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1. 发明授权

US06770702B1 Polymer 失效
标题翻译：聚合物
公开(公告)号：US06770702B1
公开(公告)日：2004-08-03
申请号：US10030526
申请日：2002-04-16
申请人： Horst Muller , Hans-Dieter Hille
发明人： Horst Muller , Hans-Dieter Hille
IPC分类号： C08J300
CPC分类号： C08F265/04 , C08F265/06 , C08F283/006 , C08F285/00 , C09D17/00 , C09D151/003 , C09D175/04 , Y10S525/902
摘要： Polymer obtainable by a multistage polymerization process which involves conducting, in a first step, an aqueous-phase polymerization of at least one ethylenically monofunctional compound alone or together with at least one ethylenically difunctional or poly-functional compound together in the presence of a polyesterpolyol, polyurethane and/or polyacrylate; and, in a subsequent step, a reaction of the resulting product with at least one ethylenically monofunctional compound alone or together with at least one ethylenically difunctional or polyfunctional compound; followed by a reaction of the resulting product with a crosslinker; and its use.
摘要翻译：通过多阶段聚合方法可获得的聚合物，其包括在第一步骤中，在聚酯多元醇存在下，单独或与至少一种烯键式双官能或多官能化合物一起进行至少一种烯键式单官能化合物的水相聚合，聚氨酯和/或聚丙烯酸酯; 并且在随后的步骤中，所得产物与至少一种烯属单官能化合物单独或与至少一种烯键式双官能或多官能化合物反应; 随后将所得产物与交联剂反应; 及其用途。

2. 发明授权

US6043301A Aqueous coating compositions 失效
标题翻译：水性涂料组合物
公开(公告)号：US6043301A
公开(公告)日：2000-03-28
申请号：US750046
申请日：1997-04-14
申请人： Hans-Dieter Hille , Horst Muller
发明人： Hans-Dieter Hille , Horst Muller
IPC分类号： C08G18/63 , C08L51/08 , C09D151/08 , C09D161/20 , C09D167/06 , C08K5/05
CPC分类号： C09D161/20 , C08G18/635 , C09D151/08 , C09D167/06 , C08L51/08
摘要： The invention relates to aqueous coating compositions comprising:an aqueous, polyester- and acrylate-based polymer dispersion obtainable by free-radical polymerization of at least:a. one (meth)acrylic acid ester;b. one ethylenically unsaturated, at least monofunctional acid; and optionallyc. one ethylenically unsaturated monomer other than (a) and (b)or mixtures thereof, with a poly ester resin capable of undergoing a free-radical polymerization;one amino resin as crosslinking agent,one water-soluble and/or water-emulsifiable polyalcohol and optionally conventional laquer additives.Furthermore, the invention relates to the use of these aqueous coating compositions as clear coats for the preparation of multi-layer coatings.
摘要翻译： PCT No.PCT / EP95 / 01982 Sec。 371日期1997年04月14日 102（e）1997年4月14日PCT PCT 1996年5月25日PCT公布。出版物WO95 / 33011 日期1995年12月7日本发明涉及水性涂料组合物，其包含：通过至少a的自由基聚合可获得的水性聚酯和丙烯酸酯基聚合物分散体。一种（甲基）丙烯酸酯; b。一种烯属不饱和的，至少单官能的酸; 并且可选地c。一种除（a）和（b）之外的烯属不饱和单体或其混合物与能够进行自由基聚合的聚酯树脂; 一种氨基树脂作为交联剂，一种水溶性和/或水可乳化的多元醇和任选的常规的漆添加剂。此外，本发明涉及这些水性涂料组合物作为透明涂层用于制备多层涂层的用途。

3. 发明授权

US5977258A Microgel 失效
标题翻译：微凝胶
公开(公告)号：US5977258A
公开(公告)日：1999-11-02
申请号：US875858
申请日：1997-11-21
申请人： Hans-Dieter Hille , Stephan Neis , Horst Muller
发明人： Hans-Dieter Hille , Stephan Neis , Horst Muller
IPC分类号： B01J13/00 , C08F2/22 , C08F2/24 , C08F283/02 , C08J3/075 , C08L67/00 , C09D7/12 , C09D167/00 , C08F8/00 , C08J3/00 , C08K3/20 , C08L67/06
CPC分类号： C08L67/00 , B01J13/0052 , C08F283/02 , C08J3/075 , C09D167/00 , C09D7/125
摘要： A microgel obtained by polymerizing in aqueous phase a monomer blend comprising at least one ethylenic monofunctional compound, selected from the group consisting of vinylic compounds, alkyl esters of acrylic or methacrylic acid, hydroxyalkyl (meth)acrylates and vinyl acetate, and at least one ethylenic di- or multifunctional compound, selected from the group consisting of diacrylates, triacrylates and/or (meth)acrylates of polyfunctional alcohols, in the presence of a polycondensation product of a polycarboxylic acid, polyhydroxycarboxylic acid, hydroxypolycarboxylic acid and/or polyhydroxypolycarboxylic acid with a polyol, and its use for aqueous or solvent-containing coating compositions, in particular for aqueous or solvent-containing base coats, effect base coats or clear coat systems in the motorcar industry.
摘要翻译： PCT No.PCT / DE96 / 00067 Sec。 371日期：1997年11月21日 102（e）日期1997年11月21日PCT 1996年1月19日PCT PCT。出版物WO96 / 24619 日期1996年8月15日通过在水相中聚合包含至少一种选自乙烯基化合物，丙烯酸或甲基丙烯酸的烷基酯，（甲基）丙烯酸羟烷基酯和乙酸乙烯酯的烯属单官能化合物，和至少一种选自二丙烯酸酯，三丙烯酸酯和/或多官能醇的（甲基）丙烯酸酯）的乙烯二官能或多官能化合物在多元羧酸，聚羟基羧酸，羟基多羧酸和/或多羟基羧酸的缩聚产物存在下，或多羟基多元羧酸与多羟基化合物的用途，以及其用于含水或含溶剂的涂料组合物，特别是用于含水或溶剂的底漆，在汽车工业中的底漆或透明涂层体系。

4. 发明授权

US5460889A Epoxide resin-modified polyester coat with alkyd topcoat 失效
标题翻译：环氧树脂改性聚酯涂层与醇酸面漆
公开(公告)号：US5460889A
公开(公告)日：1995-10-24
申请号：US370908
申请日：1995-01-10
申请人： Lutz-Werner Gross , Ulrich Poth , Dieter Hille , Klaus Weidemeier
发明人： Lutz-Werner Gross , Ulrich Poth , Dieter Hille , Klaus Weidemeier
IPC分类号： C09D163/00 , C09D167/00 , B32B15/08 , B32B27/36 , B32B27/38
CPC分类号： C09D167/00 , C09D163/00 , Y10T428/31522 , Y10T428/31529
摘要： A coating composition comprises an alkyd resin based topcoat and a water dilutable coating comprising an epoxy resin-modified polyester binder which is water-dilutable upon base neutralization of the free carboxyl groups and is prepared by the reaction of (A) a polyester containing (cyclo)aliphatic groups having at least six carbon atoms derived from (a.sub.1) a polycarboxylic acid with at least three carboxyl groups and/or (a.sub.2) a polyol with at least one carboxyl group, (a.sub.3) a polycarboxylic acid with two carboxyl groups and (a.sub.4) a polyol; and (B) a bisphenol epoxide resin.
摘要翻译：涂料组合物包含基于醇酸树脂的面漆和水可稀释涂层，其包含环氧树脂改性的聚酯粘合剂，其在游离羧基的碱中和时可水稀释，并且通过（A）含（（）具有至少6个碳原子的具有至少三个羧基的多羧酸和/或（a2）具有至少一个羧基的多元醇的（a1）多羧酸的脂族基团，（a3）具有两个羧基的多元羧酸和（ a4）多元醇; 和（B）双酚环氧树脂。

5. 发明授权

US5412023A Aqueous dispersions of cross-linked polymer microparticles 失效
标题翻译：交联聚合物微粒的水分散体
公开(公告)号：US5412023A
公开(公告)日：1995-05-02
申请号：US910080
申请日：1992-07-10
申请人： Hans-Dieter Hille , Matthias Massone
发明人： Hans-Dieter Hille , Matthias Massone
IPC分类号： C09D161/20 , C08J3/02 , C09D5/02 , C09D167/00 , C09D167/08 , C09D175/04 , C09D201/06 , C08L51/00 , C08L61/00
CPC分类号： C09D201/06 , C09D167/00 , C09D175/04
摘要： The invention relates to aqueous dispersions of cross-linked polymer microparticles, prepared in an aqueous medium from a polymer, optionally dissolved in an organic solvent, said polymer bearing at least two hydroxyl groups and comprising a number of ionic groups sufficient for the formation of a stable aqueous dispersion, as the component (A) and one further component (B) at an elevated temperature, characterized in that component (A) is a polyesterpolyol, a polyurethane or a polyacrylate having an acid value of from 5 to 168, and that component (B) is an aminoplast resin consisting of molecules containing at least two reactive groups consisting of hydroxyl and/or amino and/or ether groups, that the ratio by weight of component (A) to component (B) is between 30:70 and 95:5, and that the dispersion is stable and usable in water and/or an organic solvent or mixtures thereof. The invention further relates to a process for producing these dispersions, the use thereof and coating compositions containing said dispersions.
摘要翻译： PCT No.PCT / EP90 / 02096 Sec。 371日期：1992年7月10日 102（e）日期1992年7月10日PCT 1990年12月4日PCT PCT。出版物WO91 / 08269 日本1991年6月13日。本发明涉及交联聚合物微粒的水性分散体，其在水性介质中由聚合物制备，任选地溶解在有机溶剂中，所述聚合物带有至少两个羟基并且包含多个离子在高温下作为组分（A）和一种另外的组分（B）形成稳定的水分散体的组合物，其特征在于组分（A）是聚酯多元醇，聚氨酯或聚丙烯酸酯，其酸值为（B）是由包含至少两个由羟基和/或氨基和/或醚基组成的反应性基团的分子组成的氨基塑料树脂，组分（A）与组分（A）的重量比 B）在30:70和95:5之间，并且分散体是稳定的并且可用于水和/或有机溶剂或其混合物。本发明还涉及制备这些分散体的方法，其用途和含有所述分散体的涂料组合物。

6. 发明授权

US5210154A Water-thinnable baking paints and use thereof as filler material and intermediate stone chip resistant coat, as well as process for painting motor vehicle bodies 失效
标题翻译：作为填充材料和中间石材防止涂层的水可烘烤涂料及其用途，以及用于制作电动车辆车身的方法
公开(公告)号：US5210154A
公开(公告)日：1993-05-11
申请号：US613473
申请日：1990-12-10
申请人： Klaus Weidemeier , Winfried Schmidt , Hans-Dieter Hille , Bodo Muller
发明人： Klaus Weidemeier , Winfried Schmidt , Hans-Dieter Hille , Bodo Muller
IPC分类号： B05D7/14 , B05D7/24 , C08G18/08 , C08G59/14 , C09D161/20 , C09D163/00 , C09D167/00 , C09D167/02 , C09D167/08 , C09D175/00 , C09D175/04
CPC分类号： C09D175/04 , C08G18/0819 , C09D167/00
摘要： The invention relates to water-thinnable baking paints, the use thereof as filler material and intermediate stone chip resistant coat as well as a process for painting motor vehicle bodies.The water-thinnable baking paints comprise as binders a combination of(I) 20 to 70% by weight of a water-thinnable polyurethane resin with an acid value of 15 to 35,(II) 20 to 70% by weight of an epoxy resin-modified water-thinnable polyester which can be prepared by reacting a polyester (A) with a molecular weight (number average) below 2000, an acid value of 35-240 and a hydroxyl value of 56-320, with 0.3 to 1.5 equivalents per polyester molecule of an epoxy resin (B) having an epoxide equivalent weight of 170 to 1000, based on a bisphenol, and/or with a derivative of this epoxy resin (C) containing at least one epoxide group per molecule under reaction conditions where essentially only carboxyl groups react with epoxide groups, and(III) 0 to 20% by weight of a water-thinnable aminoplast resin, the sum of the components (I) to (III) being always 100% by weight.
摘要翻译： PCT No.PCT / EP89 / 00412 Sec。 371 1990年12月10日第 102（e）1990年12月10日日期PCT 1989年4月18日PCT PCT。出版物WO89 / 10387 日本特开1989年11月2日。本发明涉及可稀释水的烘烤油漆，其作为填料和中间石材防滑涂料的用途以及用于喷涂机动车体的方法。可水稀释的烘烤漆包含（I）20至70重量％的酸值为15至35的水稀释性聚氨酯树脂，（II）20至70重量％的环氧树脂可以通过使分子量（数均）低于2000的聚酯（A），35-240的酸值和56-320的羟值与每次0.3-1.5当量的聚酯（A）反应制备的水可稀释的聚酯基于双酚的环氧树脂（B）的环氧树脂（B）的聚酯分子，和/或该环氧树脂（C）的衍生物在每个分子中含有至少一个环氧基团的反应条件下基本上是只有羧基与环氧基团反应，和（III）0-20％（重量）的可水稀释的氨基塑料树脂，组分（I）至（III）的总和总是为100重量％。

7. 发明授权

US5183835A Epoxide resin-modified polyesters derived from carboxyl polyol 失效
标题翻译：衍生自羧基多元醇的环氧树脂改性聚酯
公开(公告)号：US5183835A
公开(公告)日：1993-02-02
申请号：US617459
申请日：1990-11-21
申请人： Lutz-Werner Gross , Ulrich Poth , Dieter Hille , Klaus Weidemeier
发明人： Lutz-Werner Gross , Ulrich Poth , Dieter Hille , Klaus Weidemeier
IPC分类号： C09D163/00 , C09D167/00
CPC分类号： C09D167/00 , C09D163/00
摘要： A water-dilutable coating comprising a binder obtained from an epoxide resin-modified polyester possessing free carboxyl groups prepared from the reaction of:A) a polyester polymerized from:a.sub.1) a polycarboxylic acid containing at least three carboxyl groups and/ora.sub.2) a polyol containing at least one carboxyl group anda.sub.3) a polycarboxylic acid containing two carboxyl groups anda.sub.4) a polyol; wherein the polyester contains (cyclo)aliphatic elements having at least six carbon atoms; andB) from 0.3-1.5 equivalents per polyester molecule of a bisphenol epoxide resin or a reaction product thereof containing at least one epoxide group per molecule with a carboxylic acid.
摘要翻译：一种水可稀释涂层，其包含由具有由以下反应制备的具有游离羧基的环氧树脂改性聚酯获得的粘合剂：A）聚合的聚酯：a1）含有至少三个羧基的多元羧酸和/或a2）含有至少一个羧基的多元醇和a3）含有两个羧基的多元羧酸和a4）多元醇; 其中所述聚酯含有具有至少6个碳原子的（环）脂族元素; 和B）每个聚酯分子的双酚环氧树脂0.3-1.5当量或每分子含有至少一个环氧基的反应产物与羧酸。

8. 发明授权

US5169922A Coating compositions and process for the preparation of a multicoat protective and/or decorative coating on a substrate surface 失效
标题翻译：涂层组合物和在基材表面上制备多层保护和/或装饰涂层的方法
公开(公告)号：US5169922A
公开(公告)日：1992-12-08
申请号：US445610
申请日：1990-04-04
申请人： Hans-Dieter Hille , Arnold Dobbelstein , Horst Grosch
发明人： Hans-Dieter Hille , Arnold Dobbelstein , Horst Grosch
IPC分类号： C08F299/00 , B05D7/00 , C08F290/00 , C08G18/10 , C08G18/32 , C08G18/38 , C08G18/65 , C08G18/67 , C09D175/00 , C09D175/04 , C09D175/14
CPC分类号： B05D7/532 , C08G18/10 , C08G18/3225 , C08G18/3271 , C08G18/3821
摘要： The invention relates to coating compositions which are particularly suitable for the preparation of the basecoat for two-coat coatings of the basecoat/clearcoat type, and which comprise organic diluents, at least one resin containing urethane and urea groups, and, where appropriate, other resins, pigments and other conventional additives in common use. The coating compositions according to the invention are those which comprise at least one resin containing urethane and urea groups, which resin is obtainable by reactinga1) a compound having two hydroxyl groups reactive toward isocyanate groups, witha2) an aliphatic and/or cycloaliphatic di-isocyanateto form a prepolymer (A) containing isocyanate groups, and by subsequently reacting the isocyanate groups of the prepolymer (A), at least in part, witha3) an adduct produced from a (meth)acrylic ester, preferably an acrylic ester, and an aliphatic or cycloaliphatic compound containing at least two aminic hydrogen atoms, the adduct containing at least one active aminic hydrogen atom.
摘要翻译： PCT No.PCT / EP88 / 00650 Sec。 371日期1990年04月4日 102（e）日期1990年4月4日PCT提交1988年7月19日PCT公布。出版物WO89 / 01004 日本1989年2月9日。本发明涉及特别适用于制备底漆/透明涂层型双涂层底漆的涂料组合物，其包含有机稀释剂，至少一种含氨基甲酸酯和尿素基团的树脂，以及在适当的情况下常用的其它树脂，颜料和其它常规添加剂。根据本发明的涂料组合物是包含至少一种含有氨基甲酸酯和脲基团的树脂的树脂，该树脂可通过使a1）具有对异氰酸酯基团具有反应性的两个羟基的化合物与a2）脂族和/或脂环族二以形成含有异氰酸酯基团的预聚物（A），然后使预聚物（A）的异氰酸酯基团至少部分地与a3）由（甲基）丙烯酸酯，优选丙烯酸酯和含有至少两个氨基氢原子的脂族或脂环族化合物，所述加合物含有至少一个活性胺氢原子。

9. 发明授权

US5512322A Process for the production of multicoat protective and/or decorative coatings on substrate surfaces 失效
标题翻译：在基材表面上生产多层保护和/或装饰涂层的方法
公开(公告)号：US5512322A
公开(公告)日：1996-04-30
申请号：US334476
申请日：1994-11-04
申请人： Hans-Dieter Hille , Stefan C. Wieditz , Arnold Dobbelstein , Horst Muller
发明人： Hans-Dieter Hille , Stefan C. Wieditz , Arnold Dobbelstein , Horst Muller
IPC分类号： B05D7/16 , C08G18/08 , C08G18/12 , C08G18/40 , C08G18/66 , C09D175/04 , B05D1/36 , C08G18/34 , C08G18/42
CPC分类号： B05D7/532 , C08G18/0819 , C08G18/12 , C08G18/4018 , C08G18/6625 , C09D175/04
摘要： The invention relates to a basecoat/clearcoat process in which the basecoat composition used contains as a film former a polyurethane resin which can be prepared by preparing an intermediate from(A) a mixture obtained from 10 to 90 mol % of linear polyether diols and 90 to 10 mol % of polyester diols,(B) diisocyanates,(C) compounds which contain two groups reactive toward isocyanate groups, at least some of these compounds having at least one group capable of forming anions,and the free isocyanate groups of the said intermediate are then reacted with(D) polyols containing at least three hydroxyl groups, and the reaction product obtained in this manner is transferred into an aqueous base, whereina) the polyester diol is prepared from diols and an acid component which consists of 60 to 100% by weight of aliphatic dicarboxylic acids of more than 18 carbon atoms and of 40 to 0% by weight of aliphatic dicarboxylic acids of 2 to 18 carbon atoms,b) the equivalent ratio of the NCO groups to the total of the OH groups of (A) and the reactive groups of (C) is 2:1 to 1.05:1 andc) the equivalent of the OH groups of the component (D) to the NCO groups of the intermediate is 0.5:1 to 4:1.
摘要翻译：本发明涉及一种底漆/透明涂料方法，其中所用的底漆组合物包含作为成膜剂的聚氨酯树脂，其可以通过从（A）得到的线性聚醚二醇和10至90摩尔的直链聚醚二醇的混合物制备中间体至10mol％的聚酯二醇，（B）二异氰酸酯，（C）含有两个对异氰酸酯基反应的基团的化合物，至少一些具有至少一个能够形成阴离子基团的化合物，以及所述然后使中间体与（D）含有至少三个羟基的多元醇反应，将以这种方式获得的反应产物转移到碱的水溶液中，其中a）聚酯二醇由二醇和酸组分制备，其由60至碳原子数为18以上的脂肪族二羧酸100重量％，碳原子数2〜18的脂肪族二羧酸40〜0重量％，b）NCO基的当量比（A）的OH基团和（C）的反应性基团的总数为2:1至1.05:1，和c）组分（D）的OH基相当于中间体的NCO基团的当量为0.5：1至4：1。

10. 发明授权

US07531614B2 Functionalized polyurethane 有权
标题翻译：官能化聚氨酯
公开(公告)号：US07531614B2
公开(公告)日：2009-05-12
申请号：US10509218
申请日：2003-03-25
申请人： Hans-Dieter Hille , Karsten Jahny , Paul Lamers
发明人： Hans-Dieter Hille , Karsten Jahny , Paul Lamers
IPC分类号： C08G18/30 , C08G18/40 , C08G18/34 , C08G18/77 , C08G18/10
CPC分类号： C08G18/10 , C08G18/0823 , C08G18/4211 , C09D175/04 , C08G18/3275 , C08L2666/16
摘要： Water-thinnable polyurethane with at least two free OH groups obtainable from a first conversion of a primary and/or secondary alkanolamine with a NCO compound giving an intermediate product, followed by the addition of a cyclic carboxylic anhydride to the intermediate product; with the NCO compound exhibiting at least one free NCO group and no blocked NCO group; all alkanolamine being converted during the first conversion to the intermediate product such that the nitrogen atom of the alkanolamine reacts with one of the free NCO groups of the prepolymer to form a urea bond; and the cyclic carboxylic anhydride reacting, with ring opening, with the OH group, originating from the alkanolamine, of the intermediate product; and its use for the production of hot curing coating compositions.
摘要翻译：具有至少两个游离OH基团的可水稀释的聚氨酯可从主链烷醇胺和/或仲链烷醇胺与NCO化合物的第一次转化获得，得到中间产物，然后向中间产物中加入环状羧酸酐; NCO化合物表现出至少一个游离NCO基团并且没有封闭的NCO基团; 所有链烷醇胺在第一次转化期间转化为中间产物，使得链烷醇胺的氮原子与预聚物的游离NCO基团之一反应形成脲键; 环状羧酸酐与中间产物的起始于链烷醇胺的OH基反应开环; 以及其用于生产热固化涂料组合物的用途。

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