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1. 发明授权

US07728149B2 Process for producing dicarboxylic acid 失效
标题翻译：二羧酸生产方法
公开(公告)号：US07728149B2
公开(公告)日：2010-06-01
申请号：US10498048
申请日：2003-01-14
申请人： Kiyokazu Murata , Hiroyuki Miura
发明人： Kiyokazu Murata , Hiroyuki Miura
IPC分类号： C07C51/16 , C07F15/06
CPC分类号： C07C51/313 , C07C55/14
摘要： A process produces a corresponding dicarboxylic acid by subjecting a cycloalkane to an oxidative cleavage reaction with oxygen in the presence of a catalyst in a liquid phase using a continuous reactor, in which a residence time τ (hr) satisfies the following condition: 0.1≦τ≦50/c, wherein c is the proportion (% by weight) of the cycloalkane to the total weight of a charged liquid. The catalyst includes, for example, cobalt compounds, manganese compounds, and mixtures of these compounds, as well as imide compounds having at least one cyclic imide skeleton.
摘要翻译：一种方法通过使用连续反应器在液相中在催化剂存在下使环烷烃与氧气进行氧化裂解反应，其中停留时间τ（hr）满足以下条件：0.1＆lt; nlE; τ/ nlE; 50 / c，其中c是环烷烃相对于带电液体的总重量的比例（重量％）。催化剂包括例如钴化合物，锰化合物和这些化合物的混合物，以及具有至少一个环状酰亚胺骨架的酰亚胺化合物。

2. 发明授权

US5914428A Process for preparation of isocyanate compounds 失效
标题翻译：异氰酸酯化合物的制备方法
公开(公告)号：US5914428A
公开(公告)日：1999-06-22
申请号：US560517
申请日：1995-11-16
申请人： Toyokazu Yagii , Teruo Itokazu , Kenji Oka , Yasutaka Tanaka , Hidetaka Kojima , Kiyokazu Murata
发明人： Toyokazu Yagii , Teruo Itokazu , Kenji Oka , Yasutaka Tanaka , Hidetaka Kojima , Kiyokazu Murata
IPC分类号： C07C68/00 , C07C263/04 , C07C265/10 , C07C265/14 , C07C269/04 , C07C263/00 , C07C261/00
CPC分类号： C07C269/04 , C07C263/04 , C07C68/005 , C07C2101/12
摘要： An aliphatic diisocyanate compound is prepared in a high yield by reacting dimethyl carbonate with an aliphatic diamine in the presence of an alkali catalyst to produce a corresponding urethane compound; and, within 48 hours after the completion of the preparation of the urethane compound, thermally decomposing the urethane compound under a reduced pressure of 1 to 700 Torr in a high-boiling-point solvent.
摘要翻译：通过在碱催化剂的存在下使碳酸二甲酯与脂族二胺反应，以高收率制备脂族二异氰酸酯化合物，生成相应的氨基甲酸酯化合物; 在氨基甲酸酯化合物的制备完成后48小时内，在高沸点溶剂中，在1〜700乇的减压下热分解氨基甲酸酯化合物。

3. 发明申请

US20050080289A1 Process for producing dicarboxylic acid 失效
标题翻译：二羧酸生产方法
公开(公告)号：US20050080289A1
公开(公告)日：2005-04-14
申请号：US10498048
申请日：2003-01-14
申请人： Kiyokazu Murata , Hiroyuki Miura
发明人： Kiyokazu Murata , Hiroyuki Miura
IPC分类号： C07C51/31 , C07C51/16 , C07F15/06
CPC分类号： C07C51/313 , C07C55/14
摘要： A process produces a corresponding dicarboxylic acid by subjecting a cycloalkane to an oxidative cleavage reaction with oxygen in the presence of a catalyst in a liquid phase using a continuous reactor, in which a residence time τ (hr) satisfies the following condition: 0.1≦τ≦50/c, wherein c is the proportion (% by weight) of the cycloalkane to the total weight of a charged liquid. The catalyst includes, for example, cobalt compounds, manganese compounds, and mixtures of these compounds, as well as imide compounds having at least one cyclic imide skeleton.
摘要翻译：一种方法通过使用连续反应器在液相中在催化剂存在下使环烷烃与氧气进行氧化裂解反应而制备相应的二羧酸，其中停留时间τ（hr）满足以下条件：0.1 < τ<50 / c，其中c是环烷烃相对于带电液体的总重量的比例（重量％）。催化剂包括例如钴化合物，锰化合物和这些化合物的混合物，以及具有至少一个环状酰亚胺骨架的酰亚胺化合物。

4. 发明授权

US5380908A Continuous production of aromatic carbonates 失效
标题翻译：连续生产芳香族碳酸酯
公开(公告)号：US5380908A
公开(公告)日：1995-01-10
申请号：US131679
申请日：1993-10-05
申请人： Kiyokazu Murata , Kozo Kawahashi , Mamoru Watabiki
发明人： Kiyokazu Murata , Kozo Kawahashi , Mamoru Watabiki
IPC分类号： C07C68/06 , C07C69/96
CPC分类号： C07C68/06
摘要： A process for continuously producing aromatic carbonates comprising continuously feeding a dialkyl carbonate, an aromatic hydroxy compound, and a catalyst to a reactor equipped with a distillation tower, continuously distilling off a by-produced aliphatic alcohol from the distillation tower so as to keep the aliphatic alcohol concentration in the reactor at 2% by weight or less, and continuously withdrawing produced alkylaryl carbonate and/or diaryl carbonate and the catalyst from the reactor; and a process for continuously producing a diaryl carbonate comprising continuously feeding an alkylaryl carbonate and a catalyst to a reactor equipped with a distillation tower, continuously distilling off a by-produced dialkyl carbonate from the distillation tower so as to keep the dialkylcarbonate concentration in the reactor at 2% by weight or less, and continuously withdrawing the produced diaryl carbonate and the catalyst from the reactor are disclosed. Continuous production of aromatic carbonates can be performed in a stable manner without being accompanied by clogging of a distillation tower.
摘要翻译：一种连续生产芳族碳酸酯的方法，包括将碳酸二烷基酯，芳族羟基化合物和催化剂连续供入到装有蒸馏塔的反应器中，从蒸馏塔中连续蒸馏出副产的脂族醇，以保持脂肪族反应器中的醇浓度为2重量％以下，从反应器中连续抽出碳酸烷基芳基酯和/或碳酸二芳基酯和催化剂; 以及连续生产碳酸二芳基酯的方法，包括将碳酸烷基芳基酯和催化剂连续加入到装有蒸馏塔的反应器中，从蒸馏塔连续蒸馏出副产的碳酸二烷基酯，以保持反应器中的碳酸二烷基酯浓度在2重量％以下，并且从反应器中连续取出所生产的碳酸二芳基酯和催化剂。芳族碳酸酯的连续生产可以稳定地进行，而不伴随着蒸馏塔的堵塞。

5. 发明授权

US5736259A Packing material for high-performance liquid chromatography and process for producing the same 失效
标题翻译：用于高效液相色谱的包装材料及其制备方法
公开(公告)号：US5736259A
公开(公告)日：1998-04-07
申请号：US537912
申请日：1995-10-20
申请人： Hiroshi Oda , Kiyokazu Murata
发明人： Hiroshi Oda , Kiyokazu Murata
IPC分类号： B01J20/281 , B01J20/291 , B01J20/32 , G01N30/50 , G01N30/88 , B32B23/04 , C07H5/04
CPC分类号： B01J20/286 , B01J20/28004 , B01J20/28085 , B01J20/29 , B01J20/3204 , B01J20/3219 , B01J20/3274 , B01J20/3289 , B01J2220/4825 , B01J2220/54 , B01J2220/58 , Y10T428/31971 , Y10T428/31975
摘要： A process for easily producing a packing material for high-performance liquid chromatography, which produces only a small amount of a dissolved matter. The process has a low cost and contributes to an improvement in the quality of the separated product, without reducing the separation capacity in the field of the separation of only a small amount of a dissolved matter derived from the polysaccharide derivative is obtained by washing the packing material comprising a polysaccharide coated on a carrier with a solvent.
摘要翻译： PCT No.PCT / JP95 / 00490 Sec。 371 1995年10月20日第 102（e）1995年10月20日日期PCT提交1995年3月17日PCT公布。 WO95 / 25279 PCT出版物日期1995年9月21日一种用于容易地生产仅产生少量溶解物质的高效液相色谱用填充材料的方法。该方法成本低，有助于提高分离产物的质量，而不会降低分离领域的分离能力，只有少量衍生自多糖衍生物的溶解物质通过洗涤包装包含用溶剂涂覆在载体上的多糖的材料。

6. 发明授权

US5138015A Process for producing polyurethane 失效
标题翻译：制备聚氨酯的方法
公开(公告)号：US5138015A
公开(公告)日：1992-08-11
申请号：US752481
申请日：1991-09-06
申请人： Toyokazu Yagii , Toshihide Maruyama , Kiyokazu Murata
发明人： Toyokazu Yagii , Toshihide Maruyama , Kiyokazu Murata
IPC分类号： C08G18/70
CPC分类号： C08G18/701
摘要： A process for producing polyurethane useful as coating material, which comprises preparing dialkyl carbonate, substantially without using phosgene, reacting the carbonate with a diamine to give a urethane, thermally decomposing the urethane into a diisocyanate, and converting the diisocyanate into a polyurethane in the presence of a Lewis acid and/or a protonic acid. The reaction of a diisocyanate compound containing a reduced amount of chlorine is promoted by a Lewis acid and/or a protonic acid.

7. 发明授权

US5773643A Process for preparation of isocyanate compounds 失效
标题翻译：异氰酸酯化合物的制备方法
公开(公告)号：US5773643A
公开(公告)日：1998-06-30
申请号：US358680
申请日：1994-12-19
申请人： Toyokazu Yagii , Teruo Itokazu , Kiyokazu Murata
发明人： Toyokazu Yagii , Teruo Itokazu , Kiyokazu Murata
IPC分类号： C07C68/00 , C07C263/04 , C07C265/10 , C07C263/00
CPC分类号： C07C263/04 , C07C68/005 , C07C2101/12
摘要： A diisocyanate compound substantially free from chlorine is prepared by the following consecutive steps (1), (2) and (3): (1) preparing dimethyl carbonate by a method selected from: (a) a method wherein carbon monoxide and oxygen are reacted with methanol, (b) a method wherein propylene oxide is reacted with carbon dioxide to prepare propylene carbonate, and then, the propylene carbonate is reacted with methanol, and (c) a method wherein a nitrous acid ester is catalytically reacted with carbon monoxide; (2) reacting the dimethyl carbonate with an aliphatic diamine in the presence of an alkali catalyst to prepare a corresponding urethane compound; and (3) thermally decomposing the urethane compound under a reduced pressure of 1 to 700 Torr in a high-boiling point solvent.
摘要翻译：通过以下连续步骤（1），（2）和（3）制备基本上不含氯的二异氰酸酯化合物：（1）通过选自以下的方法制备碳酸二甲酯：（a）一氧化碳和氧气反应的方法（b）使环氧丙烷与二氧化碳反应制备碳酸丙烯酯的方法，然后使碳酸亚丙酯与甲醇反应，和（c）亚硝酸酯与一氧化碳催化反应的方法; （2）在碱催化剂存在下使碳酸二甲酯与脂肪族二胺反应，制备相应的氨基甲酸酯化合物; 和（3）在高沸点溶剂中在1〜700托的减压下热分解氨基甲酸酯化合物。

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