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    • 4. 发明申请
    • Method and automatic system for non-destructive determination physical-chemical properties of powdered materials
    • 粉末材料的非破坏性物理化学性质的方法和自动化系统
    • US20090267623A1
    • 2009-10-29
    • US12386823
    • 2009-04-23
    • Volodymyr I. RedkoElena M. ShembelVolodymyr S. KhandetskyyDayal T. MeshriIsaac A. AngresRobert AdamsDmytro SivtsovOxana V. Red'koTymofiy V. Pastushkin
    • Volodymyr I. RedkoElena M. ShembelVolodymyr S. KhandetskyyDayal T. MeshriIsaac A. AngresRobert AdamsDmytro SivtsovOxana V. Red'koTymofiy V. Pastushkin
    • G01R27/26
    • G01N27/221
    • The present invention is a method and related automatic system for non-destructive determination of physical-chemical properties of powdered in particular as related to the quality control of powdered materials used in battery industry, for example determination of carbon monofluoride (CFx) degree of fluorination during the process of CFx synthesis. The invention consists of: scanner, which is used for movable measuring transducer within three co-ordinates; measuring generator containing electro capacitive sensor, which is used as an element of a resonance circuit; base generator similar (identical with) to the measuring one; block for subtraction the frequencies of the measuring and base generators; block of measuring the Q-factor of the resonance circuit together with an electro capacitive sensor; block for identifying extramal point of dependence of capacitive sensor capacitance upon time; block for comparative analysis of the Q-factor of the resonance circuit of the measuring autogenerator and capacitance of capacitive sensor; block for extrapolation of time dependence of capacitance of capacitive sensor at the moment when it is inserted into powder; block for computing the difference between the factual and extrapolated values of capacitance of capacitive sensor while the sensor is being inserted into powder; calibration block and registration block.
    • 本发明是一种方法和相关的自动化系统,用于非破坏性地确定粉末的物理化学性质,特别是与电池工业中使用的粉末材料的质量控制有关,例如氟化一氟化碳(CFx)的测定 在CFx合成过程中。 本发明包括:扫描仪,用于三坐标内的可移动测量传感器; 含有电容式传感器的测量发生器,其用作谐振电路的元件; 基座发生器与测量仪相似(相同); 用于减去测量和基础发生器的频率的块; 与电容式传感器一起测量谐振电路的Q因子的块; 用于识别电容式传感器电容随时间的依赖性的外部块; 测量自动发生器的谐振电路的Q因子和电容式传感器的电容的比较分析块; 用于插入电容式传感器插入粉末时的电容时间依赖性的块; 块,用于计算传感器插入粉末时电容式传感器电容的事实和外推值之间的差异; 校准块和注册块。