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1. 发明授权

US4312642A Method for the separate discharge of the individual phase streams of a multiple phase flow 失效
标题翻译：分离排放多相流的各相流的方法
公开(公告)号：US4312642A
公开(公告)日：1982-01-26
申请号：US126267
申请日：1980-03-03
申请人： Gunter Lehr , Karl-Dieter Lohr , Uwe Hucks , Hugo Vernaleken
发明人： Gunter Lehr , Karl-Dieter Lohr , Uwe Hucks , Hugo Vernaleken
IPC分类号： B29C48/76 , B01D19/00
CPC分类号： B29C47/76 , B29C47/0009 , B29C47/766
摘要： A method for the separate discharge of the individual phase streams of a multiple component flow comprising a high viscosity slow flowing liquid or suspension and a gas flowing at at least 100 times faster with the volumetric ratio of the gas to the liquid being greater than 1:1. The multicomponent flow is transversely fed through an inlet and directly into a rotating helical channel for conveying liquid in one direction. The channel has a liquid outlet spaced from the inlet in the one direction and a gas outlet spaced from the inlet in the opposite direction. A gas shut-off is formed between the inlet and the liquid outlet so as to effect the discharge of gas through the gas outlet in the opposite direction during the conveying of the liquid by the helical channel to the liquid outlet in the one direction.
摘要翻译：一种用于单独排放多组分流的单个相流的方法，其包括高粘度慢流动的液体或悬浮液和以至少100倍的速度流动的气体，其中气体与液体的体积比大于1： 1。多组分流被横向地通过入口进料并直接进入用于在一个方向上输送液体的旋转螺旋通道。通道具有在一个方向上与入口间隔开的液体出口和在相反方向上与入口间隔开的气体出口。在入口和液体出口之间形成气体切断，以便在将液体通过螺旋通道沿一个方向输送到液体出口时，在相反方向上实现气体通过气体出口的排出。

2. 发明授权

US4472558A Process for carrying out reactions caused by the transport of substances 失效
标题翻译：进行由物质运输引起的反应的过程
公开(公告)号：US4472558A
公开(公告)日：1984-09-18
申请号：US45028
申请日：1979-06-04
申请人： Clemens Casper , Henning Klussmann , Gunter Lehr , Johannes O. Sajben , Artur Reischl , Rudolf Binsack , Frank Wingler
发明人： Clemens Casper , Henning Klussmann , Gunter Lehr , Johannes O. Sajben , Artur Reischl , Rudolf Binsack , Frank Wingler
IPC分类号： B01D3/28 , B01J3/04 , B01J10/02 , B01J19/24 , C08F2/00 , C08F2/06 , C08G18/00 , C08G18/08
CPC分类号： C08G18/0838 , B01J10/02 , B01J19/243 , B01J3/042 , B01J2219/00085 , B01J2219/00162 , B01J2219/00164
摘要： This invention relates to a process for carrying out reactions which primarily occur during the transport of compounds in the liquid phase or at the liquid-gas interface. Starting components are reacted with one another and/or with gases of the inner space in a multi-phase flow tube having a liquid ring flow which may contain dissolved and/or dispersed constituents. Any necessary heat exchange takes place between the liquid and the wall of the tube or the gases.
摘要翻译：本发明涉及一种进行反应的方法，主要发生在化合物在液相或液 - 液界面输送过程中。起始组分在具有可能含有溶解和/或分散成分的液体环流的多相流动管中彼此反应和/或与内部空间的气体反应。在液体和管壁或气体之间进行任何必要的热交换。

3. 发明授权

US4327208A Continuous process for the hydrolytic production of polycaprolactam having a low-monomer and low-dimer content 失效
标题翻译：用于水解生产具有低单体和低二聚体含量的聚己内酰胺的连续方法
公开(公告)号：US4327208A
公开(公告)日：1982-04-27
申请号：US167055
申请日：1980-07-09
申请人： Gunter Lehr , Uwe Hucks , Hugo Vernaleken , Werner Nielinger , Erhard Tresper
发明人： Gunter Lehr , Uwe Hucks , Hugo Vernaleken , Werner Nielinger , Erhard Tresper
IPC分类号： C08G69/00 , C08G69/16 , C08G69/46 , C08L101/16
CPC分类号： C08G69/46
摘要： A process for the production of polyamide-6 or corresponding copolyamides by hydrolytic polymerization wherein the low molecular weight secondary reaction products and the unreacted .epsilon.-caprolactam are separated off from the polyamide melt and directly condensed on the .epsilon.-caprolactam melt to be polymerized.
摘要翻译：通过水解聚合制备聚酰胺-6或相应的共聚酰胺的方法，其中将低分子量二级反应产物和未反应的ε-己内酰胺与聚酰胺熔体分离并直接在ε-己内酰胺熔体上缩合以进行聚合。

4. 发明授权

US4212963A Polybutylene terephthalates having a low carboxyl content and continuous process for the production thereof 失效
标题翻译：具有低羧基含量的聚对苯二甲酸丁二酯和用于生产的连续方法
公开(公告)号：US4212963A
公开(公告)日：1980-07-15
申请号：US968892
申请日：1978-12-13
申请人： Gunter Lehr , Rudolf Binsack
发明人： Gunter Lehr , Rudolf Binsack
IPC分类号： C08G63/00 , C08G63/78 , C08G63/18
CPC分类号： C08G63/785 , C08G63/78
摘要： Polybutylene terephthalates having a narrow molecular weight distribution, a low carboxyl group content and an intrinsic viscosity of from 0.2 to 1.4 dl/g can be continuously produced by transporting a molten reaction mixture of terephthalic acid mono- and/or bis-(hydroxybutyl) ester or low viscosity polybutylene terephthalate at 160.degree. to 300.degree. C., together with a heated inert gas, in a diphasic annular stream through an externally heated spiral reaction tube (of substantially constant pitch) having a diameter of from 3 to 100 mm and a diameter/length ratio of from 1:400 to 1:2000 by the maintenance of a pressure difference between the beginning and the end of the reaction tube, under conditions such that the absolute pressure, determined at the point of entry of the reaction mixture into the tube, is from 1 to 100 bar and the viscosity of the annular stream is from 1 to 10,000 poises (determined at the reaction temperature), and a circular stream between the surface of the melt and the wall of the tube is produced by the curvature of the tube and a stream of gas flowing at a velocity of from 20 to 300 m/sec to accelerate the transport of material between the melt and the inert gas, whereby the reaction takes place in the liquid phase and/or at the melt/gas interface.
摘要翻译：通过将对苯二甲酸单 - 和/或双 - （羟基丁基）酯的熔融反应混合物输送，可以连续制备具有窄分子量分布，低羧基含量和特性粘度为0.2-1.4dl / g的聚对苯二甲酸丁二醇酯或低粘度聚对苯二甲酸丁二醇酯在160℃至300℃下与加热的惰性气体一起通过直径为3至100mm的外部加热的螺旋反应管（基本上恒定的间距）和二价环状流通过维持反应管的开始和结束之间的压力差，在使反应混合物进入点确定的绝对压力为管子为1至100巴，环形流的粘度为1至10,000泊（在反应温度下确定），并且在熔体表面之间的圆形流 d管的壁由管的曲率和以20-300m / sec的速度流动的气流产生，以加速在熔体和惰性气体之间的材料的输送，从而发生反应在液相和/或在熔体/气体界面处。

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