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1. 发明授权

US07070694B2 Purification of fluid compounds utilizing a distillation - membrane separation process 失效
标题翻译：使用蒸馏 - 膜分离方法纯化流体化合物
公开(公告)号：US07070694B2
公开(公告)日：2006-07-04
申请号：US10393054
申请日：2003-03-20
申请人： Craig W. Colling , George A. Huff, Jr. , Stephen J. Pietsch
发明人： Craig W. Colling , George A. Huff, Jr. , Stephen J. Pietsch
IPC分类号： B01D15/00
CPC分类号： C07C7/144 , B01D3/14 , B01D3/322 , B01D53/229 , C07C9/08 , C07C11/06
摘要： Apparatus and processes are disclosed for economical separation of fluid mixtures. Broadly, apparatus of the invention is an integrated fractional distillation and perm-selective membrane separation apparatus. More particularly, the integrated apparatus comprises a fractional distillation column and one or more membrane device utilizing solid perm-selective membranes. Processes of the invention are particularly useful for simultaneous recovery of a very pure permeate product, a desired non-permeate stream, and one or more distillate products from a fluid mixture containing at least two compounds of different boiling point temperatures.
摘要翻译：公开了用于经济分离流体混合物的装置和方法。广义地说，本发明的装置是一体的分馏和渗透选择性膜分离装置。更具体地，该集成装置包括分馏塔和利用固体选择性膜的一个或多个膜装置。本发明的方法特别可用于从含有至少两种不同沸点温度的化合物的流体混合物同时回收非常纯的渗透物产物，期望的非渗透物流和一种或多种馏出物产物。

2. 发明授权

US06881325B2 Preparation of components for transportation fuels 失效
标题翻译：运输燃料组分的制备
公开(公告)号：US06881325B2
公开(公告)日：2005-04-19
申请号：US09779287
申请日：2001-02-08
申请人： George Ernest Morris , Andrew Richard Lucy , William H. Gong , Monica Cristina Regalbuto , George A. Huff, Jr.
发明人： George Ernest Morris , Andrew Richard Lucy , William H. Gong , Monica Cristina Regalbuto , George A. Huff, Jr.
IPC分类号： C10G67/12 , C10G27/04
CPC分类号： C10G67/12
摘要： Economical processes are disclosed for the production of components for refinery blending of transportation fuels by selective oxidation of feedstocks comprising a mixture of hydrocarbons, sulfur-containing and nitrogen-containing organic compounds. Oxidation feedstock is contacted with a soluble quaternary ammonium salt containing halogen, sulfate, or bisulfate anion, and an immiscible aqueous phase comprising a source of hydrogen peroxide, and at least one member of the group consisting of phosphomolybdic acid and phosphotungstic acid, in a liquid reaction mixture under conditions suitable for reaction of one or more of the sulfur-containing and/or nitrogen-containing organic compounds. Blending components containing less sulfur and/or less nitrogen than the oxidation feedstock are recovered from the reaction mixture. Advantageously, at least a portion of the immiscible acid-containing phase is recycled to the oxidation.
摘要翻译：公开了经济方法，用于通过选择性氧化包含烃，含硫和含氮有机化合物的混合物的原料来生产用于运输燃料的炼油厂混合的组分。氧化原料与含有卤素，硫酸盐或硫酸氢盐阴离子的可溶性季铵盐和包含过氧化氢源的不混溶水相和至少一种由磷钼酸和磷钨酸组成的组中的一种在液体中接触反应混合物在适于一种或多种含硫和/或含氮有机化合物的反应条件下进行。从反应混合物中回收含有比氧化原料少的硫和/或更少的氮的混合组分。有利地，至少一部分不混溶的含酸相被再循环至氧化。

3. 发明授权

US6103103A Dehydrogenation catalyst and process 失效
标题翻译：脱氢催化剂和工艺
公开(公告)号：US6103103A
公开(公告)日：2000-08-15
申请号：US250643
申请日：1999-02-16
申请人： Bruce D. Alexander , George A. Huff, Jr. , Mark P. Kaminsky
发明人： Bruce D. Alexander , George A. Huff, Jr. , Mark P. Kaminsky
IPC分类号： B01J23/60 , B01J29/86 , C07C5/333 , C07C5/327 , C10G35/04
CPC分类号： B01J29/86 , C07C5/3337 , B01J23/60 , C07C2521/06 , C07C2521/08 , C07C2523/04 , C07C2523/06 , C07C2523/40 , C07C2523/42 , C07C2523/44 , C07C2523/56 , C07C2523/60 , C07C2529/86
摘要： A process and catalyst are provided for dehydrogenating a hydrocarbon feedstock and producing an olefinic product. The process comprises contacting the feedstock at dehydrogenation conditions with a dehydrogenation catalyst comprising from about 0.01 weight percent to about 5.0 weight percent of a platinum group metal, from about 0.02 weight percent to about 10.0 weight percent of zinc, and a support component comprising borosilicate and an alkali metal.
摘要翻译：提供了一种用于使烃原料脱氢和生产烯烃产物的方法和催化剂。该方法包括在脱氢条件下使原料与脱氢催化剂接触，所述脱氢催化剂包含约0.01重量％至约5.0重量％的铂族金属，约0.02重量％至约10.0重量％的锌，以及包含硼硅酸盐和碱金属。

4. 发明授权

US06025534A Olefin polymerization process 失效
标题翻译：烯烃聚合工艺
公开(公告)号：US06025534A
公开(公告)日：2000-02-15
申请号：US56212
申请日：1998-04-07
申请人： Anthony M. Valente , David B. Johnson , George A. Huff, Jr. , Robert L. Mehlberg
发明人： Anthony M. Valente , David B. Johnson , George A. Huff, Jr. , Robert L. Mehlberg
IPC分类号： C07C2/18 , C08F4/00 , C08F4/06 , C08F10/00 , C10G50/00 , C07C2/02
CPC分类号： C10G50/00 , C07C2/18 , C08F10/00 , C07C2527/173 , Y02P20/584
摘要： A method is provided for regenerating a fixed bed of olefin polymerization catalyst which can be performed without taking the catalyst bed out of service. The method involves the use of two different olefin-containing feedstocks, wherein the first feedstock is a conventional olefin-containing feedstock which contains little if any content of aromatic compounds. The second feedstock contains a significant concentration of aromatic compounds. In the practice of the invention, the second feedstock is substituted for the first feedstock whenever catalyst regeneration is deemed appropriate, and the flow of the second feedstock to the catalyst bed is continued for a period of time which is effective to at least partially regenerate the catalyst.
摘要翻译：提供了一种用于再生烯烃聚合催化剂固定床的方法，其可以在不使催化剂床停止使用的情况下进行。该方法涉及使用两种不同的含烯烃原料，其中第一种原料是常规的含烯烃原料，其含有少量芳族化合物。第二原料含有显着浓度的芳族化合物。在本发明的实践中，当催化剂再生被认为合适时，第二原料代替第一原料，并且将第二原料流向催化剂床的流程持续一段时间，这一时间段至少部分地再生催化剂。

5. 发明授权

US5254781A Olefins process which combines hydrocarbon cracking with coupling methane 失效
标题翻译：将烃裂解与偶联甲烷相结合的烯烃工艺
公开(公告)号：US5254781A
公开(公告)日：1993-10-19
申请号：US815244
申请日：1991-12-31
申请人： Narasimhan Calamur , George A. Huff, Jr. , Harold A. Lindahl
发明人： Narasimhan Calamur , George A. Huff, Jr. , Harold A. Lindahl
IPC分类号： B01J8/00 , B01J19/24 , B01J23/10 , B01J23/14 , C07B61/00 , C07C2/84 , C07C4/04 , C07C5/48 , C07C11/02 , C07C11/04 , C07C11/06 , C10G9/00 , C10G9/36 , C10G50/00 , C10G57/00 , C07C2/00
CPC分类号： C10G57/00 , B01J19/2475 , B01J23/10 , B01J23/14 , B01J8/009 , C07C2/84 , C07C4/04 , C07C5/48 , B01J2219/00063 , B01J2219/00117 , B01J2219/00126 , B01J2219/00155 , C07C2521/02 , C07C2521/06 , C07C2523/02 , C07C2523/08 , C07C2523/10 , C07C2523/14 , Y10S585/91 , Y10S585/911 , Y10S585/943
摘要： An olefins process is described which combines cracking of a hydrocarbon feedstock with the coupling of methane using an oxygen-affording gas such that the heat evolved in the exothermic methane coupling reaction is effectively transferred to the endothermic cracking process in a manner which does not allow the non-hydrocarbon products in the effluent of the methane coupling reaction to mix with the effluent of the cracking process. By combining the cryogenic requirements of the two processes, the refrigeration used in air liquifaction to separate oxygen for the methane coupling process can provide refrigerant nitrogen to liquify one or more of methane, ethylene and propylene which can be used in the cryogenic separation of the C.sub.2 + hydrocarbon products in the cracking process effluent.
摘要翻译：描述了一种烯烃方法，其将烃原料的裂化与使用氧气提供气体的甲烷的偶合组合，使得在放热甲烷偶合反应中放出的热量有效地转移到吸热裂解过程中，其方式不允许非烃类产物在流出物中的甲烷偶联反应与流出物的裂解过程混合。通过结合两种方法的低温要求，用于空气液化以分离用于甲烷耦合过程的氧气的制冷可以提供制冷剂氮以液化一种或多种甲烷，乙烯和丙烯，其可用于C2 + 烃类产物在裂解过程中的流出物。

6. 发明授权

US4939311A Catalysts for the oxidative conversion of methane to higher hydrocarbons 失效
标题翻译：用于将甲烷氧化转化成高级烃的催化剂
公开(公告)号：US4939311A
公开(公告)日：1990-07-03
申请号：US233063
申请日：1988-08-17
申请人： Don M. Washecheck , Aileen E. Alvarado-Swaisgood , Mark P. Kaminsky , Mark S. Kleefisch , George A. Huff, Jr.
发明人： Don M. Washecheck , Aileen E. Alvarado-Swaisgood , Mark P. Kaminsky , Mark S. Kleefisch , George A. Huff, Jr.
IPC分类号： B01J23/14 , C07C2/84
CPC分类号： B01J23/14 , C07C2/84 , C07C2523/02 , C07C2523/10 , C07C2523/14 , Y10S585/934
摘要： An oxidative coupling catalyst composition for converting methane to a higher hydrocarbon comprising a mixed oxide of: (a) a Group IIIB metal selected from the grouup consisting of yttrium, scandium and lanthanum; (b) a Group IIA metal selected from the group consisting of barium, calcium and strontium; and (c) a Group IVA metal selected from the group consisting of tin, lead and germanium and approximate ratio of 1:0.5-3:2-4, and an improved process employing same.
摘要翻译：一种用于将甲烷转化为高级烃的氧化偶联催化剂组合物，其包含以下混合氧化物：（a）选自由钇，钪和镧组成的组的IIIB族金属; （b）选自钡，钙和锶的IIA族金属; 和（c）选自锡，铅和锗的ⅣA族金属和近似比例为1:0.5-3:2-4，以及使用其的改进方法。

7. 发明授权

US07618468B2 Transportation fuels 失效
公开(公告)号：US07618468B2
公开(公告)日：2009-11-17
申请号：US11081062
申请日：2005-03-15
申请人： George A. Huff, Jr. , William H. Gong , Leslie R. Wolf , John C. Eckstrom , Douglas N. Rundell , Michael Hodges , Monica Cristina Regalbuto
发明人： George A. Huff, Jr. , William H. Gong , Leslie R. Wolf , John C. Eckstrom , Douglas N. Rundell , Michael Hodges , Monica Cristina Regalbuto
IPC分类号： C10L1/18
CPC分类号： C10L1/02 , C10G27/04 , C10G27/10 , C10L1/026
摘要： The present invention relates to Compositions of fuels for transportation are disclosed, particularly organic compositions which are liquid at ambient conditions. More specifically, it relates to transportation fuels comprising suitable organic distillates, as a predominant component, and limited, but essential, amounts of a component comprising oxygen-containing organic materials, which materials are typically derived from natural petroleum. Beneficially, the oxygen content of these transportation fuels is at least 0.02 percent by weight. Preferably the oxygen content these transportation fuels is in a range from about 0.2 percent to about 10 percent by weight.

8. 发明授权

US07381858B2 Xylene process using perm-selective separations 失效
标题翻译：二甲苯工艺使用烫发选择性分离
公开(公告)号：US07381858B2
公开(公告)日：2008-06-03
申请号：US10769539
申请日：2004-01-30
申请人： George A. Huff, Jr. , Bo Chen , Craig W. Colling , Jeffrey T. Miller
发明人： George A. Huff, Jr. , Bo Chen , Craig W. Colling , Jeffrey T. Miller
IPC分类号： C07C7/144
CPC分类号： C07C7/144 , C07C15/08
摘要： Processes are disclosed for production of purified products from a fluid mixtures of C8 aromatics by means of integration of perm-selective separations with purified product recovery operations. The perm-selective separations of the invention comprise of one or more devices using polymeric perm-selective membrane devices to separate a meta-xylene enriched stream from fluid mixtures of C8 aromatics thereby producing a fluid comprising the remaining aromatic compounds which advantageously includes para-xylene. Processes of the invention are particularly useful for recovery of very pure meta-xylene and para-xylene co-products from liquid mixtures even containing ethylbenzene as well as the three xylene isomers.
摘要翻译：公开了通过将选择性分选与纯化的产物回收操作相结合从C 8芳烃的流体混合物生产纯化产物的方法。本发明的烫发选择性分离包括使用聚合物选择性选择性膜装置的一种或多种装置，用于将富二甲苯富集流与C 8芳烃的流体混合物分离，从而产生包含剩余的有利地包括对二甲苯的芳族化合物。本发明的方法特别可用于从甚至含有乙苯的液体混合物以及三种二甲苯异构体中回收非常纯的间二甲苯和对二甲苯共产物。

9. 发明授权

US06827845B2 Preparation of components for refinery blending of transportation fuels 失效
标题翻译：炼油厂混合运输燃料零部件的准备
公开(公告)号：US06827845B2
公开(公告)日：2004-12-07
申请号：US09779285
申请日：2001-02-08
申请人： William H. Gong , Monica Cristina Regalbuto , George A. Huff, Jr.
发明人： William H. Gong , Monica Cristina Regalbuto , George A. Huff, Jr.
IPC分类号： C10G6702
CPC分类号： C10G53/14
摘要： Economical processes are disclosed for the production of components for refinery blending of transportation fuels by selective oxidation of feedstocks comprising a mixture of hydrocarbons, sulfur-containing and nitrogen-containing organic compounds. Oxidation feedstock is contacted with an immiscible phase comprising at least one organic peracid or precursors of organic peracid in a liquid phase reaction mixture maintained substantially free of catalytic active metals and/or active metal-containing compounds and under conditions suitable for oxidation of one or more of the sulfur-containing and/or nitrogen-containing organic compounds. Blending components containing less sulfur and/or less nitrogen than the oxidation feedstock are recovered from the reaction mixture. Advantageously, at least a portion of the immiscible acid-containing phase is recycled to the oxidation.
摘要翻译：公开了经济方法，用于通过选择性氧化包含烃，含硫和含氮有机化合物的混合物的原料来生产用于运输燃料的炼油厂混合的组分。氧化原料与基本上不含催化活性金属和/或含活性金属的化合物的液相反应混合物中的至少一种有机过酸或有机过酸的前体的不混溶相接触，并在适于氧化一种或多种的含硫和/或含氮有机化合物。从反应混合物中回收含有比氧化原料少的硫和/或更少的氮的混合组分。有利地，至少一部分不混溶的含酸相被再循环至氧化。

10. 发明授权

US06673230B2 Process for oxygenation of components for refinery blending of transportation fuels 失效
标题翻译：用于运输燃料炼油厂混合的组分的氧化过程
公开(公告)号：US06673230B2
公开(公告)日：2004-01-06
申请号：US09779286
申请日：2001-02-08
申请人： Gary P. Hagen , George A. Huff, Jr. , William H. Gong , Monica Cristina Regalbuto
发明人： Gary P. Hagen , George A. Huff, Jr. , William H. Gong , Monica Cristina Regalbuto
IPC分类号： C07C2712
CPC分类号： C10G27/04 , C10G27/12 , C10G53/14 , C10G67/12
摘要： Economical processes are disclosed for production of components for refinery blending of transportation fuels which are liquid at ambient conditions by selective oxygenation of refinery feedstocks comprising a mixture of organic compounds. The organic compounds are oxygenated in a liquid reaction medium with an oxidizing agent and heterogeneous oxygenation catalyst system which exhibits a capability to enhance the incorporation of oxygen into a mixture of liquid organic compounds to form a mixture comprising hydrocarbons, oxygenated organic compounds, water of reaction, and acidic co-products. The mixture is separated to recover at least a first organic liquid of low density and at least a portions of the catalyst metal, water of reaction and acidic co-products. Advantageously, the organic liquid is washed with an aqueous solution of sodium bicarbonate solution, or other soluble chemical base capable to neutralize and/or remove acidic co-products of oxidation, and recover oxygenated product.
摘要翻译：公开了经济方法，用于生产用于在环境条件下通过选择性氧化含有有机化合物的混合物的炼油原料的运输燃料的炼油厂混合的组分。有机化合物在具有氧化剂和多相氧化催化剂体系的液体反应介质中进行氧化，其显示出能够增强氧引入液体有机化合物的混合物中以形成包含烃，含氧有机化合物，反应水的混合物的能力，和酸性副产物。分离混合物以回收至少第一低密度有机液体和至少一部分催化剂金属，反应水和酸性共同产物。有利地，有机液体用碳酸氢钠溶液的水溶液或能够中和和/或除去酸性氧化副产物的其它可溶性化学碱洗涤，并回收氧合产物。

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