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1. 发明授权

US07999103B2 Metal complex compound and organic electroluminescence device using the compound 有权
标题翻译：金属络合物和使用该化合物的有机电致发光器件
公开(公告)号：US07999103B2
公开(公告)日：2011-08-16
申请号：US11608494
申请日：2006-12-08
申请人： Masa-aki Haga , Li-fen Yang , Masumi Itabashi , Misa Ashizawa , Fumio Okuda
发明人： Masa-aki Haga , Li-fen Yang , Masumi Itabashi , Misa Ashizawa , Fumio Okuda
IPC分类号： C07F15/00 , H01L51/50
CPC分类号： H05B33/10 , C07F15/0033 , C09K11/06 , C09K2211/1007 , C09K2211/1029 , C09K2211/1044 , C09K2211/185 , H01L51/0085 , H01L51/5016
摘要： Provided are an organic electroluminescence device whose wavelength of light emission is short and which can emit blue light having a high color purity, and a metal complex compound for realizing the device. The metal complex compound is of a specific structure having a partial structure including two tridentate ligands. The organic electroluminescence device includes: a pair of electrodes; and an organic thin film layer which has one layer or a plurality of layers including at least a light emitting layer and is disposed between the pair of electrodes. In the organic electroluminescence device, at least one layer of the organic thin film layer contains the metal complex compound. The organic electroluminescence device emits light by applying a voltage between both the electrodes.
摘要翻译：提供一种发光波长短且可以发出高纯度的蓝色光的有机电致发光元件，以及用于实现该器件的金属络合物。金属络合物具有包含两个三齿配体的部分结构的特定结构。有机电致发光器件包括：一对电极; 以及具有至少包含发光层并且设置在所述一对电极之间的一层或多层的有机薄膜层。在有机电致发光器件中，有机薄膜层的至少一层含有金属络合物。有机电致发光器件通过在两个电极之间施加电压而发光。

2. 发明授权

US07625639B2 Metal-complex compound and organic electroluminescence device using the compound 失效
标题翻译：金属络合物和使用该化合物的有机电致发光器件
公开(公告)号：US07625639B2
公开(公告)日：2009-12-01
申请号：US11270500
申请日：2005-11-10
申请人： Masa-aki Haga , Fumio Okuda
发明人： Masa-aki Haga , Fumio Okuda
IPC分类号： H01L51/54 , C09K11/06
CPC分类号： H01L51/0085 , C07F15/0033 , C09K11/06 , C09K2211/1029 , C09K2211/1044 , C09K2211/185 , H05B33/14 , Y10S428/917
摘要： A metal-complex compound which comprises a tridentate chelate ligand having a specified partial structure. An organic electroluminescence device which comprises at least one organic thin film layer sandwiched between a pair of electrode consisting of an anode and a cathode, wherein the organic thin film layer comprises the metal-complex compound, which emits light by applying an electric voltage between the pair of electrode. The present invention provides an organic EL device which emits blue light with high purity and of short wavelength with an enhanced efficiency of light emission.
摘要翻译：一种金属络合物，其包含具有特定部分结构的三齿螯合配位体。一种有机电致发光器件，其包括夹在由阳极和阴极组成的一对电极之间的至少一个有机薄膜层，其中所述有机薄膜层包含金属络合物，所述金属络合物通过在所述金属络合物之间施加电压而发光一对电极。本发明提供了发射高纯度和短波长的蓝光并提高发光效率的有机EL器件。

3. 发明申请

US20090085469A1 LUMINESCENT METAL COMPLEX, METHOD FOR PRODUCING SAME AND ORGANIC ELECTROLUMINESCENT LIGHT-EMITTING DEVICE USING SAME 审中-公开
标题翻译：发光金属复合物，其制造方法和使用其的有机电致发光发光装置
公开(公告)号：US20090085469A1
公开(公告)日：2009-04-02
申请号：US11817738
申请日：2006-02-27
申请人： Fumio Okuda , Masami Watanabe , Hidetsugu Ikeda
发明人： Fumio Okuda , Masami Watanabe , Hidetsugu Ikeda
IPC分类号： H01J1/63 , C07F15/00
CPC分类号： C09K11/06 , C07F15/0033 , C09K2211/185 , H01L51/0062 , H01L51/0079 , H01L51/0085 , H01L51/5016 , H05B33/14
摘要： A metal complex compound with a structure containing metals such as iridium, and a monodentate ligand such as a hydrogen atom other than a bidentate ligand. An employment of a metal compound with a ligand having two oxygen atoms as a material for preparing the metal complex compound. An organic electroluminescence device being composed of one or more organic thin film layers having at least a light emitting layer sandwiched between a pair of electrodes wherein at least one of the organic thin film layer contains the metal complex compound. The organic electroluminescence device has an excellent stability, a great efficiency and a long lifetime of light emission due to the metal complex compound.
摘要翻译：具有含有金属如铱的结构的金属络合物和除双齿配体以外的单齿配体如氢原子。使用具有两个氧原子的配体的金属化合物作为制备金属络合物的材料。一种有机电致发光器件，由一层或多层有机薄膜层构成，所述有机薄膜层至少具有夹在一对电极之间的发光层，其中至少一个有机薄膜层含有金属络合物。有机电致发光元件由于金属络合物而具有优异的稳定性，高效率和长的发光寿命。

4. 发明申请

US20070138437A1 METAL COMPLEX COMPOUND AND ORGANIC ELECTROLUMINESCENCE DEVICE USING THE COMPOUND 有权
标题翻译：金属复合化合物和使用该化合物的有机电致发光器件
公开(公告)号：US20070138437A1
公开(公告)日：2007-06-21
申请号：US11608494
申请日：2006-12-08
申请人： Masa-aki Haga , Li-fen Yang , Masumi Itabashi , Misa Ashizawa , Fumio Okuda
发明人： Masa-aki Haga , Li-fen Yang , Masumi Itabashi , Misa Ashizawa , Fumio Okuda
IPC分类号： C09K11/06
CPC分类号： H05B33/10 , C07F15/0033 , C09K11/06 , C09K2211/1007 , C09K2211/1029 , C09K2211/1044 , C09K2211/185 , H01L51/0085 , H01L51/5016
摘要： Provided are an organic electroluminescence device whose wavelength of light emission is short and which can emit blue light having a high color purity, and a metal complex compound for realizing the device. The metal complex compound is of a specific structure having a partial structure including two tridentate ligands. The organic electroluminescence device includes: a pair of electrodes; and an organic thin film layer which has one layer or a plurality of layers including at least a light emitting layer and is disposed between the pair of electrodes. In the organic electroluminescence device, at least one layer of the organic thin film layer contains the metal complex compound. The organic electroluminescence device emits light by applying a voltage between both the electrodes.
摘要翻译：提供一种发光波长短且可以发出高纯度的蓝色光的有机电致发光元件，以及用于实现该器件的金属络合物。金属络合物具有包含两个三齿配体的部分结构的特定结构。有机电致发光器件包括：一对电极; 以及具有至少包含发光层并且设置在所述一对电极之间的一层或多层的有机薄膜层。在有机电致发光器件中，有机薄膜层的至少一层含有金属络合物。有机电致发光器件通过在两个电极之间施加电压而发光。

5. 发明申请

US20060163542A1 Metal-complex compound and organic electroluminescence device using the compound 审中-公开
标题翻译：金属络合物和使用该化合物的有机电致发光器件
公开(公告)号：US20060163542A1
公开(公告)日：2006-07-27
申请号：US11295600
申请日：2005-12-07
申请人： Ryusuke Watanabe , Fumio Okuda , Keiko Yamamichi , Toshihiro Iwakuma , Seiji Tomita
发明人： Ryusuke Watanabe , Fumio Okuda , Keiko Yamamichi , Toshihiro Iwakuma , Seiji Tomita
IPC分类号： H01B1/12
CPC分类号： C09K11/06 , C07F15/0033 , C09K2211/1029 , C09K2211/185 , H01L51/0059 , H01L51/0061 , H01L51/0071 , H01L51/0072 , H01L51/0081 , H01L51/0085 , H01L51/5012 , H05B33/14
摘要： A metal-complex compound having a special structure containing metals such as iridium. An organic electroluminescence device which comprises at least one organic thin film layer sandwiched between a pair of electrodes, wherein the organic thin film layer comprises the metal-complex compound. The organic electroluminescence device employing the metal-complex compound exhibits an enhanced current efficiency and prolonged lifetime.
摘要翻译：具有含有金属如铱的特殊结构的金属络合物。一种有机电致发光器件，其包括夹在一对电极之间的至少一个有机薄膜层，其中所述有机薄膜层包含所述金属络合物。使用金属络合物的有机电致发光器件具有增强的电流效率和延长的寿命。

6. 发明申请

US20060159954A1 Metal-complex compound and organic electroluminescence device using the compound 审中-公开
标题翻译：金属络合物和使用该化合物的有机电致发光器件
公开(公告)号：US20060159954A1
公开(公告)日：2006-07-20
申请号：US11269808
申请日：2005-11-09
申请人： Masa-aki Haga , Taro Tsubomura , Fumio Okuda
发明人： Masa-aki Haga , Taro Tsubomura , Fumio Okuda
IPC分类号： H01L51/54 , H05B33/14 , C09K11/06 , C07C213/02
CPC分类号： C07D213/26 , C07D213/22 , C07D213/53 , C07D213/61 , C07D401/14 , C07D413/14 , C07F13/005 , C07F15/0033 , C07F15/004 , C07F15/0053 , C07F15/0093 , C09B57/00 , C09B57/10 , H01L51/0052 , H01L51/0081 , H01L51/0085 , H01L51/5012 , H01L51/5048 , H01L51/5052
摘要： A metal-complex compound which comprises a tridentate chelate ligand and a cyano group ligand having a specified partial structure. An organic electroluminescence device which comprises at least one organic thin film layer sandwiched between a pair of electrodes consisting of an anode and a cathode, wherein the organic thin film layer comprises the metal-complex compound, which emits light by applying an electric voltage between the pair of electrodes. The present invention provides an organic EL device which emits blue light of high purity and of short wavelength with an enhanced current efficiency.
摘要翻译：一种金属络合物，其包含具有特定部分结构的三齿螯合配体和氰基配体。一种有机电致发光器件，其包括被夹在由阳极和阴极组成的一对电极之间的至少一个有机薄膜层，其中所述有机薄膜层包括金属络合物，所述金属络合物通过施加电压一对电极。本发明提供一种发射具有高纯度和短波长的蓝光并提高电流效率的有机EL器件。

7. 发明授权

US06462155B1 Catalyst for olefin polymerization and process for producing olefin polymer with the catalyst 失效
标题翻译：用于烯烃聚合的催化剂和用催化剂生产烯烃聚合物的方法
公开(公告)号：US06462155B1
公开(公告)日：2002-10-08
申请号：US09582638
申请日：2000-08-03
申请人： Fumio Okuda
发明人： Fumio Okuda
IPC分类号： C08F442
CPC分类号： C08F10/00 , C08F10/02 , C08F110/02 , C08F2500/17 , C08F4/7042
摘要： The invention provides a catalyst comprising a transition metal compound which has a nitrogen-containing tridentate ligand and of which the transition metal is of Groups 8 to 10 of the Periodic Table, and an organoaluminium compound, the catalyst of the invention has high activity. In the method of using the catalyst for producing polyolefins, of which the advantages are that the catalysts do not require methylaluminoxane which is expensive and difficult to handle, and of which storage stability is poor, and is extremely dangerous. The invention realizes efficient production of polyolefins (especially polyethylene) on an industrial scale.
摘要翻译：本发明提供了含有含氮三齿配位体，过渡金属为周期表第8〜10族的过渡金属化合物和有机铝化合物的催化剂，本发明的催化剂具有高活性。在使用催化剂制造聚烯烃的方法中，优点在于催化剂不需要昂贵且难以处理的甲基铝氧烷，其储存稳定性差，极其危险。本发明实现了工业规模的聚烯烃（特别是聚乙烯）的有效生产。

8. 发明授权

US06335405B1 Catalysts for olefin polymer production and process for producing olefin polymer 失效
标题翻译：用于烯烃聚合物生产的催化剂和用于生产烯烃聚合物的方法
公开(公告)号：US06335405B1
公开(公告)日：2002-01-01
申请号：US09423655
申请日：1999-12-13
申请人： Fumio Okuda , Haruhito Sato , Toshiya Abiko
发明人： Fumio Okuda , Haruhito Sato , Toshiya Abiko
IPC分类号： C08F442
CPC分类号： C08F10/00 , C08F10/02 , C08F110/02 , C08F2410/01 , C08F4/80 , C08F4/025 , C08F2500/17 , C08F2500/08 , C08F4/7006
摘要： Catalysts for olefin polymerization comprising (a) a compound of a transition metal of Groups 8 to 10 of the Periodic Table, (b) clay, a clay mineral or an ion-exchanging layered compound, (c) a silane compound, and optionally (d) an organic aluminium compound and/or (e) an alkylating agent, and those comprising (a) a compound of a transition metal of Groups 8 to 10 of the Periodic Table, (b) clay, a clay mineral or an ion-exchanging layered compound, (d) an organic aluminium compounds and optionally (e) an alkylating agent have high activity, though not containing a large amount of aluminoxane. Using the catalysts, high-quality olefin polymers with good morphology are produced efficiently. The amount of the residual metal to remain in the polymers produced is small.
摘要翻译：用于烯烃聚合的催化剂包括（a）周期表第8-10族过渡金属的化合物，（b）粘土，粘土矿物或离子交换层状化合物，（c）硅烷化合物和任选的（ d）有机铝化合物和/或（e）烷基化剂，以及包含（a）周期表第8〜10族的过渡金属的化合物的组合物，（b）粘土，粘土矿物或离子交换树脂，交换层状化合物，（d）有机铝化合物和任选的（e）烷基化剂具有高活性，尽管不含有大量的铝氧烷。使用催化剂，有效地生产具有良好形态的高品质烯烃聚合物。残留在所生产的聚合物中的残余金属的量很小。

9. 发明授权

US5336803A Process for producing an organic carbonate 失效
标题翻译：生产有机碳酸酯的方法
公开(公告)号：US5336803A
公开(公告)日：1994-08-09
申请号：US848117
申请日：1992-03-09
申请人： Hiroaki Kezuka , Fumio Okuda
发明人： Hiroaki Kezuka , Fumio Okuda
IPC分类号： B01J31/28 , C07B61/00 , C07C68/00 , C07C69/96
CPC分类号： C07C68/005
摘要： A process for producing an organic carbonate which comprises reacting an organic hydroxy compound, carbon monoxide and oxygen in the presence of a catalyst comprising(a) palladium or a palladium compound, (b) a cuprous or cupric compound such as cupric acetate, (c) a quinone or an aromatic diol formed by reduction of the quinone or a mixture thereof such as hydroquinone, and (d) a halogenated onium compound such as (C.sub.4 H.sub.9)NBr is disclosed.According to the invention, an organic carbonate such as diphenyl carbonate can be produced efficiently and economically.
摘要翻译：一种制备有机碳酸酯的方法，其包括在催化剂存在下使有机羟基化合物，一氧化碳和氧反应，所述催化剂包含（a）钯或钯化合物，（b）亚铜或铜化合物如乙酸铜，（c ）通过还原醌或其混合物如氢醌形成的醌或芳族二醇，和（d）卤化鎓化合物如（C 4 H 9）NBr。根据本发明，可以有效且经济地制造碳酸二苯酯等有机碳酸酯。

10. 发明授权

US08778510B2 Pyrromethene-boron complex compounds and organic electroluminescent elements using same 有权
标题翻译：吡咯并 - 硼络合物和使用其的有机电致发光元件
公开(公告)号：US08778510B2
公开(公告)日：2014-07-15
申请号：US13138501
申请日：2010-02-25
申请人： Fumio Okuda , Kiyoshi Ikeda , Takayasu Sado , Takahiko Ochi , Yoshimitsu Tanabe , Bunji Sawano
发明人： Fumio Okuda , Kiyoshi Ikeda , Takayasu Sado , Takahiko Ochi , Yoshimitsu Tanabe , Bunji Sawano
IPC分类号： H01L51/54 , C07F5/04
CPC分类号： C07D403/06 , C07D207/44 , C07D209/44 , C07F5/022 , C09K11/06 , C09K2211/1022 , C09K2211/1029 , H01L51/0054 , H01L51/008 , H01L51/5012 , H05B33/14
摘要： A pyrromethene-boron complex compound represented by the following formula (1); wherein Z1 and Z2 are independently a hydrogen atom, a substituted or unsubstituted aryl group, a substituted or unsubstituted alkoxy group or a substituted or unsubstituted aryloxy group, at least one of Z1 and Z2 is an alkoxy group substituted with a fluorine atom or an aryloxy group substituted with a fluorine atom or a fluoroalkyl group, and Z1 and Z2 may form a ring.
摘要翻译：由下式（1）表示的亚甲基吡咯 - 硼络合物; 其中Z1和Z2独立地是氢原子，取代或未取代的芳基，取代或未取代的烷氧基或取代或未取代的芳氧基，Z1和Z2中的至少一个是被氟原子取代的烷氧基或芳氧基被氟原子或氟烷基取代的基团，Z1和Z2可以形成环。

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