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1. 发明授权

US6063284A Single column closed-loop recycling with periodic intra-profile injection 失效
标题翻译：单柱闭环回收利用周期性轮廓内注射
公开(公告)号：US6063284A
公开(公告)日：2000-05-16
申请号：US857039
申请日：1997-05-15
申请人： Charles M. Grill
发明人： Charles M. Grill
IPC分类号： B01D15/08 , B01D15/18 , G01N30/44
CPC分类号： B01D15/1814 , B01D15/1857 , G01N30/44
摘要： A preparative chromatographic cyclical process utilizing a single column comprising, at steady state: (a) establishing and maintaining a circulating chromatographic profile through said column and through one solvent pump; (b) discontinuously and periodically injecting a sample comprising at least two components, into the interior of said maintained circulating profile; and (c) collecting, discontinuously and periodically, at least two enriched fractions from said circulating profile.
摘要翻译：使用单柱的制备型色谱循环方法，其包括在稳定状态：（a）通过所述柱和通过一种溶剂泵建立和维持循环色谱图; （b）不连续地和周期地将包含至少两个组分的样品注入所述维持的循环轮廓的内部; 和（c）从所述循环曲线收集，不连续和周期性地至少两个富集部分。

2. 发明授权

US5630943A Discontinuous countercurrent chromatographic process and apparatus 失效
标题翻译：不连续的逆流色谱法和仪器
公开(公告)号：US5630943A
公开(公告)日：1997-05-20
申请号：US566425
申请日：1995-11-30
申请人： Charles M. Grill
发明人： Charles M. Grill
IPC分类号： G01N30/46 , B01D15/08 , B01D15/18 , G01N30/44
CPC分类号： B01D15/1814 , B01D15/1864 , G01N30/44 , B01D15/1857
摘要： A preparative chromatographic cyclical process comprising, at steady state: establishing a figure-of-eight circulating chromatographic profile between two chromatographic columns with the provision that said chromatographic profile never passes through a pump; discontinuously and periodically injecting a sample comprising at least two components, into said circulating profile; and collecting, discontinuously and periodically, at least two enriched fractions from said circulating profile, the apparatus for conducting this process comprising only two chromatographic columns, at least one solvent pump, an injection pump, two 4-way valves, and conduit communicating said columns and the two 4-way valves in the form of a figure-of-eight pattern without traversing a pump, and conduit communicating said at least one solvent pump and at least one of said columns.
摘要翻译：一种制备型色谱循环方法，其包括在稳定状态：在两个色谱柱之间建立八位循环色谱图，其规定所述色谱图从未通过泵; 不连续地和周期性地将包含至少两个组分的样品注入所述循环轮廓; 以及从所述循环曲线收集，不连续和周期性地至少两个富集部分，用于进行该方法的装置仅包括两个色谱柱，至少一个溶剂泵，注射泵，两个四通阀和将所述柱和两个八通阀形式的图形，而不穿过泵，以及连通所述至少一个溶剂泵和至少一个所述柱的导管。

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