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1. 发明授权

US3923707A Process for the production of pourable, pulverulent rubbers 失效
标题翻译：用于生产可倾倒，粉碎的橡胶的方法
公开(公告)号：US3923707A
公开(公告)日：1975-12-02
申请号：US48059874
申请日：1974-06-18
申请人： HUELS CHEMISCHE WERKE AG
发明人： BERG GERHARD , NORDSIEK KARL-HEINZ
IPC分类号： C08F6/00 , B29B9/00 , B29B15/00 , B29B15/02 , C08C2/00 , C08C2/06 , C08F293/00 , C08F297/00 , C08F297/04 , C08J3/12 , C08J3/16 , C08L1/08 , C08L9/00 , C08L9/08
CPC分类号： C08J3/16 , C08C2/06 , C08J2321/00
摘要： A process for preparing discrete, finely divided, tack-free, pourable, powdery, filler-free elastomer particles by emulsifying rubber solutions in water with an amine emulsifier and precipitating the emulsions, wherein rubbers are utilized which contain crystalline and/or thermoplastic proportions arranged in block form; these rubber solutions are emulsified in water in the presence of emulsifiers; the emulsions are continuously introduced into hot water optionally containing precipitants; the rubber solvent is simultaneously distilled off continuously; and the rubber, thus obtained in a finely particulate form, is separated from the water and dried in a controlled temperature range.
摘要翻译：一种通过用胺乳化剂乳化水中的橡胶溶液并沉淀乳液来制备离散的，细碎的，无粘性的，可倾倒的粉末状无填充弹性体颗粒的方法，其中使用含有结晶和/或热塑性比例排列的橡胶以块形式这些橡胶溶液在乳化剂存在下在水中乳化; 将乳液连续引入任选含有沉淀剂的热水中; 同时将橡胶溶剂蒸馏掉; 将由此获得的细颗粒形式的橡胶与水分离并在受控温度范围内干燥。

2. 发明授权

US3883494A Process for the preparation of emulsifier-containing polyvinyl chloride or vinyl chloride copolymer powders 失效
标题翻译：制备含乳化剂的聚氯乙烯或氯乙烯共聚物粉末的方法
公开(公告)号：US3883494A
公开(公告)日：1975-05-13
申请号：US28897272
申请日：1972-09-14
申请人： HUELS CHEMISCHE WERKE AG
发明人： WINTER HERMANN , SMOLINSKI MANFRED , WOLF HANS-GEORG , ROLL HARRY , HOFFMANN KURT , JACOB HELMUT
IPC分类号： B01J2/04 , C08J3/12 , C08F1/88
CPC分类号： C08J3/122 , C08J2327/06
摘要： Uniform, finely divided powdery vinyl chloride polymer particles containing less than 2 wt. % particles having a diameter greater than 40 Mu are obtained by spray-drying an aqueous dispersion of the polymer and a carrier gas through a two-fluid atomizer into a water-evaporating atmosphere at specified rates. The resultant polymer particles exhibit inproved handling properties and can be used to form improved plastisols without air separation of the particles.
摘要翻译：含有小于2重量％的均匀，细碎的氯乙烯聚合物粉末。通过将聚合物的水性分散体和载气通过双液体雾化器喷雾干燥至特定速率的水蒸发气氛中，获得直径大于40μm的％颗粒。所得到的聚合物颗粒表现出改进的操作性能，并且可以用于形成改进的增塑溶胶，而空气不分离颗粒。

3. 发明授权

US3878259A Process for manufacturing cumene 失效
标题翻译：异丙苯制造工艺
公开(公告)号：US3878259A
公开(公告)日：1975-04-15
申请号：US46067974
申请日：1974-04-15
申请人： HUELS CHEMISCHE WERKE AG
发明人： HOCKELE GUNTER , KNEPPER WILHELM
IPC分类号： B01J23/78 , C07C5/03 , C07C5/10 , C07C7/00
CPC分类号： B01J23/78 , C07C5/03 , Y02P20/52 , C07C15/085
摘要： A process for the manufacture of cumene by hydrogenating alphamethylstyrene with hydrogen in the presence of an alkalinated nickel aluminum oxide carrier catalyst, the improvement comprising, carrying out the hydrogenation at temperatures of about 60*- 160*C in the presence of a catalyst where the carrier material contains kappa and/or delta aluminum oxide having an alkali content of 0.1 - 5 percent by wweight of alkali oxide, wherein (if appropriate) molded aluminum hydroxide containing alkali is dried in a known manner, then it is heated in an air stream at about 400*- 500*C and thereafter steam treated at about 700*- 800*C. The calcined catalyst is then impregnated with a nickel salt in a conventional manner, the salt subsequently being completely decomposed into nickel oxide and volatile components, the nickel content of the catalyst (computed as nickel metal) being about 5 - 12 percent by weight referred to the calcined catalyst. The impregnated catalyst is thereupon reduced in a conventional manner.
摘要翻译：一种通过在碱式化的氧化铝载体催化剂的存在下用氢气氢化α-甲基苯乙烯来制造枯烯的方法，其改进包括在约60-160℃的温度下在催化剂存在下进行氢化其中载体材料含有碱含量为0.1-5％（重量）碱性氧化物的κ和/或δ-氧化铝，其中（如果合适的话）含有碱的模制氢氧化铝以已知方式干燥，然后在空气流在约400-500℃，然后在约700-800℃下进行蒸汽处理。然后以常规方式用镍盐浸渍煅烧的催化剂，随后将其完全分解成氧化镍和挥发性组分，催化剂的镍含量（以镍金属计算）为煅烧催化剂的约5-12重量％。随后以常规方式减少浸渍的催化剂。

4. 发明授权

US3878241A Method for the separation of acetic acid by extractive rectification 失效
标题翻译：通过萃取精馏分离乙酸的方法
公开(公告)号：US3878241A
公开(公告)日：1975-04-15
申请号：US32269973
申请日：1973-01-11
申请人： HUELS CHEMISCHE WERKE AG
发明人： MULLER WOLFGANG
IPC分类号： B01D3/40 , C07C51/00 , C07C51/44 , C07C51/48 , C07C53/08 , C07C67/00
CPC分类号： C07C51/44 , C07C51/48 , C07C53/08
摘要： In the method for separating acetic acid from water containing mixtures by extractive rectification, the improvement comprising carrying out a first step rectification with the water containing acetic acid and 1,2-dimorpholinoethane and by a second step of separating the acetic acid and 1,2-dimorpholinoethane by rectification.
摘要翻译：在通过萃取精馏从含有混合物的水分离乙酸的方法中，改进包括用含有乙酸和1,2-二吗啉代乙烷的水进行第一步精馏，通过第二步分离乙酸和1,2- 二吗啉代乙炔通过整流。

5. 发明授权

US3852373A Process for the production of liquid butadiene polymers 失效
标题翻译：生产液体二聚体聚合物的方法
公开(公告)号：US3852373A
公开(公告)日：1974-12-03
申请号：US25164872
申请日：1972-05-09
申请人： HUELS CHEMISCHE WERKE AG
发明人： HESSE K , VON PORTATIUS H
IPC分类号： C08F36/04 , C08F1/52
CPC分类号： C08F36/04 , Y10S585/952 , C08F4/7098
摘要： A process for preparing liquid butadiene polymers which comprises polymerizing 1,3-butadiene at a temperature of 10*180*C with a catalytic amount of a mixed catalyst including a solvent-soluble organonickel compound and an organoaluminum compound in contact with a molecular weight regulating amount of at least one monoolefinically unsaturated compound of the formula

WHEREIN R1 and R2 are each hydrogen, chlorine, or alkyl of 1-5 carbon atoms, and R3 is hydrogen or chlorine. High yields are attainable at elevated polymerization temperatures without extreme increases in viscosity of the product.
摘要翻译：一种制备液体丁二烯聚合物的方法，其包括在10-180℃的温度下用催化量的混合催化剂聚合1,3-丁二烯，所述混合催化剂包括与分子量接触的溶剂可溶的有机镍化合物和有机铝化合物调节量至少一种式WHEREIN R1和R2的单烯属不饱和化合物各自为氢，氯或1-5个碳原子的烷基，R3为氢或氯。在高聚合温度下可获得高产率，而不会极大地提高产品的粘度。

6. 发明授权

US3849509A Polyalkenamers and process for the preparation thereof 失效
公开(公告)号：US3849509A
公开(公告)日：1974-11-19
申请号：US36871073
申请日：1973-06-11
申请人： HUELS CHEMISCHE WERKE AG
发明人： STRECK R , WEBER H
IPC分类号： C08G61/08 , C07C11/00 , C07C3/60
CPC分类号： C08G61/08 , Y10S585/94
摘要： 1. A PROCESS FOR THE PRODUCTION OF POLYALKENAMERS BY THE CATALYZED RING-OPENING POLYMERIZATION OF CYCLIC OLEFINS EMPLOYING A CATALYST CONTAINING A METAL OF SUBGROUPS 5 TO 7 OF THE PERIODIC TABLE WHICH COMPRISES CONDUCTING THE POLYMERIZATION IN THE PRESENCE OF AN UNSATURATED CARBOXYLIC ACID ESTER WHEREIN THE ESTER GROUP IS SEPARATED FROM THE DOUBLE BONDED CARBON ATOM BY AT LEAST ONE METHYLENE GROUP OR THE SINGLE BONDED OXYGEN ATOM OF THE ESTER GROUP AND AT LEAST ONE OF THE CARBON ATOMS HAVING THE DOUBLE BOND HAS AT LEAST ONE HYDROGEN ATOM.

7. 发明授权

US3839190A Process for the production of bitumen or bitumen-containing mixtures with improved properties 失效
标题翻译：生产具有改善性质的含有或含有BITUMEN的混合物的方法
公开(公告)号：US3839190A
公开(公告)日：1974-10-01
申请号：US33445373
申请日：1973-02-21
申请人： HUELS CHEMISCHE WERKE AG
发明人： FRESE A , CHRISTOFZIK H
IPC分类号： C10C3/02
CPC分类号： C10C3/023 , C10C3/02
摘要： The softening point of bitumens having softening points of up to 120* C. is raised without adversely affecting rupturing point and other properties by heating the bitumen at a temperature above the softening point of up to 150* C. for up to 30 minutes with either sulfuric acid or a metal halide selected from the group consisting of TiCl4, AlCl3, VOCl3, VCl4 and ZrCl4.
摘要翻译：软化点高达120℃的沥青的软化点不会对破裂点和其他性能产生不利影响，通过在高于150℃的软化点的温度下加热沥青长达30分钟，任一种硫酸或选自TiCl 4，AlCl 3，VOCl 3，VCl 4和ZrCl 4的金属卤化物。

8. 发明授权

US3821328A Process for the production of copolyalkenamers 失效
标题翻译：生产共聚酯的方法
公开(公告)号：US3821328A
公开(公告)日：1974-06-28
申请号：US26517072
申请日：1972-06-22
申请人： HUELS CHEMISCHE WERKE AG
发明人： STRECK R , NORDSIEK K , WEBER H , MEYER K
IPC分类号： C08F36/00 , C08G61/08 , C08F29/02
CPC分类号： C08G61/08 , C08F36/00
摘要： Copolyalkenamers are produced by reacting a rubbery polybutadiene wherein more than 80 percent of the butadiene contact thereof is a 1,4-polymer, with a polyoctenamer or polydodecenamer or mixture thereof, in the presence of a mixed catalyst containing a compound of a metal of Subgroup 5 through 7 and a metal or a compound thereof of Main Group 1 through 4 of the Periodic Table.

9. 发明授权

US3817912A Nonflammable molding compositions of styrene polymers 失效
标题翻译：苯乙烯聚合物的非易燃成型组合物
公开(公告)号：US3817912A
公开(公告)日：1974-06-18
申请号：US21373871
申请日：1971-12-29
申请人： HUELS CHEMISCHE WERKE AG
发明人： DIEBEL K , BIRKNER H
IPC分类号： C08K5/03 , C09K3/28
CPC分类号： C08K5/03 , C08L25/04 , C08L55/02
摘要： IMPROVED NONFLAMMABLE POLYSTYRENE MOLDING COMPOSITIONS CONTAINING 1-20% OF A BROMINATED POLYALKYLBENZENE OF THE FORMULA

(R)M,(R'')N-BENZENE

WHEREIN R IS BROMOMETHYL OR DIBROMOMETHYL, M IS AN INTEGER FROM 2 TO 4, INCLUSIVE, R'' IS ALKYL OF 1-3 CARBON ATOMS, BROMINE OR CHLORINE, AT LEAST ONE R'' BEING ORTHO TO EACH R, AND N IS AN INTEGER FRP, 1 TO 4, INCLUSIVE.

10. 发明授权

US3816358A Vulcanizable rubber mixtures 失效
标题翻译： VULCANIZABLE橡胶混合物
公开(公告)号：US3816358A
公开(公告)日：1974-06-11
申请号：US26516772
申请日：1972-06-22
申请人： HUELS CHEMISCHE WERKE AG
发明人： NORDSIEK K , STRECK R
IPC分类号： C08L21/00 , C08L23/16 , C08L23/22 , C08D9/08 , C08C9/04 , C08C9/14
CPC分类号： C08L21/00 , C08K3/04 , C08K3/06 , C08K3/22 , C08K5/09 , C08L7/00 , C08L9/00 , C08L9/06 , C08L23/16 , C08L23/22 , C08L23/24 , C08L65/00 , C08L91/00 , C08L2312/00 , C08L2666/04 , Y10T152/1081 , Y10T152/10846 , C08L2666/14
摘要： Vulcanizable rubber mixtures having improved room temperature hardness containing 2-20% by weight, calculated on the rubber, of a polyoctenamer or polydodecenamer.

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