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1. 发明授权

US06313228B1 Peroxidic treatment of olefin polymers 失效
标题翻译：烯烃聚合物的过氧化物处理
公开(公告)号：US06313228B1
公开(公告)日：2001-11-06
申请号：US09441553
申请日：1999-11-17
申请人： Karl Huber , Jürgen Schwind , Klaus Lehr , Hermann Elser , Horst Klassen , Karl-Heinz Kagerbauer
发明人： Karl Huber , Jürgen Schwind , Klaus Lehr , Hermann Elser , Horst Klassen , Karl-Heinz Kagerbauer
IPC分类号： C08F830
CPC分类号： C08K5/1345 , C08F255/02 , C08K5/14 , C08L23/12
摘要： A process peroxidically treats olefin polymers with di-tert-butyl peroxide in an extruder. The olefin polymers together with di-tert-butyl peroxide under an inert gas are fed to an extruder. The olefin polymers are used in a finely divided form at from 55 to 110° C. The use of peroxidically treated olefin polymers for producing moldings, fibers, films or nonwoven spunbond fabrics is described, as is a process for producing moldings, fibers, films or nonwoven spunbond fabrics.
摘要翻译：一种在挤出机中用二叔丁基过氧化物过氧化处理烯烃聚合物的方法。在惰性气体下将烯烃聚合物与二叔丁基过氧化物一起加入到挤出机中。烯烃聚合物以55-110℃的精细分散形式使用。描述了用于生产模制品，纤维，薄膜或非织造纺粘织物的过氧化物处理的烯烃聚合物，以及用于生产模制品，纤维，薄膜的方法或非织造纺粘织物。

2. 发明授权

US06967223B1 Fiber-free shaped parts 失效
标题翻译：无纤维成型件
公开(公告)号：US06967223B1
公开(公告)日：2005-11-22
申请号：US09623115
申请日：1999-02-17
申请人： Robert Graf , Maria-Elisabeth Kaiser , Klaus Lehr , Wolfgang Six
发明人： Robert Graf , Maria-Elisabeth Kaiser , Klaus Lehr , Wolfgang Six
IPC分类号： C08K3/00 , C08L61/04 , C08J9/00
CPC分类号： C08L61/04 , C08K3/01
摘要： A fiber-free molding composition containing: (a) a binder selected from the group consisting of an epoxide, a polyisocyanate, a furane-resin-free phenolic resin, and mixtures thereof; and (b) a filler mixture containing: (i) an inorganic high-temperature-resistant filler; and (ii) a heat-activatable swelling agent.
摘要翻译：一种无纤维成型组合物，其含有：（a）选自环氧化物，多异氰酸酯，不含呋喃树脂的酚醛树脂及其混合物的粘合剂; 和（b）填料混合物，其含有：（i）无机耐高温填料; 和（ii）可热活化的溶胀剂。

3. 发明授权

US4600565A Process for making manganese (II) salt solutions containing ammonium salt 失效
标题翻译：制备含有铵盐的锰（II）盐溶液的方法
公开(公告)号：US4600565A
公开(公告)日：1986-07-15
申请号：US708299
申请日：1985-03-05
申请人： Klaus Lehr , Bernhard Hofmann , Gero Heymer
发明人： Klaus Lehr , Bernhard Hofmann , Gero Heymer
IPC分类号： C01G45/00 , C22B47/00
CPC分类号： C01G45/00 , C22B47/00
摘要： Manganese(II)salt solutions containing ammonium salt are made by subjecting a manganese-containing compound to processing treatment with an ammonium salt solution. A boiling temperature of 57.degree.-68.degree. C. is established in the suspension to be subjected to the processing treatment, by application of a vacuum. The ammonium salt solution used contains 0.5-2.5 mol/l diammonium sulfate or 1.0-5.0 mol/l ammonium nitrate.
摘要翻译：含有铵盐的锰（II）盐溶液通过使含锰化合物用铵盐溶液进行处理来制备。通过施加真空在待处理处理的悬浮液中建立沸点为57-68℃的温度。使用的铵盐溶液含有0.5-2.5mol / l硫酸二铵或1.0-5.0mol / l硝酸铵。

4. 发明授权

US4392962A Process for separating metals from aqueous solutions 失效
标题翻译：从水溶液中分离金属的工艺
公开(公告)号：US4392962A
公开(公告)日：1983-07-12
申请号：US318736
申请日：1981-11-06
申请人： Klaus Lehr , Gero Heymer , Christian May , Hermann Klein
发明人： Klaus Lehr , Gero Heymer , Christian May , Hermann Klein
IPC分类号： B01D15/04 , B01J20/20 , C01B25/08 , C01G5/00 , C01G7/00 , C01G55/00 , C02F1/62 , C22B3/00 , C22B3/24 , C22B3/44 , C22B11/00 , C22B15/00 , C22B43/00
CPC分类号： C22B11/04 , C01G5/003 , C01G55/001 , C01G7/003 , C22B15/0089 , C22B3/24 , C22B43/00 , Y02P10/234 , Y02P10/236 , Y10S210/912 , Y10S210/914
摘要： The invention relates to a process for separating seminoble and/or noble metals from an aqueous solution having compounds of these metals dissolved therein by subjecting the solution to reaction with red phosphorus. More particularly, the solution is conveyed through a zone containing a layer of granular red phosphorus particles with a size of 0.01 to 10 mm, which may be used in admixture with active carbon.
摘要翻译：本发明涉及一种通过使溶液与红磷反应从其中溶解有这些金属的化合物的水溶液中分离出半金属和/或贵金属的方法。更具体地说，该溶液被输送通过含有0.01至10mm尺寸的粒状红磷颗粒层的区域，其可与活性炭混合使用。

5. 发明授权

US4330504A Apparatus for making red phosphorus 失效
标题翻译：制备红磷的装置
公开(公告)号：US4330504A
公开(公告)日：1982-05-18
申请号：US226468
申请日：1981-01-19
申请人： Klaus Lehr , Gero Heymer , Hans-Werner Stephan , Ursus Thummler
发明人： Klaus Lehr , Gero Heymer , Hans-Werner Stephan , Ursus Thummler
IPC分类号： B01J8/10 , B01J19/28 , B02C17/00 , C01B25/02 , C01B25/023
CPC分类号： C01B25/023
摘要： The invention relates to an apparatus for making red phosphorus by subjecting molten yellow phosphorus to a thermal conversion reaction in a closed reaction zone. To this end, a hollow shaft-provided and closed ball mill is preheated to a reaction temperature within the range 280.degree. to 590.degree. C. Yellow phosphorus is continuously introduced into the ball mill through the hollow shaft in quantities per unit time which permit the reaction temperature prevailing inside the ball mill to be maintained without supply of heat from the outside. More particularly, decreasing quantities of yellow phosphorous are introduced per unit time at increasing temperature and increasing quantities of yellow phosphorus are introduced per unit time at decreasing temperature within the limits specified. Red phosphorus is allowed to cool inside the ball mill, water is poured over it and the whole is subjected to wet-grinding. An aqueous suspension of red phosphorus is finally removed from the ball mill.
摘要翻译：本发明涉及一种通过使熔融黄磷在封闭反应区中进行热转化反应来制备红磷的装置。为此，空心轴提供和封闭的球磨机被预热到280℃至590℃的反应温度。黄磷通过空心轴以每单位时间的量连续地引入球磨机，这允许球磨机内部的反应温度保持不受外界的热量的限制。更特别地，在增加的温度下每单位时间引入黄磷的量减少，并且在规定的限度内在逐渐降低的温度下每单位时间引入增加量的黄磷。使红磷在球磨机内冷却，将水倒在其上，整体进行湿磨。最终从球磨机中除去红磷水悬浮液。

6. 发明授权

US4418043A Process for separating metals from aqueous solutions 失效
标题翻译：从水溶液中分离金属的工艺
公开(公告)号：US4418043A
公开(公告)日：1983-11-29
申请号：US288667
申请日：1981-07-30
申请人： Klaus Lehr , Gero Heymer
发明人： Klaus Lehr , Gero Heymer
IPC分类号： C22B43/00 , C01G1/00 , C01G3/00 , C01G5/00 , C01G13/00 , C01G55/00 , C02F1/28 , C22B11/00 , C22B15/00 , C01G7/00
CPC分类号： C02F1/288 , C02F1/281 , C22B11/04 , C22B3/24 , Y02P10/234 , Y10S210/912
摘要： The invention relates to a process for separating seminoble metals or noble metals from aqueous solutions having compounds of these metals dissolved therein, by reaction with yellow phosphorus. More particularly the aqueous solutions are contacted with carrier material having a yellow phosphorus coating applied thereto.It is possible for the aqueous solutions to be conveyed through a zone having the yellow phosphorus-coated carrier material placed therein, and for them to be subsequently conveyed through a further zone having uncoated carrier material placed therein.
摘要翻译：本发明涉及通过与黄磷反应从其中溶解有这些金属的化合物的水溶液中分离出含半金属或贵金属的方法。更具体地，水溶液与其上施加有黄磷涂层的载体材料接触。水溶液可以通过其中放置有黄磷涂层的载体材料的区域输送，并且随后将其输送通过其中放置有未涂覆的载体材料的另一区域。

7. 发明授权

US4482527A Process for removing nitrogen dioxide from off-gas 失效
标题翻译：从废气中除去二氧化氮的方法
公开(公告)号：US4482527A
公开(公告)日：1984-11-13
申请号：US538130
申请日：1983-10-03
申请人： Klaus Lehr , Gero Heymer
发明人： Klaus Lehr , Gero Heymer
IPC分类号： B01D53/56 , C01B21/00 , B01J8/00
CPC分类号： B01D53/56 , Y02C20/10
摘要： The disclosure relates to a process for removing nitrogen dioxide from off-gas. To this end, the disclosure provides for the off-gas to be intimately contacted with a suspension consisting of red phosphorus and a liquid being inert with respect to red phosphorus, e.g. water.
摘要翻译：本公开涉及从废气中除去二氧化氮的方法。为此，本公开内容提供废气与由红磷和相对于红磷惰性的液体组成的悬浮液紧密接触。水。

8. 发明授权

US4447400A Metering device 失效
标题翻译：计量装置
公开(公告)号：US4447400A
公开(公告)日：1984-05-08
申请号：US362978
申请日：1982-03-29
申请人： Hans-Werner Stephan , Hermann Klein , Klaus Lehr
发明人： Hans-Werner Stephan , Hermann Klein , Klaus Lehr
IPC分类号： B01J4/00 , B02C23/02 , C01B25/02 , C01B25/023
CPC分类号： C01B25/023 , B01J4/008 , B02C23/02
摘要： A device for metering liquid yellow phosphorus into a rotating ball mill for the production of red phosphorus therein includes a stationary outer tubular structure surrounding an inner tubular structure rotatably mounted therein. A valve having a valve rod associated with it is installed within the inner tubular structure near its end close to the ball mill. A plug provided with a central bore receiving the valve rod is installed within the inner tubular structure near its end remote from the ball mill. A bellows surrounds a portion of the valve rod inside the inner tubular structure, the bellows being tightly connected to the plug and valve rod.
摘要翻译：用于将液体黄磷计量到用于产生红磷的旋转球磨机的装置包括围绕可旋转地安装在其中的内管状结构的固定外管状结构。具有与其相关联的阀杆的阀安装在靠近球磨机的端部附近的内管状结构内。设置有容纳阀杆的中心孔的塞子安装在靠近其远离球磨机的端部的内部管状结构内。波纹管围绕内管状结构内的阀杆的一部分，波纹管紧紧地连接到塞子和阀杆。

9. 发明授权

US4394360A Process for reducing iron in phosphoric acid solution 失效
标题翻译：在磷酸溶液中还原铁的方法
公开(公告)号：US4394360A
公开(公告)日：1983-07-19
申请号：US325811
申请日：1981-11-30
申请人： Klaus Schrodter , Klaus Lehr
发明人： Klaus Schrodter , Klaus Lehr
IPC分类号： C01G49/00 , C01B25/238 , C01B25/37 , C01G43/00 , C22B60/02 , C01B15/16 , C01B25/26
CPC分类号： C22B60/0282 , C01B25/238
摘要： Iron contained in phosphoric acid solution is reduced from the trivalent to the bivalent oxidation stage. To this end, red phosphorus is used as the reductant and the reduction is effected in the presence of copper.
摘要翻译：磷酸溶液中所含的铁从三价还原成二价氧化阶段。为此，使用红磷作为还原剂，还原在铜的存在下进行。

10. 发明授权

US4273752A Process for making red phosphorus 失效
标题翻译：制造红磷的工艺
公开(公告)号：US4273752A
公开(公告)日：1981-06-16
申请号：US123106
申请日：1980-02-20
申请人： Klaus Lehr , Gero Heymer , Hans-Werner Stephan , Ursus Thummler
发明人： Klaus Lehr , Gero Heymer , Hans-Werner Stephan , Ursus Thummler
IPC分类号： B01J8/10 , B01J19/28 , B02C17/00 , C01B25/02 , C01B25/023 , C01B25/01 , C01B25/04
CPC分类号： C01B25/023
摘要： The invention relates to a process for making red phosphorus by subjecting molten yellow phosphorus to a thermal conversion reaction in a closed reaction zone. To this end, a hollow shaft-provided and closed ball mill is preheated to a reaction temperature within the range 280.degree. to 590.degree. C. Yellow phosphorus is continuously introduced into the ball mill through the hollow shaft in quantities per unit time which permit the reaction temperature prevailing inside the ball mill to be maintained without supply of heat from the outside. More particularly, decreasing quantities of yellow phosphorus are introduced per unit time at increasing temperature and increasing quantities of yellow phosphorus are introduced per unit time at decreasing temperature within the limits specified. Red phosphorus is allowed to cool inside the ball mill, water is poured over it and the whole is subjected to wet-grinding. An aqueous suspension of red phosphorus is finally removed from the ball mill.
摘要翻译：本发明涉及通过使熔融黄磷在封闭反应区中进行热转化反应来制备红磷的方法。为此，空心轴提供和封闭的球磨机被预热到280℃至590℃的反应温度。黄磷通过空心轴以每单位时间的量连续地引入球磨机，这允许球磨机内部的反应温度保持不受外界的热量的限制。更特别地，在增加的温度下每单位时间引入黄磷的减少量，并且在规定的限度内在降低的温度下每单位时间引入增加量的黄磷。使红磷在球磨机内冷却，将水倒在其上，整体进行湿磨。最终从球磨机中除去红磷水悬浮液。

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