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1. 发明授权

US08865055B2 Production of sintered three-dimensional ceramic bodies 有权
标题翻译：烧结三维陶瓷体的生产
公开(公告)号：US08865055B2
公开(公告)日：2014-10-21
申请号：US13385414
申请日：2012-02-17
申请人： Juan L. Sepulveda , Raouf O. Loutfy , Sekyung Chang , Ricardo Ramos , Sharly Ibrahim
发明人： Juan L. Sepulveda , Raouf O. Loutfy , Sekyung Chang , Ricardo Ramos , Sharly Ibrahim
IPC分类号： C04B35/443 , C04B35/645 , B29B13/04 , C04B35/626 , C04B35/632 , B28B3/02 , B28B1/00
CPC分类号： B29B13/045 , B28B1/007 , B28B3/025 , C04B35/443 , C04B35/62655 , C04B35/632 , C04B35/645 , C04B35/6455 , C04B2235/3203 , C04B2235/445 , C04B2235/6026 , C04B2235/604 , C04B2235/608 , C04B2235/656 , C04B2235/6567 , C04B2235/6581 , C04B2235/661 , C04B2235/94 , C04B2235/96
摘要： A freeze-forging method for producing sintered three-dimensional ceramic bodies, particularly magnesium aluminate spinel domes. The method comprises forming a ceramic mix of a ready-to-sinter ceramic powder and a nonaqueous liquefied sublimable vehicle having a solidification temperature from room temperature to below 200° C.; reducing the temperature of the ceramic mix to below the vehicle's solidification temperature to freeze the mix; crushing the frozen mix into powdered form; molding the frozen powder into net shape by cold forging in a mold to form a net-shaped green body preform of the desired three-dimensional shape; and densifying the green body into a sintered three-dimensional ceramic body.
摘要翻译：用于制造烧结的三维陶瓷体，特别是铝酸镁尖晶石圆顶的冷冻锻造方法。该方法包括将固化温度从室温至低于200℃形成即可烧结陶瓷粉末和非水液化可升华载体的陶瓷混合物; 将陶瓷混合物的温度降低到低于车辆凝固温度以冷冻混合物; 将冷冻的混合物粉碎成粉末状; 通过在模具中冷锻来将冷冻粉末成型为网状，以形成具有所需三维形状的网状生坯预制件; 并将生坯致密化成烧结的三维陶瓷体。

2. 发明授权

US06589310B1 High conductivity copper/refractory metal composites and method for making same 失效
$High conductivity copper/refractory metal composites and method for making same$
标题翻译：高导电铜/难熔金属复合材料及其制备方法
公开(公告)号：US06589310B1
公开(公告)日：2003-07-08
申请号：US09571809
申请日：2000-05-16
申请人： Mark Opoku-Adusei , David E. Jech , Juan L. Sepulveda
发明人： Mark Opoku-Adusei , David E. Jech , Juan L. Sepulveda
IPC分类号： C22C104
CPC分类号： H01L23/3736 , C22C1/045 , C22C27/04 , H01L2924/0002 , H01L2924/00
摘要： The thermal conductivity, thermal conductivity, of a sintered copper/refractory metal composite having a maximum porosity of about 1% is greatly improved when the composite contains phosphorus and sintering aid in a specified weight ratio, “phosphorus/sintering aid ratio.” The copper/refractory matrix composite herein comprises, by weight, from about 5% to about 30% copper, from about 0.2% to about 0.6% sintering aid, from about 0.08% to about 0.3% phosphorus, the remaining metal is refractory metal. The phosphorus to sintering aid ratio ranges from about 0.25 to about 0.55. In one embodiment of the invention the sintering aid contains cobalt and the refractory metal is tungsten.
摘要翻译：当复合材料以特定重量比“磷/烧结助剂比例”含有磷和烧结助剂时，具有最大孔隙率约1％的烧结铜/难熔金属复合材料的导热性，导热性大大提高。本发明的铜/耐火材料基质复合材料包含约5％至约30％的铜，约0.2％至约0.6％的烧结助剂，约0.08％至约0.3％的磷，剩余的金属是难熔金属。磷与烧结助剂的比例为约0.25至约0.55。在本发明的一个实施方案中，烧结助剂含有钴，难熔金属是钨。

3. 发明申请

US20130106009A1 Production of sintered three-dimensional ceramic bodies 有权
标题翻译：烧结三维陶瓷体的生产
公开(公告)号：US20130106009A1
公开(公告)日：2013-05-02
申请号：US13385414
申请日：2012-02-17
申请人： Juan L. Sepulveda , Raouf O. Loutfy , Sekyung Chang , Ricardo Ramos , Sharly Ibrahim
发明人： Juan L. Sepulveda , Raouf O. Loutfy , Sekyung Chang , Ricardo Ramos , Sharly Ibrahim
IPC分类号： B29B13/04
CPC分类号： B29B13/045 , B28B1/007 , B28B3/025 , C04B35/443 , C04B35/62655 , C04B35/632 , C04B35/645 , C04B35/6455 , C04B2235/3203 , C04B2235/445 , C04B2235/6026 , C04B2235/604 , C04B2235/608 , C04B2235/656 , C04B2235/6567 , C04B2235/6581 , C04B2235/661 , C04B2235/94 , C04B2235/96
摘要： A freeze-forging method for producing sintered three-dimensional ceramic bodies, particularly magnesium aluminate spinel domes. The method comprises forming a ceramic mix of a ready-to-sinter ceramic powder and a nonaqueous liquefied sublimable vehicle having a solidification temperature from room temperature to below 200° C.; reducing the temperature of the ceramic mix to below the vehicle's solidification temperature to freeze the mix; crushing the frozen mix into powdered form; molding the frozen powder into net shape by cold forging in a mold to form a net-shaped green body preform of the desired three-dimensional shape; and densifying the green body into a sintered three-dimensional ceramic body.
摘要翻译：用于制造烧结的三维陶瓷体，特别是铝酸镁尖晶石圆顶的冷冻锻造方法。该方法包括将固化温度从室温至低于200℃形成即可烧结陶瓷粉末和非水液化可升华载体的陶瓷混合物; 将陶瓷混合物的温度降低到低于车辆凝固温度以冷冻混合物; 将冷冻的混合物粉碎成粉末状; 通过在模具中冷锻来将冷冻粉末成型为网状，以形成具有所需三维形状的网状生坯预制件; 并将生坯致密化成烧结的三维陶瓷体。

4. 发明申请

US20100144510A1 Production of sintered three-dimensional ceramic bodies 审中-公开
标题翻译：烧结三维陶瓷体的生产
公开(公告)号：US20100144510A1
公开(公告)日：2010-06-10
申请号：US12460450
申请日：2009-07-16
申请人： Juan L. Sepulveda , Raouf O. Loutfy , Sekyung Chang , Ricardo Ramos , Sharly Ibrahim
发明人： Juan L. Sepulveda , Raouf O. Loutfy , Sekyung Chang , Ricardo Ramos , Sharly Ibrahim
IPC分类号： C04B35/04 , B29C35/16
CPC分类号： C04B35/443 , B28B1/04 , B28B3/025 , C04B35/62655 , C04B35/632 , C04B35/645 , C04B35/6455 , C04B2235/3203 , C04B2235/445 , C04B2235/6026 , C04B2235/604 , C04B2235/608 , C04B2235/656 , C04B2235/6567 , C04B2235/6581 , C04B2235/661 , C04B2235/94 , C04B2235/96
摘要： A freeze-forging method for producing sintered three-dimensional ceramic bodies, particularly magnesium aluminate spinel domes. The method comprises forming a ceramic mix of a ready-to-sinter ceramic powder and a nonaqueous liquefied sublimable vehicle having a solidification temperature from room temperature to below 200° C.; reducing the temperature of the ceramic mix to below the vehicle's solidification temperature to freeze the mix; crushing the frozen mix into powdered form; cold forging the frozen powder in a mold to form a solidified green body of the desired three-dimensional shape; and densifying the green body into a sintered three-dimensional ceramic body.
摘要翻译：用于制造烧结的三维陶瓷体，特别是铝酸镁尖晶石圆顶的冷冻锻造方法。该方法包括将固化温度从室温至低于200℃形成即可烧结陶瓷粉末和非水液化可升华载体的陶瓷混合物; 将陶瓷混合物的温度降低到低于车辆凝固温度以冷冻混合物; 将冷冻的混合物粉碎成粉末状; 将冷冻粉末在模具中冷锻以形成所需三维形状的固化生坯; 并将生坯致密化成烧结的三维陶瓷体。

5. 发明授权

US5993731A Process for making improved net shape or near net shape metal parts 失效
标题翻译：改善净形状或近净形金属部件的工艺
公开(公告)号：US5993731A
公开(公告)日：1999-11-30
申请号：US966041
申请日：1997-11-07
申请人： David E. Jech , Juan L. Sepulveda , Anthony B. Traversone
发明人： David E. Jech , Juan L. Sepulveda , Anthony B. Traversone
IPC分类号： B22F3/00 , B22F3/10 , B22F3/23 , C22C1/04 , C22C1/05 , B22F1/00
CPC分类号： C22C1/05 , B22F3/001 , B22F3/10 , B22F3/23 , C22C1/045 , B22F2003/1042 , B22F2998/00 , B22F2998/10 , B22F2999/00
摘要： The process for producing net shape or near net shape metal parts is improved by sintering a compact in a reducing atmosphere where the compact contains a metal and chemically-bound oxygen in the form of a metal oxide, for example, and the chemically-bound oxygen is in an amount sufficient to improve the sintering of the compact. Improved sintering is facilitated when the metal oxide forms a metal/metal oxide eutectic during reduction of the chemically-bound oxygen in a reducing atmosphere during the sintering process. The compact can contain a metal oxide and a solution compound to produce an alloy part, provided the chemically-bound oxygen is present in an amount sufficient to improve sintering. In a preferred embodiment, the compact also contains a reinforcement compound and is sintered to make a metal matrix composite. The resultant density of the near net shape metal parts made by the improved sintering process is preferably about 97% or more of the theoretical density.
摘要翻译：用于制造网状或近净金属部件的方法通过在还原气氛中烧结压块而改进，其中压实体包含金属和金属氧化物形式的化学结合氧，以及化学结合的氧其量足以改善压块的烧结。当在烧结过程中还原气氛中的化学结合氧还原期间金属氧化物形成金属/金属氧化物共晶时，促进了烧结的改善。只要化学结合的氧以足以改善烧结的量存在，该压块可以包含金属氧化物和溶液化合物以产生合金部件。在优选的实施方案中，压块还包含增强化合物并烧结以制备金属基质复合材料。通过改善烧结工艺制成的近净形金属部件的合成密度优选为理论密度的约97％以上。

6. 发明申请

US20120063071A1 Machinable metal/diamond metal matrix composite compound structure and method of making same 审中-公开
标题翻译：可加工金属/金刚石金属基复合复合结构及其制造方法
公开(公告)号：US20120063071A1
公开(公告)日：2012-03-15
申请号：US13135638
申请日：2011-07-12
申请人： Raouf O. Loutfy , James C. Withers , Juan L. Sepulveda , Sharty Ibrahim , Kevin Loutfy
发明人： Raouf O. Loutfy , James C. Withers , Juan L. Sepulveda , Sharty Ibrahim , Kevin Loutfy
IPC分类号： H05K7/02 , B32B3/24 , B32B3/30 , B32B15/04
CPC分类号： C09K3/1436 , C22C1/101 , C22C1/1036 , C22C21/00 , C22C23/00 , C22C26/00 , Y10T428/12361 , Y10T428/12389 , Y10T428/12764 , Y10T428/12986
摘要： A high thermal conductivity metal/diamond metal matrix composite made from diamond particles having thin layers of beta-SiC chemically bonded to the surfaces thereof, is utilized in combination with a machinable metal/carbonaceous material metal matrix composite in an integral metal matrix composite compound structure, to provide a machinable high thermal conductivity heat-dissipating substrate for electronic devices.
摘要翻译：与其表面化学键合的具有薄层β-SiC的金刚石颗粒制成的高导热性金属/金刚石金属基质复合物与可整合的金属基质复合结构中的可机加工的金属/含碳材料金属基质复合材料，为电子设备提供可机加工的高导热性散热基板。

7. 发明申请

US20100056357A1 Ready-to-sinter spinel nanomixture and method for preparing same 失效
标题翻译：即用型烧结尖晶石纳米混合物及其制备方法
公开(公告)号：US20100056357A1
公开(公告)日：2010-03-04
申请号：US12460451
申请日：2009-07-16
申请人： Raouf O. Loutfy , Juan L. Sepulveda , Sekyung Chang
发明人： Raouf O. Loutfy , Juan L. Sepulveda , Sekyung Chang
IPC分类号： C04B35/04 , C04B35/043 , C04B35/64
CPC分类号： C04B35/443 , B82Y30/00 , C04B35/6263 , C04B35/6264 , C04B35/645 , C04B35/6455 , C04B2235/3203 , C04B2235/3222 , C04B2235/445 , C04B2235/5445 , C04B2235/5454 , C04B2235/6562 , C04B2235/661 , C04B2235/668 , C04B2235/763 , C04B2235/9653
摘要： An in-situ method for nanomixing magnesium aluminate spinel nanoparticles with a uniformly distributed controlled concentration of nanoparticles of an inorganic sintering aid, such as LiF, to produce ready-to-sinter spinel powder. The spinel-sintering aid nanomixture is formed by induced precipitation of the sintering aid nanoparticles from a dispersion of the spinel nanoparticles in an aqueous solution of the sintering aid, followed by separation, drying and deagglomeration of the spinel-sintering aid nanomixed product.
摘要翻译：纳米混合铝酸镁尖晶石纳米颗粒的原位方法，其具有均匀分布的受控浓度的无机烧结助剂如LiF的纳米颗粒，以产生即用型烧结尖晶石粉末。尖晶石烧结助剂纳米混合物通过将烧结助剂纳米颗粒从尖晶石纳米颗粒的分散体中诱导沉淀在烧结助剂的水溶液中，随后尖晶石烧结助剂纳米混合产物的分离，干燥和解团而形成。

8. 发明授权

US5686676A Process for making improved copper/tungsten composites 失效
标题翻译：制备改进的铜/钨复合材料的方法
公开(公告)号：US5686676A
公开(公告)日：1997-11-11
申请号：US646449
申请日：1996-05-07
申请人： David E. Jech , Juan L. Sepulveda , Anthony B. Traversone
发明人： David E. Jech , Juan L. Sepulveda , Anthony B. Traversone
IPC分类号： B22F3/00 , B22F3/10 , B22F3/23 , C22C1/04 , C22C1/05 , C22C27/04 , B22F3/12
CPC分类号： C22C1/05 , B22F3/001 , B22F3/10 , B22F3/23 , C22C1/045 , B22F2003/1042 , B22F2998/00 , B22F2998/10 , B22F2999/00
摘要： The sinterability of a copper/tungsten green compact is improved by using copper oxide, tungsten oxide or both as the copper and/or tungsten source. Sinterability is further enhanced by including steam in the sintering atmosphere.
摘要翻译：通过使用氧化铜，氧化钨或两者作为铜和/或钨源，可提高铜/钨生坯的烧结性。通过在烧结气氛中包括蒸汽进一步增强了烧结性。

9. 发明授权

US08313725B2 Ready-to-sinter spinel nanomixture and method for preparing same 失效
标题翻译：即用型烧结尖晶石纳米混合物及其制备方法
公开(公告)号：US08313725B2
公开(公告)日：2012-11-20
申请号：US12460451
申请日：2009-07-16
申请人： Raouf O. Loutfy , Juan L. Sepulveda , Sekyung Chang
发明人： Raouf O. Loutfy , Juan L. Sepulveda , Sekyung Chang
IPC分类号： C01B13/14 , C01F5/02 , C01F5/14 , C01F11/02 , C04B35/03
CPC分类号： C04B35/443 , B82Y30/00 , C04B35/6263 , C04B35/6264 , C04B35/645 , C04B35/6455 , C04B2235/3203 , C04B2235/3222 , C04B2235/445 , C04B2235/5445 , C04B2235/5454 , C04B2235/6562 , C04B2235/661 , C04B2235/668 , C04B2235/763 , C04B2235/9653
摘要： An in-situ method for nanomixing magnesium aluminate spinel nanoparticles with a uniformly distributed controlled concentration of nanoparticles of an inorganic sintering aid, such as LiF, to produce ready-to-sinter spinel powder. The spinel-sintering aid nanomixture is formed by induced precipitation of the sintering aid nanoparticles from a dispersion of the spinel nanoparticles in an aqueous solution of the sintering aid, followed by separation, drying and deagglomeration of the spinel-sintering aid nanomixed product.
摘要翻译：纳米混合铝酸镁尖晶石纳米颗粒的原位方法，其具有均匀分布的受控浓度的无机烧结助剂如LiF的纳米颗粒，以产生即用型烧结尖晶石粉末。尖晶石烧结助剂纳米混合物通过将烧结助剂纳米颗粒从尖晶石纳米颗粒的分散体中诱导沉淀在烧结助剂的水溶液中，随后尖晶石烧结助剂纳米混合产物的分离，干燥和解团而形成。

10. 发明授权

US6114048A Functionally graded metal substrates and process for making same 失效
标题翻译：功能分级金属基材及其制造方法
公开(公告)号：US6114048A
公开(公告)日：2000-09-05
申请号：US148126
申请日：1998-09-04
申请人： David E. Jech , Jordan P. Frazier , Richard H. Sworden , Juan L. Sepulveda
发明人： David E. Jech , Jordan P. Frazier , Richard H. Sworden , Juan L. Sepulveda
IPC分类号： B22F3/26 , B22F7/00 , B22F7/04 , B22F7/06 , C22C9/00 , C22C27/04 , H01L23/12 , H01L23/14 , H01L23/367 , H01L23/373
CPC分类号： H01L23/3677 , B22F7/008 , H01L23/3733 , H01L23/3736 , B22F2998/00 , H01L2924/0002 , Y10T428/12021 , Y10T428/12042 , Y10T428/12063 , Y10T428/12076 , Y10T428/1216 , Y10T428/12174 , Y10T428/12229 , Y10T428/12458 , Y10T428/12479 , Y10T428/12514 , Y10T428/12528 , Y10T428/12576 , Y10T428/12625 , Y10T428/12646 , Y10T428/12729 , Y10T428/12736 , Y10T428/12771 , Y10T428/12778 , Y10T428/12986
摘要： The invention provides for a functionally-graded metal substrate that is made of at least two metal compositions, a functional insert and a surrounding body that surrounds the functional insert. In a preferred embodiment of the invention a functional insert powder composition of loose powder metal is placed in a compact of a surrounding body powder composition and both metal compositions are sintered in a sintering furnace to form a sintered part. The sintered part is infiltrated in part or in whole with a molten metal compound to produce a functionally graded metal substrate having a density of at least 90% of theoretical. A heat-generating component such as a chip can be attached to the metal substrate for use in microelectronic packaging. When the functionally-graded metal substrate has two discrete compositions of copper/tungsten the surrounding body which has a CTE that ranges from about 5.6ppm/.degree. C. to about 7 ppm/.degree. C. constrains the expansion of the functional insert which has a thermal conductivity that ranges from about 200 W/mK to about 400 W/mK.
摘要翻译：本发明提供了由至少两种金属组合物制成的功能梯度金属基底，功能性插入物和围绕功能性插入物的周围体。在本发明的优选实施方案中，将松散粉末金属的功能性插入粉末组合物放置在周围体粉末组合物的压块中，并且两种金属组合物在烧结炉中烧结以形成烧结部件。烧结部分部分或全部渗入熔融金属化合物，以产生密度至少为理论值的90％的功能梯度金属基材。诸如芯片的发热部件可以附接到用于微电子封装的金属基板。当功能梯度金属基底具有铜/钨的两个离散组成时，具有约5.6ppm /℃至约7ppm /℃的CTE的周围体约束了功能性插入物的膨胀，其具有热导率范围为约200W / mK至约400W / mK。

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