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1. 发明授权

US07247742B2 Recycling polyethylene naphthalate containing materials in a process to produce diesters 有权
标题翻译：在生产二酯的过程中回收含有聚萘二甲酸乙二醇酯的材料
公开(公告)号：US07247742B2
公开(公告)日：2007-07-24
申请号：US10849750
申请日：2004-05-20
申请人： Rosemary F. McMahon , John A. Macek , Gregory P. Hussmann , Michael J. Panzer , Raymond J. Eifert , David A. Young , Allen B. Mossman , J. Deven Cleckler
发明人： Rosemary F. McMahon , John A. Macek , Gregory P. Hussmann , Michael J. Panzer , Raymond J. Eifert , David A. Young , Allen B. Mossman , J. Deven Cleckler
IPC分类号： C07C67/08 , C07C69/76
CPC分类号： C07C67/52 , C07C67/03 , C07C67/08 , C07C67/54 , C07C69/76
摘要： A process for preparing a dialkylester of a naphthalenedicarboxylic acid comprising directing a liquid phase reaction mixture comprising a low molecular weight alcohol, a naphthalenedicarboxylic acid, a dialkylester of a naphthalenedicarboxylic acid, and a polyethylene naphthalate containing material, at a given temperature and pressure through series arranged reaction zones and subsequently removing a product comprising a dialkylester formed by the reaction of the naphthalenedicarboxylic acid and the polyethylene naphthalate containing material with the low molecular weight alcohol from a reaction zone. This invention is also directed to a process for preparing a purified dialkylester of a naphthalenedicarboxylic acid comprising a series of crystallization and distillation steps, and combinations thereof.
摘要翻译：一种制备萘二甲酸二烷基酯的方法，包括在给定的温度和压力下通过串联引入包含低分子量醇，萘二甲酸，萘二羧酸的二烷基酯和含萘二甲酸乙二醇酯的材料的液相反应混合物并且随后从反应区除去包含由萘二甲酸与含聚萘二甲酸乙二醇酯的材料与低分子量醇反应形成的二烷基酯的产物。本发明还涉及一种制备萘二甲酸的纯化二烷基酯的方法，其包括一系列结晶和蒸馏步骤及其组合。

2. 发明授权

US5350874A Process for preparing diesters of naphthalenedicarboxylic acids 失效
标题翻译：萘二羧酸二酯的制备方法
公开(公告)号：US5350874A
公开(公告)日：1994-09-27
申请号：US981184
申请日：1992-11-24
申请人： Paul K. Behrens , Juergen K. Holzhauer , Gregory P. Hussmann , David L. Sikkenga
发明人： Paul K. Behrens , Juergen K. Holzhauer , Gregory P. Hussmann , David L. Sikkenga
IPC分类号： C07C67/08 , C07C69/76
CPC分类号： C07C67/08
摘要： A continuous process for preparing a dialkylester of a naphthalenedicarboxylic acid comprising passing a liquid phase reaction mixture comprising a low molecular weight alcohol, a naphthalenedicarboxylic acid and a dialkylester of a naphthalenedicarboxylic acid at an elevated temperature through series arranged reaction zones while introducing a naphthalenedicarboxylic acid and a low molecular weight alcohol to an upstream reaction zone, agitating at least one reaction zone, and removing a liquid product mixture comprising the dialkylester of the naphthalenedicarboxylic acid produced by the reaction of the naphthalenedicarboxylic acid with the low molecular weight alcohol from a downstream reaction zone.
摘要翻译：一种制备萘二甲酸二烷基酯的连续方法，包括使高分子量醇，萘二甲酸和萘二甲酸二烷基酯的液相反应混合物在升高的温度下通过串联排列的反应区，同时引入萘二甲酸和将低分子量醇与上游反应区混合，搅拌至少一个反应区，以及除去通过萘二甲酸与低分子量醇的反应产生的萘二甲酸二烷基酯的液体产物混合物，从下游反应区。

3. 发明授权

US5041633A Process for the production of an aromatic polycarboxylic acid 失效
标题翻译：用于制备芳族多元羧酸的方法
公开(公告)号：US5041633A
公开(公告)日：1991-08-20
申请号：US43838
申请日：1987-04-28
申请人： Walter Partenheimer , Gregory P. Hussmann , Juergen K. Holzhauer , Stephen V. Hoover
发明人： Walter Partenheimer , Gregory P. Hussmann , Juergen K. Holzhauer , Stephen V. Hoover
IPC分类号： C07C51/265
CPC分类号： C07C51/265
摘要： A method for producing an aromatic polycarboxylic acid by oxidizing an aromatic feed compound having at least 3 oxidizable ring substituents, wherein, after initiation of the oxidation water from an external source is added and the reaction temperature is raised.
摘要翻译：通过氧化具有至少3个可氧化环取代基的芳族进料化合物来制备芳族多元羧酸的方法，其中，从外部来源加入氧化水后，反应温度升高。

4. 发明授权

US5030749A Method for producing purified trimesic acid 失效
标题翻译：纯化三苯甲酸的制备方法
公开(公告)号：US5030749A
公开(公告)日：1991-07-09
申请号：US805113
申请日：1985-12-04
申请人： Gregory P. Hussmann
发明人： Gregory P. Hussmann
IPC分类号： C07C51/265 , C07C51/43
CPC分类号： C07C51/265 , C07C51/43
摘要： A method is disclosed for producing purified trimesic acid prepared by a process involving the liquid-phase oxidation of mesitylene in a solvent consisting of an aliphatic C.sub.2 -C.sub.6 monocarboxylic acid, water or a mixture thereof in the presence of an oxidation catalyst comprising cobalt, manganese and bromine components, crystallizing crude trimesic acid by cooling to about 80.degree. C. to about 150.degree. C., separating crystallized trimesic acid from the mother liquor at a temperature in the range of 80.degree. C. to about 105.degree. C. and washing the separated crude trimesic acid crystals with water at a temperature of from about 10.degree. C. to about 100.degree. C.
摘要翻译：公开了一种制备纯化均苯三酸的方法，该方法是在包含钴，锰，锰的氧化催化剂的存在下，通过在由脂族C 2 -C 6单羧酸，水或其混合物组成的溶剂中，将均三甲苯的液相氧化的方法制备的和溴组分，通过冷却至约80℃至约150℃使粗均苯三甲酸结晶，在80℃至约105℃的温度下从母液中分离结晶的均苯三酸，并将洗涤在约10℃至约100℃的温度下用水分离出粗均苯三酸晶体

5. 发明授权

US4900865A Method for producing a di-(mono- or poly-)carboxyaryl ether 失效
标题翻译：二（单或多）羧基芳基醚的制备方法
公开(公告)号：US4900865A
公开(公告)日：1990-02-13
申请号：US125477
申请日：1987-11-25
申请人： Gregory P. Hussmann , Juergen K. Holzhauer , George E. Kuhlmann
发明人： Gregory P. Hussmann , Juergen K. Holzhauer , George E. Kuhlmann
IPC分类号： C07C51/265
CPC分类号： C07C51/265
摘要： A method is disclosed for the liquid-phase oxidation of a di- (mono- or poly-)alkylaryl ether in the presence of a catalyst comprising cobalt, manganese and bromine components to a di- (mono- or poly-)carboxyaryl ether.
摘要翻译：公开了一种在包含钴，锰和溴组分的催化剂存在下将二 - （单 - 或多）烷基芳基醚液相氧化成二 - （单 - 或多） - 芳基芳基醚的方法。

6. 发明授权

US4898982A Preparation of diaryl ethers and diaryl sulfides 失效
标题翻译：二芳基醚和二芳基硫化物的制备
公开(公告)号：US4898982A
公开(公告)日：1990-02-06
申请号：US121151
申请日：1987-11-16
申请人： Gregory P. Hussmann
发明人： Gregory P. Hussmann
IPC分类号： B01J27/25 , B01J23/12 , C07B61/00 , C07C41/00 , C07C41/09 , C07C43/257 , C07C67/00 , C07C319/14 , C07C323/30
CPC分类号： C07C321/00 , C07C41/09
摘要： A method is disclosed for the preparation of diaryl ethers and diaryl sulfides by heating a phenol, a thiophenol, a .beta.-hydroxy-substituted fused armomatic ring-system compound or a .beta.-thio-substituted fused aromatic ring-system compound in the presence of thoria deposited on a neutral support.

7. 发明授权

US4740647A Cyclization catalyst 失效
标题翻译：环化催化剂
公开(公告)号：US4740647A
公开(公告)日：1988-04-26
申请号：US925326
申请日：1986-10-31
申请人： Gregory P. Hussmann , Patrick E. McMahon
发明人： Gregory P. Hussmann , Patrick E. McMahon
IPC分类号： C07C5/31 , C07C5/41
CPC分类号： C07C5/417 , C07C5/31 , C07C2521/02 , C07C2521/04 , C07C2523/72
摘要： Cyclization of aliphatic moieties of 3-20 carbons which comprises contacting a suitable starting compound comprising the aliphatic moiety with a catalyst comprising at least one member selected from the group consisting of copper aluminum borate and zero valent copper on a support comprising aluminum borate under appropriate reaction conditions to obtain a compound having at least one more cyclic moiety than the starting compound. Preferably, the aromatic which undergoes cyclization is an alkenyl group attached to an aromatic nucleus. The present invention can be used to dehydrocyclize alkenylbenzenes to alkylnaphthalenes. In particular, 5-(o-tolyl)pentene can be dehydrocyclized to mixtures of 1,5-, 1,6-, and 2,6-dimethylnaphthalene.
摘要翻译：包括3-20个碳的脂族部分的环化，该方法包括使包含脂族部分的合适起始化合物与包含选自硼酸铜铝和零价铜中的至少一种的催化剂在包含硼酸铝的载体上进行适当反应获得具有比起始化合物至少多一个环状部分的化合物的条件。优选地，经历环化的芳族化合物是连接到芳族核的烯基。本发明可用于将烯基苯脱氢环化成烷基萘。特别地，5-（邻甲苯基）戊烯可以脱氢环化为1,5-，1,6-和2,6-二甲基萘的混合物。

8. 发明授权

US4721815A Preparation of substituted benzophenones 失效
标题翻译：取代的二苯甲酮的制备
公开(公告)号：US4721815A
公开(公告)日：1988-01-26
申请号：US944516
申请日：1986-12-22
申请人： Gregory P. Hussmann , Carl A. Udovich
发明人： Gregory P. Hussmann , Carl A. Udovich
IPC分类号： C07C45/48 , C07C45/65 , C07C49/553
CPC分类号： C07C45/65 , C07C45/48 , C07C49/553
摘要： There is disclosed a process for the preparation of a benzophenone, which process comprises contacting a feed comprising a 3-cyclohexene carboxylic acid in the vapor phase and under suitable conditions with a ketonic decarboxylative coupling catalyst to convert said carboxylic acid into a bis (3-cyclohexene) ketone and contacting said bis (3-cyclohexene) ketone with a dehydrogenation catalyst to dehydrogenate said bis (3-cyclohexene) ketone to provide said benzophenone. Suitably, the coupling catalyst comprises an oxide of manganese. A Group VIII metal-containing catalyst is a typical dehydrogenation catalyst.
摘要翻译：公开了一种制备二苯甲酮的方法，该方法包括在气相中和在合适的条件下将包含3-环己烯羧酸的进料与酮脱羧偶联催化剂接触以将所述羧酸转化成双（3- 环己烯）酮并使所述双（3-环己烯）酮与脱氢催化剂接触以使所述双（3-环己烯）酮脱氢以提供所述二苯甲酮。合适的是，偶联催化剂包括锰的氧化物。含Ⅷ族金属的催化剂是典型的脱氢催化剂。

9. 发明授权

US4783570A Selective gas-phase isomerization of dimethylnaphthalene: 2,7-DMN triad 失效
标题翻译：二甲基萘的选择性气相异构化：2,7-DMN三单元组
公开(公告)号：US4783570A
公开(公告)日：1988-11-08
申请号：US53797
申请日：1987-05-26
申请人： Gregory P. Hussmann , Patrick E. McMahon
发明人： Gregory P. Hussmann , Patrick E. McMahon
IPC分类号： C07C5/27 , C07C5/22
CPC分类号： C07C5/2732 , C07C5/2737 , C07C2529/06 , C07C2529/86
摘要： A gas-phase isomerizaiton process wherein a feed containing one or more members of the 2,7-DMN isomer triad is selectively isomerized over a lower-acidity, supported, molecular-sieve-based catalyst composition to form essentially equilibrium amounts of the members of the 2,7-triad and reduced amounts of outside-the-triad products.
摘要翻译：一种气相异构化方法，其中含有一种或多种2,7- DMN异构体三单元组分的进料在低酸度负载的分子筛基催化剂组合物上选择性异构化，以形成基本平衡量的 2/3三合一和减少的黑社会产品数量。

10. 发明授权

US4783569A Selective gas-phase isomerization of dimethylnaphthalene: 2,6-DMN triad 失效
标题翻译：二甲基萘的选择性气相异构化：2,6-DMN三单元组
公开(公告)号：US4783569A
公开(公告)日：1988-11-08
申请号：US53796
申请日：1987-05-26
申请人： Gregory P. Hussmann , Patrick E. Mc Mahon
发明人： Gregory P. Hussmann , Patrick E. Mc Mahon
IPC分类号： B01J29/04 , B01J29/06 , B01J29/86 , C07B61/00 , C07C1/00 , C07C5/27 , C07C15/24 , C07C67/00 , C07C5/22
CPC分类号： C07C5/2732 , C07C5/2737 , C07C2529/06 , C07C2529/86
摘要： A gas-phase isomerization process wherein a feed containing one or more members of the 2,6-DMN isomer triad is selectively isomerized over a lower-acidity, supported, molecular-sieve-based catalyst composition to form essentially thermodynamic equilibrium amounts of the members of the 2,6-triad and reduced amounts of outside-the-triad products.
摘要翻译：一种气相异构化方法，其中含有一种或多种2,6-DMN异构体三联体成员的进料在低酸度负载的分子筛基催化剂组合物上选择性异构化，以形成基本上热力学平衡量的成员的双三合一和减少的三合一产品。

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