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1. 发明授权

US08865515B2 Preparation method for reduced graphene oxide using sulfonyl hydrazide-based reducing agent and optoelectronic devices thereof 有权
标题翻译：使用磺酰肼类还原剂还原石墨烯氧化物的制备方法及其光电器件
公开(公告)号：US08865515B2
公开(公告)日：2014-10-21
申请号：US13356965
申请日：2012-01-24
申请人： Seok In Na , Dong Yu Kim , Hye Young Koo , Jin Mun Yun , Jun Seok Yeo , Jun Kyung Kim
发明人： Seok In Na , Dong Yu Kim , Hye Young Koo , Jin Mun Yun , Jun Seok Yeo , Jun Kyung Kim
IPC分类号： H01L51/40 , B82Y10/00 , C01B31/04 , B82Y40/00 , B82Y30/00 , H01L51/00 , H01L51/44 , H01L51/52 , H01L51/50
CPC分类号： H01L51/0045 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C01B32/192 , H01L51/44 , H01L51/442 , H01L51/5088 , H01L51/5092 , H01L51/5206 , Y02E10/549 , Y02P70/521
摘要： A method for fabricating a graphene thin film by reducing graphene oxide and a method for fabricating an optoelectronic device using the same are provided. The method for fabricating a graphene thin film includes preparing graphene oxide; preparing graphene through reducing the graphene oxide by a sulfonyl hydrazide-based reducing agent; preparing a graphene dispersed solution by dispersing the graphene into an organic solvent; and fabricating a graphene thin film by applying the graphene dispersed solution. The sulfonyl hydrazide-based reducing agent may be a compound having a sulfonyl hydrazide substituent of Chemical Formula 1 in the present disclosure in which A may be any one in Chemical Formula 2 in the present disclosure.
摘要翻译：提供了通过还原石墨烯氧化物制造石墨烯薄膜的方法和使用其制造光电器件的方法。制造石墨烯薄膜的方法包括制备氧化石墨烯; 通过磺酰肼类还原剂还原氧化石墨烯来制备石墨烯; 通过将石墨烯分散在有机溶剂中制备石墨烯分散溶液; 并通过应用石墨烯分散溶液制造石墨烯薄膜。磺酰肼类还原剂可以是在本公开内容中具有化学式1的磺酰肼取代基的化合物，其中A可以是本公开的化学式2中的任何一个。

2. 发明申请

US20130056063A1 PREPARATION METHOD OF OXIDE ELECTRODE FOR SENSITIZED SOLAR CELL AND SENSITIZED SOLAR CELL USING THE SAME 审中-公开
标题翻译：用于敏化太阳能电池和敏化太阳能电池的氧化物电极的制备方法
公开(公告)号：US20130056063A1
公开(公告)日：2013-03-07
申请号：US13667670
申请日：2012-11-02
申请人： Kyung-Kon KIM , Nam-Gyu PARK , Dong-Young KIM , Jun-Kyung KIM
发明人： Kyung-Kon KIM , Nam-Gyu PARK , Dong-Young KIM , Jun-Kyung KIM
IPC分类号： B05D5/12 , H01L31/0224
CPC分类号： H01G9/2031 , H01G9/2059 , H01L51/0086 , Y02E10/542
摘要： The present invention relates to a method of manufacturing an oxide electrode for a dye-sensitized solar cell including metal oxide nanoparticles by using a miller, and a dye-sensitized solar cell manufactured by using the same. More particularly, the present invention provides a method of manufacturing an oxide electrode for a dye-sensitized solar cell. The method includes (a) mixing metal oxide nanoparticles, a binder resin, and a solvent to prepare a metal oxide paste, (b) coating the metal oxide paste to a miller and pulverizing the metal oxide nanoparticles to prepare a paste including the metal oxide nanoparticles uniformly dispersed therein, and (c) coating the paste including the metal oxide nanoparticles dispersed therein on a conductive transparent substrate, performing a heat treatment of the resulting substrate, and adsorbing a dye thereon to manufacture the conductive electrode.
摘要翻译：本发明涉及一种通过使用研磨机制造包括金属氧化物纳米颗粒的染料敏化太阳能电池的氧化物电极的方法和使用该方法制造的染料敏化太阳能电池。更具体地说，本发明提供一种制造用于染料敏化太阳能电池的氧化物电极的方法。该方法包括：（a）将金属氧化物纳米颗粒，粘合剂树脂和溶剂混合以制备金属氧化物浆料，（b）将金属氧化物糊料涂覆到研磨机中，并粉碎金属氧化物纳米颗粒以制备包含金属氧化物纳米颗粒均匀地分散在其中，（c）将包含分散在其中的金属氧化物纳米颗粒的糊剂涂覆在导电透明基材上，对所得基材进行热处理，并在其上吸附染料以制造导电电极。

3. 发明申请

US20120302683A1 METHOD OF PREPARING REDUCED GRAPHENE OXIDE AND REDUCED GRAPHENE OXIDE-POLYMER COMPOSITES 有权
标题翻译：制备减少氧化铜和还原型氧化烯 - 聚合物复合材料的方法
公开(公告)号：US20120302683A1
公开(公告)日：2012-11-29
申请号：US13410465
申请日：2012-03-02
申请人： Bon-Cheol KU , Ok-kyung PARK , Sung Ho LEE , Seok In NA , Han Ik JO , Jun Kyung KIM , Joong Hee LEE
发明人： Bon-Cheol KU , Ok-kyung PARK , Sung Ho LEE , Seok In NA , Han Ik JO , Jun Kyung KIM , Joong Hee LEE
IPC分类号： C08K5/18 , C07C25/00 , C07C27/00
CPC分类号： H01B1/04 , B82Y30/00 , B82Y40/00 , C01B32/194 , C01B32/23 , C01P2002/72 , C01P2002/82 , C01P2002/88 , C01P2004/04 , C01P2006/40 , C08G61/10 , C08G2261/314 , C08K3/00 , C08K3/04 , C08K3/042 , C09C1/44 , C08L77/00 , C08L79/08 , C08L79/06 , C08L67/00 , C08L23/00
摘要： Methods of preparing reduced graphene oxide and reduced graphene oxide-polymer composites. The methods include covalently binding a halogen-substituted aromatic compounds to a graphene oxide and heat treating the graphene oxide with the halogen-substituted aromatic compounds covalently bound thereto at a low temperature, for example, 450° C. or less. By using the methods, reduced graphene oxide and reduced graphene oxide-polymer composites that have high electrical conductivities (e.g., 30,000 S/m or more) may be obtained.
摘要翻译：制备还原型石墨烯氧化物和还原型氧化烯 - 氧化物 - 聚合物复合材料的方法。所述方法包括将卤素取代的芳族化合物共价结合到石墨烯氧化物上，并在低温，例如450℃或更低的温度下与共价键合的卤素取代的芳族化合物热处理氧化石墨烯。通过使用这些方法，可以获得具有高电导率（例如，30,000S / m以上）的还原型氧化石墨烯和氧化还原型石墨烯 - 聚合物复合材料。

4. 发明申请

US20120190139A1 PREPARATION METHOD FOR REDUCED GRAPHENE OXIDE USING SULFONYL HYDRAZIDE-BASED REDUCING AGENT AND OPTOELECTRONIC DEVICES THEREOF 有权
标题翻译：使用基于硫代氢化物的还原剂及其光电装置减少氧化亚铁的制备方法
公开(公告)号：US20120190139A1
公开(公告)日：2012-07-26
申请号：US13356965
申请日：2012-01-24
申请人： Seok In NA , Dong Yu KIM , Hye Young KOO , Jin Mun YUN , Jun Seok YEO , Jun Kyung KIM
发明人： Seok In NA , Dong Yu KIM , Hye Young KOO , Jin Mun YUN , Jun Seok YEO , Jun Kyung KIM
IPC分类号： H01L51/56 , C01B31/02 , H01L51/48 , B82Y30/00 , B82Y40/00
CPC分类号： H01L51/0045 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C01B32/192 , H01L51/44 , H01L51/442 , H01L51/5088 , H01L51/5092 , H01L51/5206 , Y02E10/549 , Y02P70/521
摘要： A method for fabricating a graphene thin film by reducing graphene oxide and a method for fabricating an optoelectronic device using the same are provided. The method for fabricating a graphene thin film comprises: (a) preparing graphene oxide; (b) preparing graphene through reducing the graphene oxide by a sulfonyl hydrazide-based reducing agent; (c) preparing a graphene dispersed solution by dispersing the graphene into an organic solvent; and (d) fabricating a graphene thin film by applying the graphene dispersed solution. The sulfonyl hydrazide-based reducing agent may be a compound having a sulfonyl hydrazide substituent of Chemical Formula 1 in the present disclosure in which A may be any one in Chemical Formula 2 in the present disclosure.
摘要翻译：提供了通过还原石墨烯氧化物制造石墨烯薄膜的方法和使用其制造光电器件的方法。制造石墨烯薄膜的方法包括：（a）制备氧化石墨烯; （b）通过用磺酰肼类还原剂还原氧化石墨烯来制备石墨烯; （c）通过将石墨烯分散在有机溶剂中制备石墨烯分散溶液; 和（d）通过施加石墨烯分散溶液制造石墨烯薄膜。磺酰肼类还原剂可以是在本公开内容中具有化学式1的磺酰肼取代基的化合物，其中A可以是本公开的化学式2中的任何一个。

5. 发明授权

US08178201B2 Electroconductive particle comprising graphene-coated polymer particle, anisotropic conductive film comprising same and method of making thereof 有权
标题翻译：包含石墨烯涂覆的聚合物颗粒，包括其的各向异性导电膜的导电颗粒及其制备方法
公开(公告)号：US08178201B2
公开(公告)日：2012-05-15
申请号：US12579791
申请日：2009-10-15
申请人： Sang-Soo Lee , Kyunghee Kim , Soon Ho Lim , Min Park , Jun Kyung Kim , Heesuk Kim , Hyunjung Lee
发明人： Sang-Soo Lee , Kyunghee Kim , Soon Ho Lim , Min Park , Jun Kyung Kim , Heesuk Kim , Hyunjung Lee
IPC分类号： B32B5/16 , B05D7/00
CPC分类号： H05K3/323 , C08J3/128 , C08J2325/04 , H01B1/24 , H05K2201/0221 , H05K2201/0323 , Y10T428/249921 , Y10T428/254 , Y10T428/2991 , Y10T428/2998
摘要： An electroconductive particle that includes (a) a polymer microparticle, and (b) a graphene coating layer grafted on the polymer microparticle, which has improved long-term stability of the conductivity, surface conductivity, durability, and thermal resistance, and is applicable for producing an anisotropic conductive film used for packaging electronic devices.
摘要翻译：一种导电颗粒，其包括（a）聚合物微粒和（b）接枝在聚合物微粒上的石墨烯涂层，其具有改善的导电性，表面电导率，耐久性和耐热性的长期稳定性，并且适用于制造用于包装电子器件的各向异性导电膜。

6. 发明申请

US20100266838A1 METHOD FOR FABRICATION OF CONDUCTIVE FILM USING METAL WIRE AND CONDUCTIVE FILM 审中-公开
标题翻译：使用金属线和导电膜制造导电膜的方法
公开(公告)号：US20100266838A1
公开(公告)日：2010-10-21
申请号：US12575685
申请日：2009-10-08
申请人： Hyun-Jung LEE , Hee-Suk KIM , Jun-Kyung KIM , Kyoung-Ah OH , Seung-Woong NAM , Soon-Ho LIM
发明人： Hyun-Jung LEE , Hee-Suk KIM , Jun-Kyung KIM , Kyoung-Ah OH , Seung-Woong NAM , Soon-Ho LIM
IPC分类号： B32B5/16 , B05D3/06 , B05D5/12
CPC分类号： H01B1/24 , H01B1/22 , H05K1/097 , H05K2201/026 , H05K2201/0281 , H05K2203/0285 , Y10T428/25
摘要： A method for fabricating a conductive film, and a conductive film fabricated by the same. The method comprises: preprocessing carbon nanotubes by at least one of a cutting step using ultrasonic wave, and a chemical reaction step with acid; dispersing the carbon nanotubes in a solvent; mixing metal wires with the carbon nanotubes dispersion solution; and forming an electrode layer by coating the mixed resultant on a substrate. Accordingly, can be easily fabricated the conductive film having high transmittance and high electric conductivity.
摘要翻译：一种导电膜的制造方法和由其制造的导电膜。该方法包括：通过使用超声波的切割步骤和与酸的化学反应步骤中的至少一个来预处理碳纳米管; 将碳纳米管分散在溶剂中; 将金属线与碳纳米管分散液混合; 以及通过将混合的结果涂覆在基底上来形成电极层。因此，可以容易地制造具有高透射率和高导电性的导电膜。

7. 发明申请

US20100263908A1 METHOD FOR FABRICATION OF CONDUCTIVE FILM USING CONDUCTIVE FRAME AND CONDUCTIVE FILM 审中-公开
标题翻译：使用导电框架和导电膜制造导电膜的方法
公开(公告)号：US20100263908A1
公开(公告)日：2010-10-21
申请号：US12575699
申请日：2009-10-08
申请人： Hyun-Jung LEE , Hee-Suk KIM , Sun-Young NOH , Sun-Na Hwang , Soon-Ho LIM , Min PARK , Jun-Kyung KIM
发明人： Hyun-Jung LEE , Hee-Suk KIM , Sun-Young NOH , Sun-Na Hwang , Soon-Ho LIM , Min PARK , Jun-Kyung KIM
IPC分类号： H01B5/00 , B05D1/36 , C23C16/00 , B05D1/02 , B29C47/00 , C25D13/00 , C25D5/34
CPC分类号： C09D5/24 , B82Y30/00 , C08K3/041 , C09D7/70 , C23C18/08 , C25D13/02 , H01B1/24
摘要： Disclosed are a method for fabricating a conductive film, and a conductive film fabricated by the same. The method comprises: forming a mixed solution consisting of at least one of a metallic precursor and a conductive polymer; spraying atomized droplets of the mixed solution on a surface of a substrate so as to form conductive frames; and coupling carbon nanotubes to the conductive frames so as to enhance electric conductivity. Accordingly, the conductive film can have enhanced electric conductivity, and can be easily fabricated.
摘要翻译：公开了一种制造导电膜的方法及其制造的导电膜。该方法包括：形成由金属前体和导电聚合物中的至少一种组成的混合溶液; 将混合溶液的雾化液滴喷射到基板的表面上，形成导电框架; 并将碳纳米管偶联到导电框架上以提高导电性。因此，导电膜可以具有增强的导电性，并且可以容易地制造。

8. 发明申请

US20100206361A1 PREPARATION METHOD OF OXIDE ELECTRODE FOR SENSITIZED SOLAR CELL AND SENSITIZED SOLAR CELL USING THE SAME 审中-公开
标题翻译：用于敏化太阳能电池和敏化太阳能电池的氧化物电极的制备方法
公开(公告)号：US20100206361A1
公开(公告)日：2010-08-19
申请号：US12446837
申请日：2006-12-08
申请人： Kyung-Kon Kim , Nam-Gyu Park , Dong-Young Kim , Jun-Kyung Kim
发明人： Kyung-Kon Kim , Nam-Gyu Park , Dong-Young Kim , Jun-Kyung Kim
IPC分类号： H01L31/00 , B05D5/12
CPC分类号： H01G9/2031 , H01G9/2059 , H01L51/0086 , Y02E10/542 , Y02P70/521
摘要： The present invention relates to a method of manufacturing an oxide electrode for a dye-sensitized solar cell including metal oxide nanoparticles by using a miller, and a dye-sensitized solar cell manufactured by using the same. More particularly, the present invention provides a method of manufacturing an oxide electrode for a dye-sensitized solar cell. The method includes (a) mixing metal oxide nanoparticles, a binder resin, and a solvent to prepare a metal oxide paste, (b) coating the metal oxide paste to a miller and pulverizing the metal oxide nanoparticles to prepare a paste including the metal oxide nanoparticles uniformly dispersed therein, and (c) coating the paste including the metal oxide nanoparticles dispersed therein on a conductive transparent substrate, performing a heat treatment of the resulting substrate, and adsorbing a dye thereon to manufacture the conductive electrode.
摘要翻译：本发明涉及一种通过使用研磨机制造包括金属氧化物纳米颗粒的染料敏化太阳能电池的氧化物电极的方法和使用该方法制造的染料敏化太阳能电池。更具体地说，本发明提供一种制造用于染料敏化太阳能电池的氧化物电极的方法。该方法包括：（a）将金属氧化物纳米颗粒，粘合剂树脂和溶剂混合以制备金属氧化物浆料，（b）将金属氧化物糊料涂覆到研磨机中，并粉碎金属氧化物纳米颗粒以制备包含金属氧化物纳米颗粒均匀地分散在其中，（c）将包含分散在其中的金属氧化物纳米颗粒的糊剂涂覆在导电透明基材上，对所得基材进行热处理，并在其上吸附染料以制造导电电极。

9. 发明申请

US20080131685A1 MICROCAPSULE-CONDUCTIVE PARTICLE COMPLEX, PREPARATION METHOD THEREOF AND ANISOTROPIC CONDUCTIVE ADHESIVE FILM USING THE SAME 审中-公开
标题翻译：微导电颗粒复合物，其制备方法和使用其的各向异性导电粘合膜
公开(公告)号：US20080131685A1
公开(公告)日：2008-06-05
申请号：US11939538
申请日：2007-11-13
申请人： Sang-Soo LEE , Jun-Kyung Kim , Hae-Eun Jung , Min Park , Soon-Ho Lim , Hyun-Jung Lee
发明人： Sang-Soo LEE , Jun-Kyung Kim , Hae-Eun Jung , Min Park , Soon-Ho Lim , Hyun-Jung Lee
IPC分类号： B32B5/16
CPC分类号： H01B1/22 , H05K3/323 , H05K2201/0224 , H05K2203/1163 , Y10T428/254 , Y10T428/2989
摘要： The present invention relates to a microcapsule-conductive particle complex comprising a conductive particle consisting of conductive metallic particle or polymer particle coated on a surface with a conductive metallic layer; a microcapsule being adsorbed by the conductive particle or adsorbing the conductive particle, comprising a core and a shell, wherein the core contains organic compound which is a curing agent for a fast curing at a low temperature and the shell has a surface functional group with affinity for metal of the conductive metallic layer on its surface, a preparation method thereof and an anisotropic conductive film (ACF) using the same.
摘要翻译：本发明涉及一种微胶囊导电颗粒复合体，其包含由导电金属颗粒或涂覆在具有导电金属层的表面上的聚合物颗粒组成的导电颗粒; 微胶囊被导电颗粒吸附或吸附导电颗粒，包括芯和壳，其中芯包含作为在低温下快速固化的固化剂的有机化合物，并且壳具有亲和力的表面官能团其表面上的导电金属层的金属，其制备方法和使用其的各向异性导电膜（ACF）。

10. 发明申请

US20120168383A1 GRAPHENE-IRON OXIDE COMPLEX AND FABRICATION METHOD THEREOF 审中-公开
标题翻译：石墨氧化物复合物及其制造方法
公开(公告)号：US20120168383A1
公开(公告)日：2012-07-05
申请号：US13230993
申请日：2011-09-13
申请人： Hye Young KOO , Won San CHOI , Jun Kyung KIM
发明人： Hye Young KOO , Won San CHOI , Jun Kyung KIM
IPC分类号： C02F1/62 , C02F1/28 , C01G49/00 , B32B3/00 , B82Y40/00 , B82Y30/00
CPC分类号： C02F1/288 , B82Y30/00 , B82Y40/00 , C01B32/184 , C01B32/23 , C01B2204/22 , C01B2204/32 , C02F1/44 , C02F2101/20 , Y10T428/24355
摘要： A graphene-iron oxide complex consists of graphene and needle-like iron oxide nanoparticles grown on a surface of the graphene, and a fabricating method thereof includes (A) preparing a reduced graphene dispersed solution, (B) mixing the dispersed solution with a solution containing iron oxide precursors to prepare a mixture, (C) stirring the mixture to prepare a graphene-iron oxide dispersed solution containing the graphene-iron oxide complex that needle-like iron oxide nanoparticles are grown on the surface of the graphene, and (D) separating the graphene-iron oxide complex from the graphene-iron oxide complex dispersed solution.
摘要翻译：石墨烯 - 氧化铁络合物由在石墨烯表面生长的石墨烯和针状氧化铁纳米粒子组成，其制造方法包括（A）制备还原型石墨烯分散溶液，（B）将分散溶液与溶液（C）搅拌混合物以制备含石墨烯 - 氧化铁络合物的石墨烯 - 氧化铁分散溶液，其中针状氧化铁纳米颗粒在石墨烯的表面上生长，（D ）从石墨烯 - 铁氧化物复合物分散溶液中分离石墨烯 - 氧化铁络合物。

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