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1. 发明授权

US3929895A 4-Acetyl-2,3-dimethyl-6-isopropenylmethyl-cyclohexene 失效
标题翻译： 4-乙酰基-2,3-二甲基-6-异丙烯基甲基 - 环己烯
公开(公告)号：US3929895A
公开(公告)日：1975-12-30
申请号：US46275074
申请日：1974-04-22
申请人： INT FLAVORS & FRAGRANCES INC
发明人： HALL JOHN B
IPC分类号： C11B9/00 , C07C49/61
CPC分类号： C11B9/0046 , C07C45/75 , C07C49/557 , C07C403/02 , C07C2601/16 , C11B9/0034 , C07C47/45 , C07C49/553
摘要： AND (III) AND A MIXTURE OF COMPOUNDS HAVING THE

II. A mixture of compounds having the structure:

A superatmospheric process for directly producing a Diels-Alder adduct which comprises admixing: I. A conjugated diene which can be either alpha-terpinene, alloocimene, cyclopentadiene or myrcene; with II. A carbonyl group-containing compound which can be either acetone, acetaldehyde propionaldehyde or methylethyl ketone; with III. An aldehyde source which can be either a formaldehyde source or an acetaldehyde source which aldehyde source will yield formaldehyde or acetaldehyde; in the presence of IV. A secondary amine catalyst such as a lower dialkyl amine or a cyclic amine such as morpholine, pyrrolidine or piperidine, AT A TEMPERATURE IN THE RANGE OF FROM ABOUT 120*C up to about 200*C for a period of time from about 2 hours up to about 8 hours, and novel products produced therefrom to wit: I. A mixture of compounds having the structures:
摘要翻译：用于直接生产Diels-Alder加合物的超大气压法，其包括：

2. 发明授权

US3928645A Enhancing red-berry flavor with 4-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-2-butanone and 4-(6,6-dimethyl-2-methylene-3-cyclohexen-1-yl)-2-butanone 失效
标题翻译：用4-（2,6,6-三甲基-1,3-环己二烯-1-基）-2-丁酮和4-（6,6-二甲基-2-亚甲基-3-环己烯-1） - 基）-2-丁酮
公开(公告)号：US3928645A
公开(公告)日：1975-12-23
申请号：US46274874
申请日：1974-04-22
申请人： INT FLAVORS & FRAGRANCES INC
发明人： MOOKHERJEE BRAJA DULAL , TRENKLE ROBERT WALTER , VOCK MANFRED HUGO , SHUSTER EDWARD J
IPC分类号： A23L27/20 , A24B3/12 , A24B15/34 , A61K8/30 , A61K8/33 , A61K8/35 , A61K8/37 , A61Q13/00 , C07C67/00 , C07C401/00 , C07C403/16 , C11B9/00 , C11D3/50 , C12G3/06 , A23L1/235
CPC分类号： C12G3/06 , A23L27/203 , A24B15/34 , C11B9/0034
摘要： Methods for preparing foodstuffs, flavoring compositions for foodstuffs, tobacco compositions, flavoring compositions for tobacco, perfume compositions and ingredients for perfume compositions by including therein 4-(2,6,6-trimethyl-1,3cyclohexadien-1-yl)-2-butanone or 4-(6,6-dimethyl-2-methylene-3cyclohexen-1-yl)-2-butanone to produce: A. In food flavorings, raspberry, waxey, tobacco, rosey, ionone flavor notes or combinations of these and woody, tobacco, floral aroma notes for improving the taste and aroma of artificial strawberry, or other red berry (e.g., raspberry) flavoring compositions; B. In perfumes, a sweet, fruity, woody, berry ''''mimosa'''' character as well as the foodstuff flavoring compositions and perfume compositions containing 4-(2,6,6-trimethyl-1,3cyclohexadien-1-yl)-2-butanone and/or 4-(6,6-dimethyl-2methylene-3-cyclohex-1-yl)-2-butanone; and C. In tobaccos, natural, sweet, oily notes.
摘要翻译：制备食品的方法，食品调味组合物，烟草组合物，烟草调味组合物，香料组合物和用于香料组合物的成分，其中包括4-（2,6,6-三甲基-1,3-环己二烯-1-基） - 2-丁酮或4-（6,6-二甲基-2-亚甲基-3-环己烯-1-基）-2-丁酮制备：

3. 发明授权

US3928248A Fragrance materials containing 4-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-2-butanol and/or 4-(6,6-dimethyl-2-methylene-3-cyclo-hexen-1-yl)-2-butanol, and/or acetals thereof, and methods for producing same 失效
标题翻译：含有4-（2,6,6-三甲基-1,3-环己二烯-1-基）-2-丁醇和/或4-（6,6-二甲基-2-亚甲基-3-环己烯）哌啶-1-基）-2-丁醇，和/或其缩醛，及其制备方法
公开(公告)号：US3928248A
公开(公告)日：1975-12-23
申请号：US56118875
申请日：1975-03-24
申请人： INT FLAVORS & FRAGRANCES INC
发明人： MOOKHERJEE BRAJA DULAL , VOCK MANFRED HUGO , BENAIM CARLOS , SHUSTER EDWARD J
IPC分类号： A23L27/20 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0034 , A23L27/203 , Y10S585/947
摘要： Methods for preparing perfume compositions and ingredients for perfume compositions by including therein 4-(2,6,6-trimethyl-1,3cyclohexadien-1-yl)-2-butanol or 4-(6,6-dimethyl-2-methylene-3cyclohexen-1-yl)-2-butanol or acetals thereof to produce in perfumes, a leathery, green, orris, seashore, mimosa, clary sage, woody, fruity, ionone character with a slight musky nuance.
摘要翻译：通过在其中包含4-（2,6,6-三甲基-1,3-环己二烯-1-基）-2-丁醇或4-（6,6-二甲基-2-丙醇）的香料组合物制备香料组合物和成分的方法，亚甲基-3-环己烯-1-基）-2-丁醇或其缩醛，以在香料，革质，绿色，orris，海滨，含羞草，谷类，木本，水果，紫罗兰酮的性质中产生轻微的麝香。

4. 发明授权

US3927083A Bicyclic compounds and processes for making and using same 失效
标题翻译：双环化合物及其制备和使用方法
公开(公告)号：US3927083A
公开(公告)日：1975-12-16
申请号：US41178973
申请日：1973-11-01
申请人： INT FLAVORS & FRAGRANCES INC
发明人： HALL JOHN B , LALA LEKHU KEWALRAM , BEETS MUUS G J , TAYLOR WILLIAM I
IPC分类号： C07C45/28 , C07C49/633 , C07C49/637 , A61K7/46
CPC分类号： C07C49/637 , C07C45/28 , C07C49/633 , C07C2602/24 , C11B9/0053
摘要： Bicyclic compounds containing four to six alkyl groups and having the formula:

WHEREIN THE DASHED LINE IS A SINGLE OR DOUBLE CARBON-TO-CARBON BOND; X is a carbonyl oxygen or two hydrogen atoms; Y is -CHR9or -CHR10-CHR11-; R1, R2, R3 and R4 are the same or different alkyl; R7, R8, R9, R10 and R11 are hydrogen or the same or different alkyl, R7 or R8 being alkyl when R9 is alkyl; R5 is not present and R6 is hydrogen when the dashed line is a double bond; and R5 and R6 are hydrogen, or taken together, form an oxirane ring when the dashed line is a single bond, together with methods of preparation for such bicyclic compounds, perfume compositions containing the compounds, and methods for altering aromas utilizing such compounds.
摘要翻译：含有四至六个烷基并具有下式的双环化合物：

5. 发明授权

US3920755A Process for producing alkenals and intermediates therefor 失效
标题翻译：生产枸杞子和其中间体的方法
公开(公告)号：US3920755A
公开(公告)日：1975-11-18
申请号：US51556974
申请日：1974-10-17
申请人： INT FLAVORS & FRAGRANCES INC
发明人： SCHREIBER WILLIAM L , PITTET ALAN O
IPC分类号： C11B9/00 , C07C43/30
CPC分类号： C07C45/45 , C07C45/004 , C07C45/515 , C07C45/62 , C07C45/67 , C11B9/0015 , C07C49/255 , C07C47/20 , C07C47/21
摘要： Processes for producing novel 2-alkylidene-3-alkynals and 2alkylidene-3-alkenals which comprise reacting an alkyl metallo acetylide with a dialkoxy acetonitrile or a dialkoxy dialkyl acetamide to form an imine salt, hydrolyzing the imine salt to form a 1,1-dialkoxy-3-alkyn-2-one, alternatively (a) first treating the alkynone with an alkylidene tri-substituted phosphorane or an alkylidene phosphorous triamide or an alkyl phosphoramide anionic compound to provide a dialkoxy alkylidene alkyne, and then either (1) hydrolyzing the dialkoxy alkylidene alkyne to form a novel aldehyde, an alkylidene alkynal, and if desired, reducing the triple bond of the alkylidene alkynal to a double bond to obtain the corresponding alkylidene alkenal or (2) first reducing the dialkoxy alkylidene alkyne to form a 1,1dialkoxy-2-alkylidene-3-alkene and if desired then hydrolyzing said 1,1-dialkoxy-2-alkylidene-3-alkene to form the desired 2alkylidene-3-alkenal; or (b) first reducing the alkynone to form a 1,1-dialkoxy-3-alken-2-one and then treating the 1,1-dialkoxy3-alken-2-one with an alkylidene tri-substituted phosphorane or an alkylidene phosphorous triamide or an alkyl phosphoramide anionic compound to provide a dialkoxy alkylidene alkene and, if desired, then hydrolyzing said dialkoxy alkylidene alkene to form the desired 2-alkylidene-3-alkenal; together with novel alkylidene alkynals and acetals thereof so produced.

6. 发明授权

US3917870A Enhancing grape flavor with 2-phenyl-3-carboethoxyfuran and bis (cyclohexyl) disulfide 失效
标题翻译：用2-苯基-3-乙氧羰基呋喃和双（环己基）二硫化物增强葡萄风味
公开(公告)号：US3917870A
公开(公告)日：1975-11-04
申请号：US51881874
申请日：1974-10-29
申请人： INT FLAVORS & FRAGRANCES INC
发明人： SLANGAN GARY , PITTET ALAN O , GIACINO CHRISTOPHER , HRUZA SR DENIS E , SHUSTER EDWARD J
IPC分类号： A23L27/20 , A23L27/29 , A24B15/34 , A24B15/40 , C11B9/00 , A23L1/235
CPC分类号： A24B15/34 , A23L27/203 , A23L27/2052 , A23L27/29 , A24B15/406 , C11B9/00
摘要： Methods for preparing foodstuffs, flavoring compositions for foodstuffs, perfume compositions, ingredients for perfume compositions, tobacco compositions and flavoring compositions for tobacco by including therein 2-phenyl-3-carboethoxyfuran and/or bis (cyclohexyl) disulfide to produce: A. In food flavorings, concord grape, wine, incense/fruity, pungent, sulfury (berry), minty, musty, weak sweet buttery, sweet carrot, dry woody cinnamon or warm benzaldehyde-nut like flavor notes or combinations of these and bitter after taste, benzoateester taste and heavy floral backnotes for improving the taste and aroma of artificial grape or other fruit flavoring compositions; B. In perfumes, a sweet, balsamic slightly nutty and sulfurous notes; and C. In tobacco flavorings, aromatic, sweet, resinous and balsamic-like notes as well as the foodstuff flavoring compositions, perfume compositions and tobacco compositions containing 2-phenyl-3-carboethoxyfuran and/or bis (cyclohexyl) disulfide. 2-Phenyl-3-carboethoxyfuran has the structure:

Bis (cyclohexyl) disulfide has the structure:
摘要翻译：用于制备食品的方法，食品调味组合物，香料组合物，用于香料组合物的成分，烟草组合物和用于烟草的调味组合物，其中包括2-苯基-3-乙氧羰基呋喃和/或双（环己基）二硫化物以产生：

7. 发明授权

US3908023A Imparting cinnamon-like flavor with certain 3-phenyl pentenal acetals 失效
标题翻译：用某些3-苯基戊烯醛缩醛赋予肉桂样风味
公开(公告)号：US3908023A
公开(公告)日：1975-09-23
申请号：US51495174
申请日：1974-10-15
申请人： INT FLAVORS & FRAGRANCES INC
发明人： SCHREIBER WILLIAM LEWIS , VOCK MANFRED , HALL JOHN B , SHUSTER EDWARD JOSEPH , QUINN ALTON DEWITT
IPC分类号： A23L27/20 , A24B15/30 , C07C45/51 , A23L1/226
CPC分类号： A24B15/301 , A23L27/204 , A23L27/2052
摘要： Foodstuff flavor and aroma augmenting compositions containing a quantity of at least one di-lower alkyl or lower alkylene acetal of a 3-phenyl pentenal sufficient to alter the aroma and/or organoleptic characteristics of said compositions, methods for preparing same, and foodstuff materials containing at least one of said acetals.
摘要翻译：含有足以改变所述组合物的香气和/或感官特征的3-苯基戊烯酸的至少一种二低级烷基或低级亚烷基缩醛的食品香料和香气增强组合物，其制备方法和含有至少一种所述缩醛。

8. 发明授权

US3907900A Stero configurations of 3((2-mercapto-1-methylpropyl)thio)-2-butanol 失效
标题翻译： 3（（2-巯基-1-甲基丙基）硫基）-2-丁醇的甾体构型
公开(公告)号：US3907900A
公开(公告)日：1975-09-23
申请号：US49989874
申请日：1974-08-23
申请人： INT FLAVORS & FRAGRANCES INC
发明人： EVERS WILLIAM JOHN , VOCK MANFRED HUGO , PELSE IGOR ALEXANDER
IPC分类号： A23C19/00 , A23L13/00 , A23L13/40 , A23L13/60 , A23L23/10 , A23L27/20 , A23L27/21 , A23L27/26 , A23L27/60 , B01J31/00 , C07B61/00 , C07C67/00 , C07C313/00 , C07C319/14 , C07C323/12 , C07C323/25 , A23L1/26 , C07C149/18
CPC分类号： C07C323/00 , A23L13/426 , A23L27/2022 , A23L27/206 , A23L27/21 , A23L27/60
摘要： The flavor of a foodstuff is altered by use of one of the four compounds, the structure of which is one of the configurations of 3((2-mercapto-1-methylpropyl) thio)-2-butanol represented by the structures:

Each of these configurations produ
摘要翻译：通过使用四种化合物之一来改变食品的风味，其结构是由以下结构表示的3（（2-巯基-1-甲基丙基）硫代）-2-丁醇的构型之一：以下结构：通过本文所述的方法制备的这些构型使顺式或反式2,3-丁烷环硫化物与“赤式”或“苏式”2-羟基-3-巯基丁烷反应，由以下结构表示：

9. 发明授权

US3903900A Tobacco articles and compositions containing 1,2-cyclohexanedione and methods for producing same 失效
标题翻译：含有1,2-环己酮的烟草制品及其组合物及其生产方法
公开(公告)号：US3903900A
公开(公告)日：1975-09-09
申请号：US51506674
申请日：1974-10-15
申请人： INT FLAVORS & FRAGRANCES INC
发明人： WOLT JOHN , GIACINO CHRISTOPHER , QUINN ALTON DEWITT , SHUSTER EDWARD J , VINALS JOAQUIN F
IPC分类号： A23L27/20 , A24B15/34 , C07C49/403 , C11B9/00 , A24B15/04
CPC分类号： C11B9/0034 , A23L27/203 , A23L27/2052 , A23L27/2054 , A24B15/34 , C07C49/403
摘要： Methods for preparing tobacco compositions, flavoring compositions for tobaccos and tobacco articles by including therein 1,2-cyclohexanedione and, optionally, in addition, other cyclic di-ketones such as maltol, cyclotene and 2,5-dimethyl-4hydroxy-3(2H)-furanone to produce a maple and spicey note and more natural sweet tobacco note, or to enhance the flavor and fragrance note imparted by other cyclic di-ketones such as maltol, cyclotene, and 2,5-dimethyl-4-hydroxy-3(2H)-furanone as well as the tobacco compositions containing 1,2-cyclohexanedione and, optionally, in addition, other cyclic di-ketones such as maltol, cyclotene and 2,5-dimethyl-4-hydroxy-3(2H)-furanone.

10. 发明授权

US3879466A Bicyclo-{8 2.2.2{9 octa-5,7-dien-2-ones and a process for their preparation 失效
标题翻译：双环 - {8 2.2.2 {9八氢-5,7-二烯-2-酮及其制备方法
公开(公告)号：US3879466A
公开(公告)日：1975-04-22
申请号：US43684774
申请日：1974-01-28
申请人： INT FLAVORS & FRAGRANCES INC
发明人： LIGHT KENNETH K
IPC分类号： C07C43/162 , A23L27/20 , A24B15/34 , C07C27/00 , C07C35/22 , C07C35/52 , C07C41/00 , C07C43/15 , C07C43/166 , C07C43/205 , C07C45/00 , C07C49/385 , C07C49/587 , C07C67/00 , C11B9/00 , C11D3/50 , C11D9/00 , C07C49/54
CPC分类号： C07C45/69 , A23L27/203 , A24B15/345 , C07C43/15 , C07C43/166 , C07C45/62 , C07C45/63 , C07C49/477 , C07C49/513 , C07C49/693 , C07C49/733 , C11B9/00 , C11B9/0042 , C11D3/50 , C11D9/00 , Y10S426/805
摘要： Chemical compounds having the structure:

WHEREIN Z is a moiety selected from the group consisting of:

AND WHEREIN R1, R2, R3, R4, R5, R6, R7, R8, R9 and R10 are the same or different and each is selected from the group consisting of methyl and hydrogen and wherein R11 is selected from the group consisting of methyl, ethyl and hydrogen; and wherein X is selected from the group consisting of bromo, chloro, hydroxyl, benzyloxyl and alkoxyl and a process for preparing such compounds involving intimately admixing a methyl substituted cyclohexadienone having the structure:

WITH ONE OF THE FOLLOWING ACETYLENIC COMPOUNDS HAVING THE STRUCTURES:

The compounds thus produced are valuable intermediates used in producing chemical compounds having valuable organoleptic properties; particularly in perfumery, in flavoring foodstuffs and in flavoring tobacco.
摘要翻译：具有以下结构的化合物：

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