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1. 发明授权

US4423256A Recovery of secondary alkanols 失效
标题翻译：二级链烷醇的回收
公开(公告)号：US4423256A
公开(公告)日：1983-12-27
申请号：US435429
申请日：1982-10-20
申请人： Paul V. Shaw , Larry W. Payne , Charles E. Sanborn , Eugene F. Lutz
发明人： Paul V. Shaw , Larry W. Payne , Charles E. Sanborn , Eugene F. Lutz
IPC分类号： C07C29/06 , C07C29/80
CPC分类号： C07C29/06 , C07C29/80
摘要： An improved method for recovery of product alkanol and reactant olefin from a reaction mixture obtained via the sulfation and hydrolysis of C.sub.6 to C.sub.20 olefins, which comprise steps for a limited first evaporation of the reaction mixture under alkaline conditions to obtain an alkanol and olefin rich vapor and a liquid containing by-products of the sulfation and hydrolysis reactions, acid wash of the resulting liquid, and a second evaporation of alkanol and olefin from the washed liquid under acidic conditions. In addition to accomplishing separation of alkanol and olefin, the invention enhances selective utilization of C.sub.6 to C.sub.20 olefins for production of C.sub.6 to C.sub.20 alkanols.
摘要翻译：从通过硫酸化和水解C6至C20烯烃获得的反应混合物中回收产物链烷醇和反应物烯烃的改进方法，其包括在碱性条件下有限地首先蒸发反应混合物以获得链烷醇和富烯烃蒸气的步骤和含有硫酸化和水解反应的副产物的液体，所得液体的酸洗，以及在酸性条件下从洗涤液体中第二次蒸发链烷醇和烯烃。除了完成链烷醇和烯烃的分离之外，本发明增强C6-C20烯烃的选择性利用以生产C 6至C 20链烷醇。

2. 发明授权

US4173586A Process for cleavage of unsaturated multi-cyclic ketones 失效
标题翻译：裂解不饱和多环酮的方法
公开(公告)号：US4173586A
公开(公告)日：1979-11-06
申请号：US942845
申请日：1978-09-15
申请人： Larry W. Payne , Howard E. Miller , James R. Ryffel
发明人： Larry W. Payne , Howard E. Miller , James R. Ryffel
IPC分类号： C07C1/207 , C07C29/00 , C07C45/67 , C07C45/85 , C07C27/00 , C07C3/30
CPC分类号： C07C45/673 , C07C1/2076 , C07C29/00 , C07C45/85 , C07C2101/14 , C07C2101/16 , C07C2523/882 , C07C2523/883 , C07C2531/025
摘要： A process for cleavage of unsaturated multi-cyclic ketones involves thermal cracking of the liquid ketone at elevated temperatures in the absence of water to produce cyclohexanone and a variety of other cleavage products. Para-toluenesulfonic acid and transition metal oxides are advantageously employed as catalysts.
摘要翻译：用于裂解不饱和多环酮的方法包括在不存在水的情况下在升高的温度下液体酮的热裂解以产生环己酮和各种其它裂解产物。对甲苯磺酸和过渡金属氧化物有利地用作催化剂。

3. 发明授权

US4579690A Process for the deoiling of olefin sulfonates 失效
标题翻译：烯烃磺酸盐去油的方法
公开(公告)号：US4579690A
公开(公告)日：1986-04-01
申请号：US687108
申请日：1984-12-28
申请人： Larry W. Payne
发明人： Larry W. Payne
IPC分类号： B01D11/04 , C07C67/00 , C07C301/00 , C07C303/06 , C07C303/42 , C07C303/44 , C07C309/20 , C07C139/14
CPC分类号： C07C303/42
摘要： An improved process for the solvent extraction of free oil from C.sub.8 to C.sub.24 olefin sulfonation products, which comprises steps for contacting an olefin sulfonation product containing free oil with an alkane-based extraction solvent and phase separating the resulting mixture into an extract phase enriched in free oil and a raffinate phase enriched in sulfonated matter. The invention is particularly directed to the use in such a process of an extraction solvent which comprises one or more C.sub.4 to C.sub.9 alkanes and between about 5 and 35 percent by weight of dimethyl ketone. Deoiled sulfonation products are known for utility as components of detergent formulations for industrial, household and personal care uses.
摘要翻译：用于从C 8至C 24烯烃磺化产物溶剂萃取游离油的改进方法，其包括使含有游离油的烯烃磺化产物与基于烷烃的萃取溶剂接触并将所得混合物相分离成富含游离的萃取相的步骤油和富集磺化物质的萃余液相。本发明特别涉及在这种包含一种或多种C 4至C 9烷烃和约5-35％重量二甲基酮的萃取溶剂的方法中的用途。已知脱水磺化产品用作工业，家庭和个人护理用途的洗涤剂配方的组分。

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