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1. 发明授权

US06635350B2 Polymeric 1,5- or 1,8-disubstituted anthraquinone-derivative colorants and articles comprising such colorants 有权
标题翻译：聚合1,5-或1,8-二取代的蒽醌衍生物着色剂和包含这种着色剂的制品
公开(公告)号：US06635350B2
公开(公告)日：2003-10-21
申请号：US09981279
申请日：2001-10-16
申请人： Daniel M. Connor , John W. Miley, Jr.
发明人： Daniel M. Connor , John W. Miley, Jr.
IPC分类号： B32B900
CPC分类号： C09D11/037 , C08G65/2627 , C08G65/331 , C08G65/3317 , C08K5/0041 , C08K5/18 , C09B69/00 , Y10T428/31504 , Y10T428/31786 , Y10T428/31855
摘要： Red colorants comprising a chromophore having at least one poly(oxyalkylene) chain attached to the 1-position, as well as at least one poly(oxyalkylene) chain attached to either the 5-position or the 8-position of an anthraquinone backbone are provided. Such colorants exhibit excellent base stability, effective colorations, excellent low extraction rates, and high lightfastness levels, particularly when incorporated within certain media and/or on the surface of certain substrates, particularly polyesters. The poly(oxyalkylene) chains also increase the solubility in different solvents or resins thereby permitting the introduction of such excellent coloring chromophores within diverse media and/or diverse substrates as well as provides a liquid colorant which facilitates handling. Compositions and articles comprising such colorants are provided as well as methods for producing such inventive colorants are also provided.
摘要翻译：提供了包含具有至少一个连接到1-位的聚（氧化烯）链的发色团的红色着色剂以及连接到蒽醌主链的5-位或8-位的至少一个聚（氧化烯）链。这些着色剂表现出优异的碱稳定性，有效着色，优异的低提取速率和高耐光性水平，特别是当结合到某些介质和/或某些基材，特别是聚酯的表面上时。聚（氧化烯）链还增加了在不同溶剂或树脂中的溶解度，从而允许在不同的介质和/或不同的基底内引入这些优异的着色发色团，并提供便于处理的液体着色剂。提供了包含这种着色剂的组合物和制品，并且还提供了制备这种本发明着色剂的方法。

2. 发明授权

US5973043A Carbamoyl substituted acetals and compositions containing the same 失效
标题翻译：氨基甲酰基取代的缩醛和含有它们的组合物
公开(公告)号：US5973043A
公开(公告)日：1999-10-26
申请号：US130921
申请日：1997-11-26
申请人： John W. Miley , C. Charles Carroll , John G. Lever , Nathan A. Mehl , Joseph M. Salley
发明人： John W. Miley , C. Charles Carroll , John G. Lever , Nathan A. Mehl , Joseph M. Salley
IPC分类号： C07D493/04 , C08K5/00 , C08K5/205 , C08L101/00 , C08J3/00 , C07D323/04 , C08K5/16 , C08L23/00
CPC分类号： C07D493/04 , C08K5/0008 , C08K5/0083 , C08K5/205
摘要： A diacetal of a polyhydric alcohol is provided having at least one carbamoyl substituent bonded to an oxy group of the alcohol. The compound is useful as a nucleating agent in polymer resins and as a gelling agent.
摘要翻译：提供了具有至少一个与醇的氧基键合的氨基甲酰取代基的多元醇的二缩醛。该化合物可用作聚合物树脂和胶凝剂中的成核剂。

3. 发明授权

US4985546A Polyoxylalkylene amino diol substituted colorants 失效
标题翻译：聚氧乙烯基氨基二醇取代的着色剂
公开(公告)号：US4985546A
公开(公告)日：1991-01-15
申请号：US371907
申请日：1989-06-19
申请人： John W. Miley , John W. Rekers
发明人： John W. Miley , John W. Rekers
IPC分类号： C07C217/08 , C07D317/22 , C07D319/06 , C08G18/50 , C08G59/50 , C08G65/26 , C08G65/322 , C08G65/325 , C08G65/338 , C09B69/00
CPC分类号： C07C217/08 , C07D317/22 , C07D319/06 , C08G18/5021 , C08G59/504 , C08G65/2606 , C08G65/322 , C08G65/3255 , C08G65/338 , C09B69/00 , Y10S534/03
摘要： A substituted colorant which may be copolymerized with a condensation polymer to provide a covalently bound, nonextractable coloring, having the formula ##STR1## wherein R and R.sub.1 are independently selected from hydrogen or lower alkyl; R.sub.4 is selected from hydrogen or lower alkyl; x is 0 or 1; N and M are each integers of from 1 to about 100 and the sum of N and M is from 3 to about 100. The hydroxyl groups are protected by formation of a ring structure during alkoxylation and amination of the substituent.
摘要翻译：可以与缩聚物共聚以提供共价结合的不可萃取着色的取代的着色剂，其具有下式：其中R和R 1独立地选自氢或低级烷基; R4选自氢或低级烷基; x为0或1; N和M各自为1至约100的整数，N和M的总和为3至约100.羟基在取代基的烷氧基化和胺化期间通过形成环结构来保护。

4. 发明授权

US4977281A Polyoxyalkylene amino alcohols and polyoxyalkylene amino 1,3-dioxanes and 1,3-dioxolanes 失效
标题翻译：聚氧化烯氨基醇和聚氧化烯氨基1,3-二恶烷和1,3-二氧戊环
公开(公告)号：US4977281A
公开(公告)日：1990-12-11
申请号：US135421
申请日：1987-12-21
申请人： John W. Miley , John W. Rekers
发明人： John W. Miley , John W. Rekers
IPC分类号： C07C217/08 , C07D317/22 , C07D319/06 , C08G18/50 , C08G59/50 , C08G65/26 , C08G65/32 , C08G65/322 , C08G65/325 , C08G65/338 , C09B69/00 , C09B69/10
CPC分类号： C07D317/22 , C07C217/08 , C07D319/06 , C08G18/5021 , C08G59/504 , C08G65/2606 , C08G65/322 , C08G65/3255 , C08G65/338 , C09B69/00
摘要： Primary amino polyoxyalkylene 1,3-dioxane or 1,3-dioxolane compounds are provided of the formula: ##STR1## wherein R and R.sub.1 are independently selected from hydrogen or a lower alkyl group; R.sub.2 and R.sub.3 are independently selected from hydrogen, phenyl or lower alkyl groups; R.sub.4 is selected from hydrogen or a lower alkyl group; x is 0 or 1; N and M are each integers of from 1 to about 100 and the sum of N an M is from 2 to about 100; also disclosed are polyoxyalkylene amino alcohol compounds which may be derived from the compounds of Formula I above having the formula: ##STR2## wherein R, R.sub.1, R.sub.4, x, N and M all have the values given above. Also provided is a process for preparing a primary amino polyoxyalkylene 1,3-dioxane or 1,3-dioxolane.

5. 发明授权

US4846996A Liquid, non-crystallizing two mole diphenol alkoxylate mixtures 失效
标题翻译：液体，非结晶的两摩尔二酚烷氧基化物混合物
公开(公告)号：US4846996A
公开(公告)日：1989-07-11
申请号：US154697
申请日：1988-02-11
申请人： Clifford C. Carroll , John W. Miley , Richard A. Van Dahm
发明人： Clifford C. Carroll , John W. Miley , Richard A. Van Dahm
IPC分类号： C07C43/23 , C07C323/20 , C08G18/10 , C08G63/547
CPC分类号： C08G63/547 , C07C323/20 , C07C43/23 , C08G18/10
摘要： A mixture of diphenols is provided of the general formula: ##STR1## wherein the mixture comprises three components as follows; (a) from about 2% to about 35% by weight of compound A corresponding to formula (I) wherein R.sub.1 and R.sub.6 are H; R.sub.2, R.sub.3, R.sub.4 and R.sub.5 are selected from H and Br; and --X-- is selected from CH.sub.3 --C--CH.sub.3, --S--, or --O--;(b) from about 15% to about 50% by weight of compound B corresponding to formula (I) wherein R.sub.1 is H; R.sub.6 is CH.sub.3 ; R.sub.2, R.sub.3, R.sub.4, R.sub.5 are selected from H or Br; and --X-- is selected from CH.sub.3 --C--CH.sub.3, --S--, or --O--; and(c) from about 15% to about 80% by weight of compound C corresponding to formula (I) wherein R.sub.1 and R.sub.6 are CH.sub.3 ; R.sub.2, R.sub.3, R.sub.4 and R.sub.5 are selected from H or Br; and --X-- is selected from CH.sub.3 --C--CH.sub.3, --S--, or --O--.
摘要翻译：提供了以下通式的二酚的混合物：其中混合物包含如下三种组分：（a）约2％至约35％重量的对应于其中R 1和R 6为H的式（I）的化合物A; R2，R3，R4和R5选自H和Br; 和-X-选自CH 3 -CH 3，-S-或-O-; （b）约15％至约50％重量的对应于其中R 1为H的式（I）的化合物B; R6是CH3; R2，R3，R4，R5选自H或Br; 和-X-选自CH 3 -CH 3，-S-或-O-; 和（c）约15％至约80％重量的对应于其中R 1和R 6为CH 3的式（I）的化合物C; R2，R3，R4和R5选自H或Br; 和-X-选自CH 3 -CH 3，-S-或-O-。

6. 发明授权

US06667392B2 Polymeric acetoacetanilide azo colorants 有权
公开(公告)号：US06667392B2
公开(公告)日：2003-12-23
申请号：US09994031
申请日：2001-11-21
申请人： Jusong Xia , Eric B. Stephens , Mary G. Mason , John W. Miley , Leonard J. Starks , Eugene K. Stephenson
发明人： Jusong Xia , Eric B. Stephens , Mary G. Mason , John W. Miley , Leonard J. Starks , Eugene K. Stephenson
IPC分类号： C07C24508
CPC分类号： C09B69/00
摘要： This invention relates to colorants comprising a chromophore having a single azo acetoacetanilide moiety, wherein said moiety each have at least one poly(oxyalkylene) chain. Such colorants exhibit extremely good base stability and lightfastness, particularly when incoporated within certain media and/or on the surface of certain substrates. These poly(oxyalkylene) chains provide solubility in different solvents or resins thereby permitting the introduction of such excellent coloring chromophores within diverse media and/or or diverse substrates. Compositions and articles comprising such colorants are provided as are methods for producing such inventive colorants.

7. 发明授权

US5919846A Colorant having isocyanate substituent 失效
标题翻译：具有异氰酸酯取代基的着色剂
公开(公告)号：US5919846A
公开(公告)日：1999-07-06
申请号：US25824
申请日：1998-02-19
申请人： Raj Batlaw , John W. Miley
发明人： Raj Batlaw , John W. Miley
IPC分类号： C08G18/10 , C08G18/38 , C09B69/00 , C09D11/00 , D06P1/00 , D06P1/02 , D06P1/13 , D06P1/14 , D06P1/39 , D06P5/30 , C08G18/02
CPC分类号： D06P5/30 , C08G18/10 , C08G18/38 , C09B69/00 , C09D11/32 , D06P1/0052 , D06P1/02 , D06P1/13 , D06P1/14 , D06P1/39
摘要： A novel colorant compound is provided which is the addition product of an organic chromophore having at least one reactive hydroxyl or amine substituent, a polyisocyanate, and a carboxylic acid, sulfonic acid, or salt of either thereof. The polyisocyanate, added in a molar excess relative to the number of such reactive substituents, reacts with the reactive hydroxyl or amine groups to provide terminal isocyanate groups. Subsequently, the carboxylic acid or salt thereof, also added in an amount excessive in relation to the number of terminal isocyanate groups, reacts therewith to from urethane moieties on the colorant. Such a compound provides excellent ink compositions upon dilution and are very soluble within all the standard ink diluents. Furthermore, such colorants provide good jettability, waterfastness, washfastness, and the like, within ink-jet applications on various types of printing substrates. A method for producing such a colorant and specifically printed substrates colored therewith is also provided.
摘要翻译：提供了一种新的着色剂化合物，其是具有至少一个反应性羟基或胺取代基的有机发色团，多异氰酸酯，和其任一种的羧酸，磺酸或其盐的加成产物。加入摩尔过量的多异氰酸酯相对于这些反应性取代基的数目与反应性羟基或胺基反应以提供端基异氰酸酯基团。随后，相对于末端异氰酸酯基团的数量加入过量的羧酸或其盐与着色剂上的氨基甲酸酯部分反应。这种化合物在稀释时提供优异的油墨组合物，并且在所有标准油墨稀释剂中都非常可溶。此外，这些着色剂在各种类型的印刷基材上的喷墨应用中提供良好的可喷射性，耐水性，耐洗涤性等。还提供了制备这种着色剂的方法和用其着色的特定印刷基板。

8. 发明授权

US4846846A Process for preparing polyurethane resins colored with anthraquinone colorants and products produced thereby 失效
标题翻译：制备用蒽醌着色剂着色的聚氨酯树脂和由此生产的产品的方法
公开(公告)号：US4846846A
公开(公告)日：1989-07-11
申请号：US210887
申请日：1988-06-20
申请人： John W. Rekers , John W. Miley
发明人： John W. Rekers , John W. Miley
IPC分类号： C09B1/28 , C08G18/30 , C08G18/32 , C08G18/38 , C08G18/48 , C08G18/50 , D06P3/24
CPC分类号： C08G18/50 , C08G18/38 , D06P3/248 , Y10S8/926
摘要： A process for coloring polyurethane resins made by a polyaddition reaction of a polyol and an isocyanate is provided, which comprises adding to the reaction mixture before or during the polyaddition reaction a reactive coloring agent suitable for incorporation in the resin with the formation of covalent bonds, said coloring agent having the formula: ##STR1## in which R.sub.1 and R.sub.2 are independently selected from an alkyl group having from 1 to about 12 carbon atoms, X is --CH.sub.2 --, a and a' are integers from 1 to about 6, and Y and Y' are independently selected from polymeric units of hydroxy alkylenes or alkylene oxide monomers selected from ethylene oxide, propylene oxide, butylene oxide, cyclohexene oxide, or glycidol, b and b' are independently either 0 or 1, and Z and Z' are reactive groups independently selected from --OH, --NH.sub.2, or --SH.

9. 发明授权

US4310644A Vinyl ester resin compositions 失效
标题翻译：乙烯基酯树脂组合物
公开(公告)号：US4310644A
公开(公告)日：1982-01-12
申请号：US178149
申请日：1980-08-14
申请人： John W. Miley
发明人： John W. Miley
IPC分类号： C08F299/00 , C08F290/00 , C08G59/00 , C08L63/00 , C08L63/10
CPC分类号： C08L63/10
摘要： A vinyl ester resin composition having excellent physical, mechanical and handling properties is provided which comprises: a vinyl ester resin made by condensing an epoxy resin and an ethylenically unsaturated monocarboxylic acid; and a thixotropy imparting amount of a thixotropy imparting material selected from at least one condensation product of a sugar alcohol with an aromatic aldehyde.
摘要翻译：提供了具有优异的物理，机械和处理性能的乙烯基酯树脂组合物，其包括：通过使环氧树脂和烯属不饱和一元羧酸缩合制备的乙烯基酯树脂; 以及赋予触变性量的触变性赋予材料，其选自至少一种糖醇与芳族醛的缩合产物。

10. 发明授权

US06500935B2 Aromatic bis-acetoacetamide intermediates 失效
公开(公告)号：US06500935B2
公开(公告)日：2002-12-31
申请号：US09994085
申请日：2001-11-21
申请人： Jusong Xia , John W. Miley
发明人： Jusong Xia , John W. Miley
IPC分类号： C09B33153
CPC分类号： C09B33/153
摘要： Specific novel compounds of aromatic bis-acetoamide structures are provided as intermediate compounds to forming different types of coloring agents, at least. Such compounds are useful as intermediates in the production of certain bis-acetoanilide azo dyes, pigments, and polymeric colorants. Such compounds facilitate production of such coloring agents that exhibit favorable tinctorial strength and intense color from orange to greenish yellow within and on different substrates and media. Coloring agents and methods of making such agents are encompassed within this invention as well.

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