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    • 2. 发明授权
    • HCT Crystal growth method
    • HCT晶体生长法
    • US4545848A
    • 1985-10-08
    • US439800
    • 1982-11-08
    • Sandor L. LehoczkyFrank R. Szofran
    • Sandor L. LehoczkyFrank R. Szofran
    • C30B11/00C30B21/02
    • C30B11/00C30B29/48
    • A method of preparing pseudobinary mercury, cadmium, telluride (HCT) crystals by controlled crystal growth in a fused silica ampule uses a modified Bridgman-Stockbarger method. In this method, the alloy is cast into one end of the ampule, inverted, heated to a temperature between the liquidus and solidus temperatures of the alloy and directionally solidified in a two zone furnace. The parameters of the solidification treatment are controlled according to the formulaT.sub.U.sup.4 -T.sub.I.sup.4 =T.sub.I.sup.4 -T.sub.L.sup.4,where T.sub.U =the temperature of the furnace upper zone, T.sub.L =the temperature of the furnace lower zone, and T.sub.I =the solidus temperature of the crystal composition. The rate of transfer of the crystal through the furnace and the size of the zone barrier are also controlled. The modified method imparts homogeneity to the crystal composition, both axially of the crystal and radially. The crystals produced by the method have superior properties and a much higher yield.
    • 通过熔融二氧化硅安瓿中受控晶体生长制备假二元汞,镉,碲化物(HCT)晶体的方法使用改进的Bridgman-Stockbarger方法。 在该方法中,将合金铸造到安瓿的一端,倒置,加热到合金的液相线和固相线温度之间的温度,并在两区域炉中定向凝固。 凝固处理的参数根据公式TU4-TI4 = TI4-TL4进行控制,其中TU =炉上部区域的温度,TL =炉下部区域的温度,TI =晶体的固相线温度 组成。 晶体通过炉的转移速率和区域阻挡层的尺寸也受到控制。 该改性方法在晶体的轴向和径向上均匀地赋予晶体组成。 该方法生产的晶体具有优异的性能和更高的收率。