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1. 发明申请

US20100056696A1 Low emission, high scrub VAE latex Paints 有权
标题翻译：低排放，高磨擦VAE乳胶漆
公开(公告)号：US20100056696A1
公开(公告)日：2010-03-04
申请号：US12584152
申请日：2009-09-01
申请人： Elizabeth A. Poole , Rajeev Farwaha , Brett C. Beauregard , Alexander Madl , Jõrg L. Schulte , Harmin Muller , Kristy Jo Beckman
发明人： Elizabeth A. Poole , Rajeev Farwaha , Brett C. Beauregard , Alexander Madl , Jõrg L. Schulte , Harmin Muller , Kristy Jo Beckman
IPC分类号： C09D5/02 , C08L31/04
CPC分类号： C09D131/04 , C08K3/013 , C08L31/04 , C08L33/08 , C09D133/08 , C08L2666/04
摘要： A water-based, low-emission latex paint formulation includes a vinyl acetate/ethylene (VAE) latex including a VAE resin with from 80 to 95 weight % vinyl acetate residue and from 5 to 20 weight % ethylene residue, optionally including additional monomers as well as a pigment composition including inorganic solids selected from inorganic pigments, inorganic fillers and mixtures thereof present in an amount such that the paint formulation has a pigment volume concentration (PVC) of from 25% to 85%. The formulations are suitable for eggshell and flat latex paints and exhibit surprising durability.
摘要翻译：水性低发射乳胶漆制剂包括乙酸乙烯酯/乙烯（VAE）胶乳，其包含具有80至95重量％乙酸乙烯酯残余物和5至20重量％乙烯残余物的VAE树脂，任选地包括另外的单体作为以及作为颜料组合物，其包含选自无机颜料，无机填料及其混合物的无机固体，其量使得涂料配方的颜料体积浓度（PVC）为25％至85％。该配方适用于蛋壳和扁平乳胶漆，并表现出令人惊奇的耐用性。

2. 发明申请

US20050043463A1 Preparation of multimodal polymer dispersions using polymeric stabilizer, and use thereof 有权
标题翻译：使用聚合物稳定剂制备多峰聚合物分散体及其用途
公开(公告)号：US20050043463A1
公开(公告)日：2005-02-24
申请号：US10918121
申请日：2004-08-12
申请人： Harmin Muller
发明人： Harmin Muller
IPC分类号： C08F2/24 , C08L1/00
CPC分类号： C08F2/24
摘要： A description is given of a process for preparing bimodal or multimodal polymers from olefinically unsaturated monomers in an aqueous medium. The process features the introduction as initial charge of selected mixtures of polymeric stabilizers and of at least one selected ionic comonomer. In the polymerization process the monomer is metered continuously or discontinuously into the said initial charge. In this way it is possible by means of simple process measures to prepare bimodal or multimodal dispersions.
摘要翻译：描述了在水性介质中由烯属不饱和单体制备双峰或多峰聚合物的方法。该方法的特征在于引入作为聚合物稳定剂和至少一种选择的离子共聚单体的所选混合物的初始电荷。在聚合过程中，将单体连续地或不连续地计量到所述初始电荷中。以这种方式，可以通过简单的过程措施来制备双峰或多峰分散体。

3. 发明申请

US20090203832A1 Process for Preparing Polymer Dispersions, the Resulting Dispersions and Their Use 有权
标题翻译：制备聚合物分散体的方法，所得的分散体及其用途
公开(公告)号：US20090203832A1
公开(公告)日：2009-08-13
申请号：US12367039
申请日：2009-02-06
申请人： Harmin Muller , Harald Petri , Thomas Drechsel
发明人： Harmin Muller , Harald Petri , Thomas Drechsel
IPC分类号： C08L29/04 , C08F2/44
CPC分类号： C08F2/24
摘要： A description is given of a process of emulsion polymerization of free-radically polymerizable ethylenically unsaturated monomers selected from the group of the monoesters or diesters of ethylenically unsaturated monocarboxylic or dicarboxylic acids with alkanols, vinyl esters and/or vinylaromatics and, if desired, further monomers copolymerizable therewith, at least 60% of the total conversion in the polymerization taking place at a temperature of 100° C. to 160° C., the polymerization being performed in the presence of emulsifiers and an amount of 0% to 1% by weight, based on the total amount of the monomers used, of protective colloid.The process can be used to obtain significantly faster conversions for comparable quality of the process products.The dispersions obtained can be employed in a wide variety of different applications, such as binders for paints or as adhesives.
摘要翻译：描述了可自由基聚合的烯键式不饱和单体的乳液聚合方法，该单体选自烯键式不饱和单羧酸或二羧酸的单酯或二酯与链烷醇，乙烯基酯和/或乙烯基芳族化合物，以及如果需要，其它单体可与其共聚的聚合反应的总转化率的至少60％在100℃至160℃的温度下进行，聚合反应在乳化剂存在下进行，其量为0重量％至1重量％，基于所用单体的总量，保护胶体。该过程可用于获得显着更快的转化率，以达到可比较的过程产品质量。所获得的分散体可以用于各种不同的应用，例如用于油漆的粘合剂或粘合剂。

4. 发明申请

US20050222374A1 Method for the production of aqueous polymer dispersions containing very few residual monomers and use thereof 有权
标题翻译：制备含有非常少的残留单体的聚合物水分散体的方法及其用途
公开(公告)号：US20050222374A1
公开(公告)日：2005-10-06
申请号：US10527178
申请日：2003-07-26
申请人： Harmin Muller , Martin Jakob , Carsten Heldmann , Thomas Wirth
发明人： Harmin Muller , Martin Jakob , Carsten Heldmann , Thomas Wirth
IPC分类号： C08F6/00 , C08G63/02
CPC分类号： C08F6/006
摘要： The invention relates to a method for reducing the amount of residual monomers in aqueous polymer dispersions means of chemical post-treatment. Post-treatment in the aqueous polymer dispersion is carried out by adding a redox system which contains a) 0.005-5 wt. % of an oxidation agent which contains an organic peroxide. and b) 0.005-5 wt. % of a reduction agent which contains sulfinic acids or salts thereof. Additionally. the redox system can, optionally, contain catalytic amounts of a polyvalent metallic ion which can be treated in several valent stages. Post-treatment can be carried out at a temperature ranging from 20-100° C. and at a PH-value ranging from 2-9. The invention also relates to the use of the inventive post-treated polymer dispersion for producing adhesives, coarings, powders, constructive chemical products or for refining textiles or paper.
摘要翻译：本发明涉及减少聚合物水分散体中化学后处理方法中残余单体量的方法。在聚合物水分散体中的后处理是通过加入氧化还原体系进行的，所述氧化还原体系含有：a）0.005-5wt。含有有机过氧化物的氧化剂的％。和b）0.005-5wt。％的还原剂含有亚磺酸或其盐。另外。氧化还原体系可以任选地含有催化量的多价金属离子，其可以在几个阶段中进行处理。后处理可以在20-100℃的温度和2-9的PH值下进行。本发明还涉及本发明的后处理聚合物分散体用于生产粘合剂，结焦，粉末，建构性化学产品或用于精制纺织品或纸的用途。

5. 发明申请

US20130156997A1 Flame Retardant Carpet Products With Coating and/or Adhesive Layers Formed From Vinyl Acetate/Ethylene Copolymer Dispersions 有权
标题翻译：具有由乙酸乙烯酯/乙烯共聚物分散体形成的涂层和/或粘合剂层的阻燃地毯产品
公开(公告)号：US20130156997A1
公开(公告)日：2013-06-20
申请号：US13811956
申请日：2011-08-12
申请人： Harmin Muller , Paul Wormald , Paolo Bavaj
发明人： Harmin Muller , Paul Wormald , Paolo Bavaj
IPC分类号： D06N7/00
CPC分类号： D06N7/0063 , D06N7/0073 , D06N2203/042 , D06N2209/067 , Y10T428/23921
摘要： Disclosed are carpet products comprising at least one flexible substrate and at least one coating and/or adhesive layer associated with the at least one flexible substrate. The coating and/or adhesive layer is formed from an aqueous composition comprising: A) an emulsifier-stabilized vinyl acetate/ethylene (VAE) emulsion copolymer dispersion and B) at least one particulate filler material selected from particulate inorganic compounds and particulate plastic material. The vinyl acetate/ethylene copolymer in the copolymer dispersion has a selected ethylene content or glass transition temperature. It is also preferably substantially free of cross-linkable co-monomer moieties which generate formaldehyde upon curing and preferably has a particle size, dw, ranging from about 50 to about 500 nm. The carpet product is substantially free of polyvinyl chloride and bitumen and exhibits a Class B1 flame-retardancy in accordance with DIN 4102-14, corresponding to a critical heat flux of ≧about 4.5 kW/m2.
摘要翻译：公开了包含至少一个柔性基底和与至少一个柔性基底相关联的至少一个涂层和/或粘合剂层的地毯产品。涂层和/或粘合剂层由水性组合物形成，该组合物包含：A）乳化剂稳定的乙酸乙烯酯/乙烯（VAE）乳液共聚物分散体和B）至少一种选自颗粒无机化合物和颗粒状塑料材料的颗粒填料。共聚物分散体中的乙酸乙烯酯/乙烯共聚物具有选定的乙烯含量或玻璃化转变温度。还优选基本上不含可固化的共聚单体部分，其在固化时产生甲醛，优选具有约50至约500nm范围内的粒度dw。地毯产品基本上不含聚氯乙烯和沥青，并且符合DIN 4102-14的B1类阻燃性，对应于> = 4.5kW / m 2的临界热通量。

6. 发明授权

US08053511B2 Process for preparing polymer dispersions, the resulting dispersions and their use 有权
标题翻译：制备聚合物分散体的方法，所得分散体及其用途
公开(公告)号：US08053511B2
公开(公告)日：2011-11-08
申请号：US12367039
申请日：2009-02-06
申请人： Harmin Muller , Harald Petri , Thomas Drechsel
发明人： Harmin Muller , Harald Petri , Thomas Drechsel
IPC分类号： C08L29/04 , C08F2/44
CPC分类号： C08F2/24
摘要： A description is given of a process of emulsion polymerization of free-radically polymerizable ethylenically unsaturated monomers selected from the group of the monoesters or diesters of ethylenically unsaturated monocarboxylic or dicarboxylic acids with alkanols, vinyl esters and/or vinylaromatics and, if desired, further monomers copolymerizable therewith, at least 60% of the total conversion in the polymerization taking place at a temperature of 100° C. to 160° C., the polymerization being performed in the presence of emulsifiers and an amount of 0% to 1% by weight, based on the total amount of the monomers used, of protective colloid.The process can be used to obtain significantly faster conversions for comparable quality of the process products.The dispersions obtained can be employed in a wide variety of different applications, such as binders for paints or as adhesives.
摘要翻译：描述了可自由基聚合的烯键式不饱和单体的乳液聚合方法，该单体选自烯键式不饱和单羧酸或二羧酸的单酯或二酯与链烷醇，乙烯基酯和/或乙烯基芳族化合物，以及如果需要，其它单体可与其共聚的聚合反应的总转化率的至少60％在100℃至160℃的温度下进行，聚合反应在乳化剂存在下进行，其量为0重量％至1重量％，基于所用单体的总量，保护胶体。该过程可用于获得显着更快的转化率，以达到可比较的过程产品质量。所获得的分散体可以用于各种不同的应用，例如用于油漆的粘合剂或粘合剂。

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