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1. 发明授权

US06841641B2 Copolymers comprising low surface tension (meth) acrylates 失效
标题翻译：包含低表面张力（甲基）丙烯酸酯的共聚物
公开(公告)号：US06841641B2
公开(公告)日：2005-01-11
申请号：US10237357
申请日：2002-09-09
申请人： Kurt G. Olson , Simion Coca , James B. O'Dwyer , Joanne H. Smith
发明人： Kurt G. Olson , Simion Coca , James B. O'Dwyer , Joanne H. Smith
IPC分类号： C08F220/10 , C08F20/22 , C08F220/22 , C08F230/08
CPC分类号： C08F220/10
摘要： The present invention is directed to a copolymer that includes a first radically polymerizable low surface tension (meth)acrylate monomer and one or more other radically polymerizable ethylenically unsaturated monomers. The copolymer has a polydispersity index of less than 2.5. The present invention further includes a controlled radical polymerization method to make the above described low surface tension containing copolymers. The method includes the steps of adding a first radically polymerizable low surface tension (meth)acrylate monomer and one or more other radically polymerizable ethylenically unsaturated monomers to a solution containing a suitable atom transfer radical polymerization (ATRP) initiator.
摘要翻译：本发明涉及包含第一自由基聚合性低表面张力（甲基）丙烯酸酯单体和一种或多种其它可自由基聚合的烯属不饱和单体的共聚物。共聚物的多分散指数小于2.5。本发明还包括制备上述低表面张力共聚物的受控自由基聚合方法。该方法包括将第一自由基聚合性低表面张力（甲基）丙烯酸酯单体和一种或多种其它可自由基聚合的烯属不饱和单体加入到含有合适的原子转移自由基聚合（ATRP）引发剂的溶液中的步骤。

2. 发明申请

US20080255307A1 Copolymers comprising low surface tension (meth)acrylates 审中-公开
标题翻译：包含低表面张力（甲基）丙烯酸酯的共聚物
公开(公告)号：US20080255307A1
公开(公告)日：2008-10-16
申请号：US12132928
申请日：2008-06-04
申请人： Kurt G. Olson , Simion Coca , James B. O'Dwyer , Joanne H. Smith
发明人： Kurt G. Olson , Simion Coca , James B. O'Dwyer , Joanne H. Smith
IPC分类号： C08G63/00
CPC分类号： C08F220/10
摘要： The present invention is directed to a copolymer that includes a first radically polymerizable low surface tension (meth)acrylate monomer and one or more other radically polymerizable ethylenically unsaturated monomers. The copolymer has a polydispersity index of less than 2.5. The present invention further includes a controlled radical polymerization method to make the above described low surface tension containing copolymers. The method includes the steps of adding a first radically polymerizable low surface tension (meth)acrylate monomer and one or more other radically polymerizable ethylenically unsaturated monomers to a solution containing a suitable atom transfer radical polymerization (ATRP) initiator.
摘要翻译：本发明涉及包含第一自由基聚合性低表面张力（甲基）丙烯酸酯单体和一种或多种其它可自由基聚合的烯属不饱和单体的共聚物。共聚物的多分散指数小于2.5。本发明还包括制备上述低表面张力共聚物的受控自由基聚合方法。该方法包括将第一自由基聚合性低表面张力（甲基）丙烯酸酯单体和一种或多种其它可自由基聚合的烯属不饱和单体加入到含有合适的原子转移自由基聚合（ATRP）引发剂的溶液中的步骤。

3. 发明授权

US06586530B1 Low surface tension (meth) acrylate containing block copolymer prepared by controlled radical polymerization 失效
标题翻译：通过控制自由基聚合制备的含低级表面张力（甲基）丙烯酸酯的嵌段共聚物
公开(公告)号：US06586530B1
公开(公告)日：2003-07-01
申请号：US09965546
申请日：2001-09-27
申请人： Jonathan D. Goetz , Kurt A. Humbert , Karl F. Schimmel , Karen A. Barkac , Simion Coca , Joanne H. Smith
发明人： Jonathan D. Goetz , Kurt A. Humbert , Karl F. Schimmel , Karen A. Barkac , Simion Coca , Joanne H. Smith
IPC分类号： C08F25900
CPC分类号： C08F293/005 , C08F2438/01
摘要： A block copolymer including a block of residues of a low surface tension (meth)acrylate monomer; a block of residues of a monomer free of hydroxyl group and amine group residues; and, optionally, a third block of residues of a monomer free of hydroxyl groups and amine groups. The first, second and third blocks are made of different residues from each other and the block copolymer has a polydispersity index of less than 2.5. A controlled radical polymerization method is disclosed to make the low surface tension block copolymers. The method includes the steps of sequentially adding a first monomer composition that is free of hydroxyl groups and amine groups and a second monomer composition that includes the low surface tension monomer to a suitable atom transfer radical polymerization initiator and polymerizing the monomer compositions to form a block copolymer.
摘要翻译：包含低表面张力（甲基）丙烯酸酯单体的残基的嵌段的嵌段共聚物; 一个不含羟基和胺基残基的单体的残基块; 和任选地，不含羟基和胺基的单体的第三组残基。第一，第二和第三嵌段由彼此不同的残基组成，嵌段共聚物的多分散指数小于2.5。公开了一种控制自由基聚合方法来制备低表面张力嵌段共聚物。该方法包括以下步骤：将不含羟基和胺基的第一单体组合物和包含低表面张力单体的第二单体组合物顺序加入到合适的原子转移自由基聚合引发剂中并聚合单体组合物以形成嵌段共聚物。

4. 发明授权

US06583223B2 Coating compositions which contain a low surface tension (meth) acrylate containing block copolymer flow control agent 失效
标题翻译：含有低表面张力（甲基）丙烯酸酯的嵌段共聚物流动控制剂的涂料组合物
公开(公告)号：US06583223B2
公开(公告)日：2003-06-24
申请号：US09965547
申请日：2001-09-27
申请人： Jonathan D. Goetz , Kurt A. Humbert , Karl F. Schimmel , Karen A. Barkac , Simion Coca , Joanne H. Smith
发明人： Jonathan D. Goetz , Kurt A. Humbert , Karl F. Schimmel , Karen A. Barkac , Simion Coca , Joanne H. Smith
IPC分类号： C08L5300
CPC分类号： C08F293/005
摘要： A thermosetting composition that includes a first reactant having functional groups; a second reactant having functional groups coreactive with the functional groups of the first reactant; and a block copolymer flow control agent. The block copolymer includes a first block made up of residues of a radically polymerizable fluoroalkyl(meth)acrylate monomer, a second block made up of residues of a second radically polymerizable ethylenically unsaturated monomer, and optionally a third block made up of residues of a third radically polymerizable ethylenically unsaturated monomer. The first, second and third blocks are made of different residues from each other and the block copolymer has a polydispersity index of less than 2.5. Also disclosed is a method of coating a substrate including the steps of applying the present thermosetting composition to the substrate; coalescing the thermosetting composition to form a substantially continuous film; and curing said thermosetting composition by the application of heat.
摘要翻译：一种热固性组合物，其包含具有官能团的第一反应物; 具有与第一反应物的官能团起核心作用的官能团的第二反应物; 和嵌段共聚物流动控制剂。嵌段共聚物包括由可自由基聚合的（甲基）丙烯酸烷基酯单体的残基构成的第一嵌段，由第二可自由基聚合的烯键式不饱和单体的残基构成的第二嵌段，以及任选地由第三个可自由基聚合的烯属不饱和单体。第一，第二和第三嵌段由彼此不同的残基组成，嵌段共聚物的多分散指数小于2.5。还公开了一种涂覆基材的方法，包括以下步骤：将本发明的热固性组合物施用于基材; 聚合该热固性组合物以形成基本连续的膜; 并通过加热来固化所述热固性组合物。

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