2BH.sub.3 and H.sub.2 B(NH.sub.3).sub.2 BH.sub.4 is in the form of a compacted solid propellant pellet. The pellets are formed to the desired configuration employing pressures from about 500 to about 10,000 pounds total load. The solid propellant pellets are useful as a H.sub.2 or D.sub.2 generation sources for fuels for lasers.
摘要翻译：公开了一种全胺胺体气体发生系统，其由作为其自身分解的热刺激的压实固体推进剂丸粒形式的肼双 - 硼烷或其氘代衍生物组成。另外由乙硼烷二铵或其氘化衍生物构成的全胺硼烷气体产生系统在自发持续反应由热源引发之后提供比自持反应更高的纯度的氢或氘的较高产率（例如，足以引发反应的电加热镍铬丝。这种由N2H4.2BH3和H2B（NH3）2BH4组成的所有胺硼烷气体发生系统是压实的固体推进剂颗粒的形式。使用约500至约10,000磅总负荷的压力将丸粒形成为期望的构型。固体推进剂颗粒可用作用于激光的燃料的H2或D2产生源。

8. 发明授权

US4997497A Castable smoke-producing pyrotechnic compositions 失效
标题翻译：铸造烟草烟火组合物
公开(公告)号：US4997497A
公开(公告)日：1991-03-05
申请号：US504811
申请日：1990-04-05
申请人： Edgar R. Wilson , Milton B. Frankel , Joseph E. Flanagan , Louis R. Grant
发明人： Edgar R. Wilson , Milton B. Frankel , Joseph E. Flanagan , Louis R. Grant
IPC分类号： C06B45/10 , C06D3/00
CPC分类号： C06B45/105 , C06D3/00 , Y10S149/117
摘要： A castable smoke-producing pyrotechnic composition comprising a hydroxy-terminated azido polymer binder with a polyisocyanate curative, an energetic plasticizer, and a dye in an amount sufficient to generate colored smoke.

9. 发明授权

US4468263A Solid propellant hydrogen generator 失效
标题翻译：固体推进剂氢发生器
公开(公告)号：US4468263A
公开(公告)日：1984-08-28
申请号：US450849
申请日：1982-12-20
申请人： Glen D. Artz , Louis R. Grant
发明人： Glen D. Artz , Louis R. Grant
IPC分类号： C06D5/06 , H01S3/095 , C06B43/00
CPC分类号： H01S3/095 , C06D5/06
摘要： Solid reactant hydrogen gas generator formulations which yield greater than5 weight percent hydrogen of greater than 98 mole percent hydrogen purity are formulated of a primary heat and hydrogen source selected from ammonia borane from about 50 to about 70 weight percent and hydrazine bisborane from about 0-30.00 weight percent, a first hydrogen-containing compound that functions as an auxiliary heat and hydrogen source consisting of ammonium nitrate from about 10.20 to about 17.82 weight percent, and a second hydrogen-containing compound that functions as an auxiliary heat and hydrogen source consisting of (NH.sub.4).sub.2 B.sub.10 H.sub.10 from about 9.80 to about 17.18 weight percent.
摘要翻译：配制大于98％（重量）氢纯度的氢重量比大于15％重量的固体反应物氢气发生剂配方，选自氢氧化烃源自约50％至约70％（重量百分比）的氨基硼氢化物， 30.00重量％的第一含氢化合物，其作为由约10.20至约17.82重量％的硝酸铵组成的辅助热源和氢源，以及作为辅助热源和氢源的第二含氢化合物，（NH 4）2B 10 H 10约9.80至约17.18重量％。

10. 发明授权

US4120904A Synthesis of fluorotrinitromethane 失效
标题翻译：氟硝基甲烷的合成
公开(公告)号：US4120904A
公开(公告)日：1978-10-17
申请号：US801453
申请日：1977-05-26
申请人： Donald Pilipovich , Louis R. Grant, Jr. , Richard D. Wilson
发明人： Donald Pilipovich , Louis R. Grant, Jr. , Richard D. Wilson
IPC分类号： C07C205/08 , C07C79/12
CPC分类号： C07C201/12
摘要： In the synthesis of fluorotrinitromethane by reacting tetranitromethane with an adduct of an alkali metal fluoride and a fluorinated or chlorofluorinated acetone in an aprotic dipolar solvent, chlorine or bromine is added during the reaction so as to eliminate side reactions.
摘要翻译：在通过四硝基甲烷与碱金属氟化物和氟化或氯氟化丙酮在非质子偶极溶剂中的加合物的合成中，在反应期间加入氯或溴以消除副反应。

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