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1. 发明授权

US4305766A Gelled aqueous slurry explosives containing gas bubbles 失效
标题翻译：含有气泡的凝胶含水浆液炸药
公开(公告)号：US4305766A
公开(公告)日：1981-12-15
申请号：US89531
申请日：1979-10-29
申请人： Anthony C. F. Edmonds , Jitka Kirchnerova , Terrence C. Matts , Joseph R. J. Pare
发明人： Anthony C. F. Edmonds , Jitka Kirchnerova , Terrence C. Matts , Joseph R. J. Pare
IPC分类号： C06B47/14 , C06B45/00
CPC分类号： C06B47/14
摘要： An improved method of gassing an aqueous slurry explosive composition with an inorganic nitrite gassing agent is provided. The method makes use of a thiocyanate ion-containing material in the composition as a gassing accelerator. The presence of the thiocyanate ion produces improved rate and quantity of gas generation even under low temperature where gas generation is normally retarded.
摘要翻译：提供了一种利用无机亚硝酸盐放气剂对含水浆料炸药组合物进行放气的改进方法。该方法在组合物中使用含硫氰酸根离子的材料作为气体加速器。硫氰酸根离子的存在即使在气体产生通常延迟的低温下也能产生改善的气体产生速率和数量。

2. 发明授权

US4842698A Solid state arsenic probe for use in pyrometallurgical processes 失效
标题翻译：用于火法冶金工艺的固态砷探针
公开(公告)号：US4842698A
公开(公告)日：1989-06-27
申请号：US52027
申请日：1987-05-19
申请人： Jitka Kirchnerova , James M. Skeaff , Christopher W. Bale
发明人： Jitka Kirchnerova , James M. Skeaff , Christopher W. Bale
IPC分类号： G01N27/407 , G01N27/413 , G01N27/49
CPC分类号： G01N27/4074 , G01N27/4045
摘要： A potentiometric electrochemical sensor for detecting gaseous concentrations of arsenic oxides or arsenic-bearing species at elevated temperatures. The sensor is comprised of: an ionically conducting solid state membrane which may be made of silver zirconium arsenate, sodium beta-alumina or silver beta-alumina; a reference electrode which may be silver wire packed in silver powder; and a working electrode which may consist of a platinum mesh electrode or a silver wire exposed to the arsenic oxide-bearing gas. The probe is responsive to arsine [AsH.sub.3 ] concentrations in the range 5-1000 ppm in oxidizing gases, such as air, which have been raised to the temperature range 600.degree.-900.degree. C. The compound silver zirconium arsentate is also novel.
摘要翻译：一种用于在升高的温度下检测砷氧化物或含砷物质的气体浓度的电位电化学传感器。传感器包括：离子导电固态膜，其可由砷酸银锆，β-氧化铝或银β-氧化铝制成; 参考电极，其可以是银线包装在银粉中; 以及可以由暴露于含有氧化砷的气体的铂网电极或银线构成的工作电极。该探针响应于氧化性气体例如空气中的5-1000ppm范围内的砷砷[AsH 3]浓度已经升高到600-900℃的温度范围。化合物银锆砷酸盐也是新颖的。

3. 发明授权

US5981445A Process of making fine ceramic powders from aqueous suspensions 失效
标题翻译：从水性悬浮液制备精细陶瓷粉末的工艺
公开(公告)号：US5981445A
公开(公告)日：1999-11-09
申请号：US668422
申请日：1996-06-17
申请人： Jitka Kirchnerova , Danilo Klvana
发明人： Jitka Kirchnerova , Danilo Klvana
IPC分类号： B01J23/00 , B01J37/32 , C01B13/14 , C01G3/00 , C01G37/00 , C01G53/00 , C04B35/45 , C04B35/50 , H01L39/00 , C01F17/00
CPC分类号： C04B35/50 , B01J23/002 , B01J37/32 , C01B13/14 , C01G3/006 , C01G37/006 , C01G51/68 , C04B35/4508 , B01J2523/00 , C01P2002/34 , C01P2002/54 , C01P2002/72 , C01P2002/88 , C01P2006/12 , C01P2006/60 , Y10S977/776
摘要： The new preparation process for making fine high specific surface ceramic powders suitable as catalysts or precursors for ceramics uses lanthanum (or other rare earth lanthanide) oxide as one of the precursors. The oxide is mixed with water to form a liquid slurry, whereby it is transformed to the hydroxide by reaction with water. The resulting hydroxide slurry, which can be milled to reduce the particle size and to speed up the reaction, is then combined, while stirring vigorously to assure homogenous mixing, with a solution of required amount of remaining metal nitrate precursors, for example strontium and cobalt nitrates. The reaction between lanthanum hydroxide and transition metal nitrates produces a colored (color depending on the transition metal) slurry consisting of metal hydroxides suspended in aqueous nitrate solution with pH>2. This perovskite precursor slurry is spray-frozen and freeze dried. The freeze-dried material is transformed to perovskite by slow controlled calcination at temperatures above 550.degree. C. For example calcination 12 h at 585.degree. C. and subsequently 4 h at 620.degree. C. produces nearly phase pure perovskite having specific surface area of >10 m.sup.2 /g, depending on the composition. The perovskite precursor slurry can alternatively be processed first by spray-drying (instead of spray-freezing/freeze-drying) and subsequent calcination.
摘要翻译：用于制备适合作为陶瓷或催化剂前体的精细高比表面陶瓷粉末的新制备方法使用镧（或其它稀土镧系元素）氧化物作为前体之一。将氧化物与水混合以形成液体浆料，由此通过与水反应将其转化为氢氧化物。然后将所得氢氧化物淤浆（其可以研磨以减小粒度和加速反应）合并，同时剧烈搅拌以确保均匀混合，与所需量的剩余的金属硝酸盐前体（例如锶和钴）的溶液硝酸盐氢氧化镧和过渡金属硝酸盐之间的反应产生悬浮在pH> 2的硝酸盐水溶液中的金属氢氧化物组成的着色（颜色取决于过渡金属）浆料。将该钙钛矿前体浆液喷雾冷冻并冷冻干燥。通过在高于550℃的温度下缓慢控制煅烧将冷冻干燥的材料转化为钙钛矿。例如在585℃下煅烧12小时，随后在620℃煅烧4小时，产生几乎相纯的钙钛矿，比表面积> 10 m2 / g，取决于组成。另外可以通过喷雾干燥（代替喷雾冷冻/冷冻干燥）和随后的煅烧来首先处理钙钛矿前体浆料。

4. 发明授权

US4198253A Explosive compositions containing sulphonated guar gum derivatives 失效
标题翻译：含有磺化瓜耳胶衍生物的爆炸组合物
公开(公告)号：US4198253A
公开(公告)日：1980-04-15
申请号：US968560
申请日：1978-12-11
申请人： Jitka Kirchnerova , Errol L. Falconer
发明人： Jitka Kirchnerova , Errol L. Falconer
IPC分类号： C06B47/14 , C06B33/02
CPC分类号： C06B47/14
摘要： A slurry explosive composition is provided which has improved water resistance and thermal stability and resists segregation. The composition consists of an inorganic oxygen-supplying salt, a liquid carrier or solvent for the salt, a solid or liquid fuel and, as a thickener a sulfonated guar gum derivative.
摘要翻译：提供了一种具有改善的耐水性和热稳定性并且抗偏析的浆料炸药组合物。该组合物由无机供氧盐，用于盐的液体载体或溶剂，固体或液体燃料和作为增稠剂的磺化瓜尔胶衍生物组成。

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