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1. 发明授权

US06936739B2 Fluorine-containing bisphenols, their preparation, their precursors and intermediates, and use of the fluorine-containing bisphenols 失效
标题翻译：含氟双酚，其制备方法，其前体和中间体，以及含氟双酚的用途
公开(公告)号：US06936739B2
公开(公告)日：2005-08-30
申请号：US10157520
申请日：2002-05-29
申请人： Albrecht Marhold , Käthe Baumann
发明人： Albrecht Marhold , Käthe Baumann
IPC分类号： C07B61/00 , C07C17/04 , C07C17/20 , C07C17/26 , C07C17/269 , C07C25/18 , C07C25/24 , C07C37/00 , C07C37/055 , C07C39/367 , C07C41/01 , C07C43/225 , C08G63/682 , C08G64/10 , C08G65/38 , C07C39/12
CPC分类号： C07C43/225 , C07C17/04 , C07C17/206 , C07C17/269 , C07C25/18 , C07C25/24 , C07C37/055 , C07C39/367 , C07C41/16 , C08G65/4006 , C08G2650/48 , C09K19/14 , C09K21/08 , C09K2019/0455
摘要： This invention relates to 1,2-di(4-hydroxyaryl)tetrafluoroethanes of the general formula (I) wherein R are each, independently of one another, hydrogen, F, Cl, Br, I, CN, COOR2, C1-C4-alkyl, C1-C4-alkoxy, C1-C4-alkylthio, C1-C4-perfluoroalkyl, C1-C4-perfluoroalkoxy, C1-C4-perfluoroalkylthio, C1-C4-polyfluoroalkyl, C1-C4-polyfluoroalkoxy, or C1-C4-polyfluoroalkylthio, R2 is C1-C4-alkyl, and n is an integer from 0 to 4. This invention further relates to the preparation of such compounds as well as to precursors and intermediates that can be used in their preparation.
摘要翻译：本发明涉及通式（I）的1,2-二（4-羟基芳基）四氟乙烷，其中R各自彼此独立地为氢，F，Cl，Br，I，CN，COOR 2， C 1 -C 4 - 亚烷基，C 1 -C 4 - 烷氧基，C 1 -C 4烷基，C 1 -C 4 - C 1 -C 4亚烷基硫基，C 1 -C 4 - 全氟烷基，C 1〜 C 1 -C 4 - 全氟烷氧基，C 1 -C 4 - 全氟烷硫基，C 1 -C 3 - 4个 - 多氟烷基，C 1 -C 4 - 多氟烷氧基或C 1 -C 4 - - 多氟烷硫基，R 2是C 1 -C 4 - 烷基，n是0-4的整数。本发明还涉及这些化合物的制备以及可用于其制备的前体和中间体。

2. 发明授权

US07268260B2 Fluorine-containing bisphenols, their preparation, their precursors and intermediates, and use of the fluorine-containing bisphenols 失效
标题翻译：含氟双酚，其制备方法，其前体和中间体，以及含氟双酚的用途
公开(公告)号：US07268260B2
公开(公告)日：2007-09-11
申请号：US11498421
申请日：2006-08-03
申请人： Albrecht Marhold , Käthe Baumann
发明人： Albrecht Marhold , Käthe Baumann
IPC分类号： C07C39/12
CPC分类号： C07C43/225 , C07C17/04 , C07C17/206 , C07C17/269 , C07C25/18 , C07C25/24 , C07C37/055 , C07C39/367 , C07C41/16 , C08G65/4006 , C08G2650/48 , C09K19/14 , C09K21/08 , C09K2019/0455
摘要： This invention relates to 1,2-di(4-hydroxyaryl)tetrafluoroethanes of the general formula (I) wherein R are each, independently of one another, hydrogen, F, Cl, Br, I, CN, COOR2, C1-C4-alkyl, C1-C4-alkoxy, C1-C4-alkylthio, C1-C4-perfluoroalkyl, C1-C4-perfluoroalkoxy, C1-C4-perfluoroalkylthio, C1-C4-polyfluoroalkyl, C1-C4-polyfluoroalkoxy, or C1-C4-polyfluoroalkylthio, R2 is C1-C4-alkyl, and n is an integer from 0 to 4. This invention further relates to the preparation of such compounds as well as to precursors and intermediates that can be used in their preparation.
摘要翻译：本发明涉及通式（I）的1,2-二（4-羟基芳基）四氟乙烷，其中R各自彼此独立地为氢，F，Cl，Br，I，CN，COOR 2， C 1 -C 4 - 亚烷基，C 1 -C 4 - 烷氧基，C 1 -C 4烷基，C 1 -C 4 - C 1 -C 4亚烷基硫基，C 1 -C 4 - 全氟烷基，C 1〜 C 1 -C 4 - 全氟烷氧基，C 1 -C 4 - 全氟烷硫基，C 1 -C 3 - 4个 - 多氟烷基，C 1 -C 4 - 多氟烷氧基或C 1 -C 4 - - 多氟烷硫基，R 2是C 1 -C 4 - 烷基，n是0-4的整数。本发明还涉及这些化合物的制备以及可用于其制备的前体和中间体。

3. 发明授权

US06596906B2 Process for preparing fluorine-containing benzaldehydes 失效
公开(公告)号：US06596906B2
公开(公告)日：2003-07-22
申请号：US09957979
申请日：2001-09-21
申请人： Käthe Baumann , Albrecht Marhold
发明人： Käthe Baumann , Albrecht Marhold
IPC分类号： C07C4563
CPC分类号： C07C45/41 , C07C47/55 , C07C47/575
摘要： The invention relates to a particularly advantageous preparation of fluorine-containing benzaldehydes by reacting a corresponding aromatic acid chloride with hydrogen in the presence of a supported palladium catalyst and a catalyst moderator.

4. 发明授权

US07112704B2 Fluorine-containing bisphenols, their preparation, their precursors and intermediates, and use of the fluorine-containing bisphenols 失效
公开(公告)号：US07112704B2
公开(公告)日：2006-09-26
申请号：US11151249
申请日：2005-06-13
申请人： Albrecht Marhold , Käthe Baumann
发明人： Albrecht Marhold , Käthe Baumann
IPC分类号： C07C39/12
CPC分类号： C07C43/225 , C07C17/04 , C07C17/206 , C07C17/269 , C07C25/18 , C07C25/24 , C07C37/055 , C07C39/367 , C07C41/16 , C08G65/4006 , C08G2650/48 , C09K19/14 , C09K21/08 , C09K2019/0455
摘要： This invention relates to 1,2-di(4-hydroxyaryl)tetrafluoroethanes of the general formula (I) wherein R are each, independently of one another, hydrogen, F, Cl, Br, I, CN, COOR2, C1–C4-alkyl, C1–C4-alkoxy, C1–C4-alkylthio, C1–C4-perfluoroalkyl, C1–C4-perfluoroalkoxy, C1–C4-perfluoroalkylthio, C1–C4-polyfluoroalkyl, C1–C4-polyfluoroalkoxy, or C1–C4-polyfluoroalkylthio, R2 is C1–C4-alkyl, and n is an integer from 0 to 4. This invention further relates to the preparation of such compounds as well as to precursors and intermediates that can be used in their preparation.

5. 发明授权

US07019056B2 Flame retardants which contain phosphorus, and flame-retardant thermoplastic molding compositions 有权
公开(公告)号：US07019056B2
公开(公告)日：2006-03-28
申请号：US10039266
申请日：2002-01-04
申请人： Andreas Seidel , Käthe Baumann , Thomas Eckel , Michael Zobel , Jörn Stölting , Dieter Wittmann
发明人： Andreas Seidel , Käthe Baumann , Thomas Eckel , Michael Zobel , Jörn Stölting , Dieter Wittmann
IPC分类号： C08K5/523
CPC分类号： C07F9/12 , C08K5/523 , C08L69/00
摘要： An oligophosphate of general formula is disclosed. The oligophosphate is suitable as a flame retardant for thermoplastic molding compositions that exhibit a good flame-retardant effect, improved dimensional stability under the effect of heat, a good level of toughness and excellent flowability.

6. 发明授权

US06333434B1 Preparation of trifluoromethylanilines 失效
标题翻译：三氟甲基苯胺的制备
公开(公告)号：US06333434B1
公开(公告)日：2001-12-25
申请号：US09707180
申请日：2000-11-06
申请人： Albrecht Marhold , Käthe Baumann
发明人： Albrecht Marhold , Käthe Baumann
IPC分类号： C07C20900
CPC分类号： C07C209/365 , C07C211/52
摘要： The invention relates to a process for the preparation of trifluoromethylanilines of formula (I) wherein R1 is hydrogen, fluorine, chlorine, bromine, methyl, monochloromethyl, dichloromethyl, or formyl, and R2 is hydrogen, fluorine or chlorine, with the proviso that when R1 and R2 are both hydrogen, the amino group is para to the trifluoromethyl group, comprising (a) nitrating a benzotrichloride of formula (II) wherein R1 and R2 are each as defined for formula (I), thereby forming a nitrobenzotrichloride, (b) converting the trichloromethyl group of the nitrobenzotrichloride into a trifluoromethyl group by reaction with anhydrous hydrofluoric acid, thereby forming a nitrobenzotrifluoride, and (c) reducing the nitro groups of the nitrobenzotrifluoride to form a trifluoromethylaniline of formula (I).
摘要翻译：本发明涉及一种制备式（I）的三氟甲基苯胺的方法，其中R 1是氢，氟，氯，溴，甲基，一氯甲基，二氯甲基或甲酰基，R 2是氢，氟或氯，条件是当R1和 R 2均为氢，氨基为三氟甲基的对位，包括（a）硝化式（II）的苯并三氯化物，其中R 1和R 2各自如式（I）所定义，从而形成硝基三氯甲烷，（b）转化通过与无水氢氟酸反应将硝基三氯甲苯的三氯甲基转化为三氟甲基，从而形成硝基三氟甲苯，（c）还原硝基三氟甲苯的硝基以形成式（I）的三氟甲基苯胺。

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