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1. 发明授权

US08420261B2 Thin film alloy electrodes 有权
标题翻译：薄膜合金电极
公开(公告)号：US08420261B2
公开(公告)日：2013-04-16
申请号：US12795740
申请日：2010-06-08
申请人： Larry J. Krause , Lowell D. Jensen
发明人： Larry J. Krause , Lowell D. Jensen
IPC分类号： H01M4/52 , H01M4/58
CPC分类号： H01M4/463 , H01M4/38 , H01M4/386 , H01M4/387 , H01M4/505 , H01M4/525 , H01M6/40 , H01M10/0436 , H01M10/052
摘要： Thin film alloy electrodes are provided that are useful as negative electrodes in lithium-ion electrochemical cells. The alloys include aluminum and at least one additional electrochemically active metal or composite. They can be used as a current collector or as a complete electrode.
摘要翻译：提供了可用作锂离子电化学电池中的负极的薄膜合金电极。合金包括铝和至少一种另外的电化学活性金属或复合材料。它们可以用作集电器或完整的电极。

2. 发明申请

US20080311464A1 Method of Using an Electrochemical Cell 有权
标题翻译：电化学电池的使用方法
公开(公告)号：US20080311464A1
公开(公告)日：2008-12-18
申请号：US12064966
申请日：2006-10-02
申请人： Larry J. Krause , Mark N. Obrovac
发明人： Larry J. Krause , Mark N. Obrovac
IPC分类号： H01M10/44
CPC分类号： H01M10/44 , H01M4/134 , H01M4/382 , H01M4/386 , H01M10/0525 , H01M10/446
摘要： The silicon as an anode material for use in lithium ion batteries according to the present invention provides a method for cell manufacturing. The degree to which the silicon is lithiated during cycling can be controlled, thereby lowering the volume expansion while maintaining an acceptable volumetric capacity, and reducing the failure rate of the silicon containing anodes in lithium ion batteries. The crystalline silicon anode is first charged so that the anode becomes partially lithiated. The voltage of the anode during this charging step is typically less than the lithiation potential of crystalline silicon at ambient temperatures, for example, less than 17 OmV versus lithium metal. The total number of charge-discharge cycles during conditioning is at least two or more.
摘要翻译：作为根据本发明的用于锂离子电池的负极材料的硅提供了一种用于电池制造的方法。可以控制硅在循环期间锂化的程度，从而降低体积膨胀，同时保持可接受的体积容量，并降低锂离子电池中含硅阳极的故障率。首先对晶体硅阳极进行充电，使得阳极部分锂化。在该充电步骤期间阳极的电压通常小于环境温度下的结晶硅的锂化电位，例如小于17OmV相对于锂金属。调理期间的充放电循环总数至少为两个以上。

3. 发明授权

US06664004B2 Electrode compositions having improved cycling behavior 有权
公开(公告)号：US06664004B2
公开(公告)日：2003-12-16
申请号：US09883865
申请日：2001-06-18
申请人： Larry J. Krause , James R. Landucci , Kevin W. Eberman
发明人： Larry J. Krause , James R. Landucci , Kevin W. Eberman
IPC分类号： H01M462
CPC分类号： H01M4/40 , B22F7/04 , B22F2998/10 , H01M4/02 , H01M4/04 , H01M4/13 , H01M4/134 , H01M4/364 , H01M4/366 , H01M4/38 , H01M4/386 , H01M4/387 , H01M4/405 , H01M4/44 , H01M4/46 , H01M4/621 , H01M4/624 , H01M4/625 , H01M4/626 , H01M10/052 , H01M10/0525 , H01M10/446 , H01M2004/027 , C25C5/02 , B22F9/04 , C25D7/00
摘要： An electrode composition that includes a plurality of composite particles and a plurality of electrically conductive diluent particles admixed with the composite particles. Each of the composite particles includes an electrochemically active metal particle and an electrically conductive layer partially covering the particle. In one aspect, the layer is present in an amount no greater than about 75 wt. % of the composite, while in another aspect the layer is present in an amount no greater than about 75 vol. % of the composite. Also featured are lithium ion batteries featuring electrodes made from these compositions.

4. 发明授权

US06436578B1 Electrode compositions with high coulombic efficiencies 有权
公开(公告)号：US06436578B1
公开(公告)日：2002-08-20
申请号：US09738517
申请日：2000-12-15
申请人： Robert L. Turner , Donald J. McClure , Larry J. Krause , Mary M. Buckett , Jeffery R. Dahn , Ou Mao
发明人： Robert L. Turner , Donald J. McClure , Larry J. Krause , Mary M. Buckett , Jeffery R. Dahn , Ou Mao
IPC分类号： H01M404
摘要： An electrode composition that includes (a) an electrochemically active metal element which, prior to cycling, is in the form of an intermetallic compound or an elemental metal and (b) a non-electrochemically active metal element. The electrode compositions have high initial capacities that are retained even after repeated cycling. The electrode compositions also exhibit high coulombic efficiencies.

5. 发明授权

US5514493A Perfluoroalkylsulfonates, sulfonimides, and sulfonyl methides, and electrolytes containing them 失效
标题翻译：全氟烷基磺酸盐，磺酰亚胺和磺酰基甲基化物，以及含有它们的电解质
公开(公告)号：US5514493A
公开(公告)日：1996-05-07
申请号：US398859
申请日：1995-03-06
申请人： Jennifer E. Waddell , William M. Lamanna , Larry J. Krause , George G. I. Moore , Steven J. Hamrock
发明人： Jennifer E. Waddell , William M. Lamanna , Larry J. Krause , George G. I. Moore , Steven J. Hamrock
IPC分类号： C07D295/08 , C07C303/38 , C07C309/14 , C07C311/48 , C07C317/28 , C07D241/04 , H01M6/04 , H01M6/16 , H01M10/40
CPC分类号： H01M6/166 , C07C303/38 , H01M6/04
摘要： An electrolyte composition that includes a salt disposed in a matrix in which the salt has a formula selected from the group consisting of ##STR1## in which X.sup.- is --O.sup.-, --N.sup.- SO.sub.2 R.sub.f.sup.3, or ##STR2## Z is --CF.sub.2 --, --O--, --NR.sub.f.sup.8 --, or --SF.sub.4 --; R.sub.f.sup.1 and R.sub.f.sup.2, independently, are --CF.sub.3, --C.sub.m F.sub.2m+1, or --(CF.sub.2).sub.q --SO.sub.2 --X.sup.- M.sup.+ ; R.sub.f.sup.3, R.sub.f.sup.4, and R.sub.f.sup.5, independently, are --CF.sub.3, --C.sub.mf.sub.2m+1, --(CF.sub.2).sub.q --X.sup.- M.sup.+, ##STR3## R.sub.f.sup.8 is --CF.sub.3, --C.sub.m F.sub.2m+1, or --(CF.sub.2).sub.q --SO.sub.2 --X.sup.- M.sup.+ ; R.sub.f.sup.6 and R.sub.f.sup.7, independently, are perfluoroalkylene moieties having the formula --C.sub.r F.sub.2r ; n is 1-4; r is 1-4; m is 1-12; q is 1-4; and M.sup.+ is a counterion.
摘要翻译：一种电解质组合物，其包括设置在基质中的盐，其中所述盐具有选自由下列组成的组的式：-CF 2 - ， - O - ， - NR f 8 - 或-SF 4 - ; Rf1和Rf2独立地是-CF3，-CmF2m + 1或 - （CF2）q-SO2-X-M +; Rf3，Rf4和Rf5独立地是-CF3，-Cmf2m + 1， - （CF2）qX-M +，图像Rf8是-CF3，-CmF2m + 1或 - （CF2）q-SO2 -X-M +; Rf6和Rf7独立地是具有式-CrF 2r的全氟亚烷基部分; n为1-4; r为1-4; m为1-12; q为1-4; 而M +是一个反离子。

6. 发明授权

US5652072A Battery containing bis(perfluoroalkylsulfonyl)imide and cyclic perfluoroalkylene disulfonylimide salts 失效
公开(公告)号：US5652072A
公开(公告)日：1997-07-29
申请号：US531598
申请日：1995-09-21
申请人： William M. Lamanna , Larry J. Krause
发明人： William M. Lamanna , Larry J. Krause
IPC分类号： H01M10/0568 , H01M10/40
CPC分类号： H01M10/0568
摘要： A high performance battery containing an aluminum current collector is described which includes a noncorrosive salt disposed in a matrix, said salt being a bis(perfluoroalkylsulfonyl)imide having a total of at least 3 carbon atoms or a cyclic(perfluoroalkylenedisulfonyl)-imide.

7. 发明授权

US5015538A Process for pulse electroplating electroactive polymers and articles derived therefrom 失效
标题翻译：脉冲电镀电活性聚合物及其衍生物的方法
公开(公告)号：US5015538A
公开(公告)日：1991-05-14
申请号：US411109
申请日：1989-09-22
申请人： Larry J. Krause , Nena M. McCallum
发明人： Larry J. Krause , Nena M. McCallum
IPC分类号： C25D3/48 , C25D5/06 , H01L21/48 , H05K1/03 , H05K3/00 , H05K3/06 , H05K3/10 , H05K3/24 , H05K3/38
CPC分类号： H01L21/4846 , C25D3/48 , C25D5/06 , H05K3/241 , H05K1/0346 , H05K2201/0154 , H05K2203/0723 , H05K3/0017 , H05K3/062 , H05K3/108 , H05K3/388 , Y10S204/09 , Y10S205/926 , Y10S428/935 , Y10T428/12569 , Y10T428/12708 , Y10T428/12715 , Y10T428/12868 , Y10T428/12889 , Y10T428/1291
摘要： The invention consists of a process for pulse electroplating electroactive polymer substrates at potentials sufficient to cause reduction of the substrates. The inventive process can be used to make polymer-metal composites having one or more metal films. More specifically, it can be used to electroplate polyimide substrates with gold, or to electroplate gold over a copper plated polyimide substrate. These inventive composites exhibit improved polymer-metal adhesion when they are exposed to elevated temperatures and humidities, i.e., 85.degree. C. and 85% R.H.
摘要翻译：本发明包括在足以引起基底减少的电位下脉冲电镀电活性聚合物基底的方法。本发明的方法可用于制备具有一个或多个金属膜的聚合物 - 金属复合材料。更具体地，它可以用于将电镀聚酰亚胺基底用金，或者在镀铜的聚酰亚胺基底上电镀金。当这些本发明的复合材料暴露于升高的温度和湿度即85℃和85％R.H时，它们显示出改进的聚合物 - 金属粘合性。

8. 发明授权

US4775556A Process for metallized imaging 失效
标题翻译：金属化成像工艺
公开(公告)号：US4775556A
公开(公告)日：1988-10-04
申请号：US893392
申请日：1986-08-05
申请人： Larry J. Krause , Jack A. Rider
发明人： Larry J. Krause , Jack A. Rider
IPC分类号： C23C14/04 , C23C14/48 , C23C18/16 , C23C18/20 , C23C18/28 , C23C18/31 , B05D3/10
CPC分类号： C23C18/1605 , C23C18/1603 , C23C18/166 , C23C18/1689 , C23C18/208 , C23C18/36 , C23C18/38
摘要： Formation of well-adhered metal layers on aromatic polymeric substrates through a two-step process is based upon reversible charge storage in the electroactive center-containing polymeric substrate. Articles particularly useful for electronic, imaging and solar applications are produced. The process disclosed may be a totally additive process such that articles can be produced in a continuous manner.
摘要翻译：通过两步法在芳族聚合物基材上形成良好附着的金属层是基于含电活性中心的聚合物基质中的可逆电荷存储。产生对电子，成像和太阳能应用特别有用的物品。所公开的方法可以是完全添加的方法，使得可以以连续的方式制造制品。

9. 发明授权

US07972725B2 Polyimide electrode binders 有权
标题翻译：聚酰亚胺电极粘合剂
公开(公告)号：US07972725B2
公开(公告)日：2011-07-05
申请号：US11218448
申请日：2005-09-01
申请人： Larry J. Krause , Lowell D. Jensen
发明人： Larry J. Krause , Lowell D. Jensen
IPC分类号： H01M4/62 , H01M4/58 , H01M4/40
CPC分类号： H01M4/133 , C08G73/106 , H01M4/134 , H01M4/38 , H01M4/386 , H01M4/387 , H01M4/405 , H01M4/587 , H01M4/621 , H01M4/622 , H01M10/052 , H01M10/0525
摘要： Irreversible first cycle capacity loss in lithium secondary cells having a cell electrode based on a powdered material and a binder may be significantly decreased or eliminated by using an aliphatic or cycloaliphatic polyimide binder. Compared to conventional polyimide binders prepared by reacting an aromatic dianhydride and a diamine, the disclosed polyimide binders have decreased aromatic carbonyl content, may be less likely to undergo electrochemical reduction, and may be less likely to consume electrons that might otherwise help lithiate the electrode.
摘要翻译：通过使用脂族或脂环族聚酰亚胺粘合剂，可以显着降低或消除具有基于粉末材料和粘合剂的电池电极的锂二次电池的不可逆的第一循环容量损失。与通过使芳族二酐和二胺反应制备的常规聚酰亚胺粘合剂相比，所公开的聚酰亚胺粘合剂具有降低的芳族羰基含量，可能不太可能经历电化学还原，并且可能不太可能消耗可能有助于锂电极的电子。

10. 发明授权

US06699336B2 Amorphous electrode compositions 有权
标题翻译：无定形电极组合物
公开(公告)号：US06699336B2
公开(公告)日：2004-03-02
申请号：US09751169
申请日：2000-12-29
申请人： Robert L. Turner , Brian D. Fredericksen , Larry J. Krause , Jeffrey R. Dahn , Dominique C. Larcher , Ian A. Courtney , Ou Mao
发明人： Robert L. Turner , Brian D. Fredericksen , Larry J. Krause , Jeffrey R. Dahn , Dominique C. Larcher , Ian A. Courtney , Ou Mao
IPC分类号： C22C4500
CPC分类号： C22C45/00 , C22C21/00 , C22C21/02 , C22C21/14 , C22C45/08 , C23C4/10 , C23C4/123 , C23C14/022 , C23C14/0682 , H01M4/0471 , H01M4/134 , H01M4/364 , H01M4/366 , H01M4/38 , H01M4/386 , H01M4/387 , H01M4/405 , H01M4/44 , H01M4/46 , H01M4/621 , H01M4/624 , H01M10/052 , H01M10/0525
摘要： An electrode composition that includes an electrode material consisting essentially of at least one electrochemically inactive elemental metal and at least one electrochemically active elemental metal in the form of an amorphous mixture at ambient temperature. The mixture remains amorphous when the electrode composition is incorporated into a lithium battery and cycled through at least one full charge-discharge cycle at ambient temperature.
摘要翻译：一种电极组合物，其包括在环境温度下基本上由至少一种电化学惰性元素金属和至少一种无定形混合物形式的电化学活性元素金属组成的电极材料。当电极组合物结合到锂电池中并在环境温度下循环至少一次完全充电 - 放电循环时，该混合物保持非晶态。

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