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1. 发明授权

US5230708A Methods and compositions to enhance stain resistance of nylon carpet fibers: thlocyanate to reduce yellowing 失效
标题翻译：增强尼龙地毯纤维耐污染性的方法和组合物：硫氰酸盐以减少黄变
公开(公告)号：US5230708A
公开(公告)日：1993-07-27
申请号：US361671
申请日：1989-06-01
申请人： Dale A. Hangey , Paul W. Harris , Daniel J. Corcoran, Jr. , Michael P. Friedberger , Charles J. Cole , William A. Archie , Roger N. Spitz
发明人： Dale A. Hangey , Paul W. Harris , Daniel J. Corcoran, Jr. , Michael P. Friedberger , Charles J. Cole , William A. Archie , Roger N. Spitz
IPC分类号： D06M15/277 , D06M15/41
CPC分类号： D06M15/412 , D06M15/277 , D06M2101/12 , D06M2101/34 , Y10S8/924 , Y10S8/929 , Y10T428/23979 , Y10T428/23986 , Y10T428/23993 , Y10T428/2969
摘要： This invention relates to improved methods and compositions to enhance stain resistance of carpet fiber. The improved methods relate to a continuous aftertreatment for dyed carpet fabric and to two-step processes, either batch-batch, batch-continuous or continuous-continuous. The improved compositions are used in the processes to enhance stain resistance of carpet or carpet fiber and to overcome various prior drawbacks, such as, yellowing, oxidation and durability to cleaning. The sulfonated aromatic condensates are used to enhance stain resistance, and can be combined with fluorocarbon compounds for soil resistance, thiocyanates, and/or salts having divalent cations, such as magnesium sulfate. Also various dispersing agents, buffering acids and sequestering agents are disclosed.
摘要翻译：本发明涉及改善地毯纤维耐污染性的方法和组合物。改进的方法涉及染色地毯织物的连续后处理和批次间歇，间歇连续或连续连续的两步法。改进的组合物用于增强地毯或地毯纤维的抗污性和克服各种先前缺点的方法，例如变黄，氧化和对清洁的耐久性。磺化芳族缩合物用于增强耐污染性，并且可以与用于土壤抗性的碳氟化合物，硫氰酸盐和/或具有二价阳离子的盐如硫酸镁组合。还公开了各种分散剂，缓冲酸和螯合剂。

2. 发明授权

US4695497A Method of imparting stain resistance to colored substrates which include a filamentary material 失效
标题翻译：赋予包括丝状材料的有色基材耐污性的方法
公开(公告)号：US4695497A
公开(公告)日：1987-09-22
申请号：US263
申请日：1987-01-02
申请人： Monte L. Nagy, Jr. , Charles J. Cole
发明人： Monte L. Nagy, Jr. , Charles J. Cole
IPC分类号： D06M13/428 , D06M15/295 , B32B3/02 , B32B33/00
CPC分类号： D06M15/295 , D06M13/428 , Y10T428/23986 , Y10T428/23993 , Y10T428/2969 , Y10T428/3154 , Y10T428/31544 , Y10T442/2279
摘要： A method of imparting stain resistance to colored substrates which include a filamentary material is disclosed. A first dispersion of a polymer is applied to the filamentary material as a finish during the manufacture of the filamentary material, and a second dispersion of a polymer is applied as an overspray after the filamentary material has been formed into a colored substrate, to achieve at least 300 ppm fluorine from each application on the filamentary material (at least 600 ppm fluorine total). The dispersions are independently selected from the group consisting ofi. a first polymer comprising(a) from about 50 to about 85 parts by weight of units derived from a fluorinated monomer or mixture of fluorinated monomers having the formula ##STR1## (b) from about 15 to about 50 parts by weight of units derived from one or more monomers having the formula ##STR2## ii. a dispersion comprising (a) from about 10 to about 50 parts by weight the first polymer;(b) from about 5 to about 10 parts by weight an emulsifier; and(c) from about 40 to 85 parts by weight a second polymer derived from a monomer having the formula ##STR3## wherein R.sub.f is straight or branched-chain perfluoroalkyl containing 4-20 carbon atoms;R is H or CH.sub.3 ;n is an integer from 1-15; andX is Cl or Br.
摘要翻译：公开了对包括丝状材料的着色基底赋予耐污染性的方法。聚合物的第一分散体在丝状材料的制造过程中作为整理剂施加到丝状材料上，并且在丝状材料已经形成为着色的基底之后，将聚合物的第二分散体作为过度喷涂施加，以达到在丝状材料上的每种应用中至少含有300ppm的氟（总共至少600ppm的氟）。分散体独立地选自i。包含（a）约50至约85重量份衍生自氟化单体的单元或具有式（b）的氟化单体的混合物，约15至约50重量份衍生自一种或多种具有下式的单体：分散体，其包含（a）约10至约50重量份的第一聚合物; （b）约5至约10重量份的乳化剂; 和（c）约40至85重量份的衍生自具有式“IMAGE”的单体的第二聚合物，其中Rf为含4-20个碳原子的直链或支链全氟烷基; R为H或CH 3; n为1-15的整数; X为Cl或Br。

3. 发明授权

US07170401B1 System to detect the presence of an unattended child in a vehicle 失效
标题翻译：用于检测车辆中无人值班儿童的存在的系统
公开(公告)号：US07170401B1
公开(公告)日：2007-01-30
申请号：US10889144
申请日：2004-07-13
申请人： Charles J. Cole
发明人： Charles J. Cole
IPC分类号： B60Q1/00
CPC分类号： G08B21/22 , B60N2/002 , B60N2/26 , B60R25/10
摘要： A system detects the presence of an unattended child within a vehicle and when the child is so detected, disables the vehicle's door locks by preventing doors from being locked or remaining locked and sounds an alarm. The presence of a child is detected by measuring pressure on the back seat and measurements above a threshold limit signify a child is present or if any of the rear seat belts are buckled a child is detected. The system can be shut off by the driver, although the system has an override in the shutoff mode so that if the temperature rises above or falls below a certain level and the presence of a child is detected, the alarm is sounded. In this mode, the presence of the child can also be detected by a motion sensor.
摘要翻译：系统检测车内无人照看的儿童的存在，并且当孩子被检测到时，通过防止门被锁定或保持锁定并发出警报来禁用车门的门锁。通过测量后座上的压力来检测儿童的存在，并且超过阈值限度的测量值表示存在儿童，或者如果检测到任何后座安全带被扣住，则检测到儿童。系统可以由驾驶员关闭，虽然系统在关闭模式下有超驰，因此如果温度升高到或低于一定水平，并且检测到孩子的存在，则会发出警报。在该模式中，也可以通过运动传感器来检测儿童的存在。

4. 发明授权

US4591473A Method of spinning a nylon yarn having improved retention of a soil repellent finish on the nylon yarn 失效
标题翻译：纺丝尼龙纱线的方法，该尼龙纱线具有改进尼龙纱线上防污性能的保持性
公开(公告)号：US4591473A
公开(公告)日：1986-05-27
申请号：US591244
申请日：1984-03-20
申请人： Robert A. Lofquist , Gene C. Weedon , Charles J. Cole
发明人： Robert A. Lofquist , Gene C. Weedon , Charles J. Cole
IPC分类号： C08G69/04 , D06M15/507 , B29C59/00 , C08J9/36 , D01F6/90
CPC分类号： C08G69/04 , D06M15/507
摘要： This invention is a method to improve retention of a finish on nylon yarn, said finish containing the reaction product of epichlorohydrin with the reaction product of pyromellitic dianhydride with a long chain fluoroalcohol, comprising polymerizing said nylon in the presence of about 0.5 to 1 mole percent of a primary-tertiary diamine of the structure ##STR1## where R.sub.1 is an alpha, omega-alkylene group of 2 to 10 carbon atoms where cycloaliphatic, R.sub.2 and R.sub.3 are alkyl radicals of 1 to 4 carbon atoms, R.sub.4 is an alkylene radical of 1 to 10 carbon atoms and R.sub.5 is R.sub.4 or arylalkyl, R.sub.6 is H or alkyl of 1 to 4 carbons, so that said nylon polymer is melt stable. Also, for batch processing, polyethyleneimines of 300 to 1200 molecular weight, methylaminobispropylamine, N-(2-aminoethyl)-1,3-propanediamine, and 3,3'-iminobispropylamine are useful.
摘要翻译：本发明是一种改善尼龙纱线上饰面保留性的方法，所述表面处理剂含有表氯醇与1,2,4,5-苯四酸二酐与长链氟代醇的反应产物的反应产物，包括在约0.5-1摩尔％其中R 1是2至10个碳原子的α，ω-亚烷基，其中脂环族基，R 2和R 3是具有1至4个碳原子的烷基，R 4是 1至10个碳原子的亚烷基，R 5是R 4或芳基烷基，R 6是H或1至4个碳的烷基，使得所述尼龙聚合物是熔体稳定的。此外，对于分批处理，分子量为300〜1200的聚乙烯亚胺，甲基氨基丙基胺，N-（2-氨基乙基）-1,3-丙二胺和3,3'-亚氨基双丙基胺是有用的。

5. 发明授权

US5145487A Methods and compositions to enhance stain resistance of carpet fibers using sulfonated aromatic condensates 失效
标题翻译：使用磺化芳族缩合物增强地毯纤维耐污染性的方法和组合物
公开(公告)号：US5145487A
公开(公告)日：1992-09-08
申请号：US818475
申请日：1992-01-06
申请人： Dale A. Hangey , Paul W. Harris , Charles J. Cole , Daniel J. Corcoran, Jr.
发明人： Dale A. Hangey , Paul W. Harris , Charles J. Cole , Daniel J. Corcoran, Jr.
IPC分类号： D06M15/277 , D06M15/41
CPC分类号： D06M15/412 , D06M15/277 , D06M2101/12 , D06M2101/34 , Y10S8/924 , Y10S8/929
摘要： This invention relates to improved methods and compositions to enhance stain resistance of carpet fiber. The improved methods relate to a continuous aftertreatment for dyed carpet fabric and to two-step processes, either batch-batch, batch-continuous or continuous-continuous. The improved compositions are used in the processes to enhance stain resistance of carpet or carpet fiber and to overcome various prior drawbacks, such as, yellowing, oxidation and durability to cleaning. The sulfonated aromatic condensates are used to enhance stain resistance, and can be combined with fluorocarbon compounds for soil resistance, thiocyanates, and/or salts having divalent cations, such as magnesium sulfate. Also various dispersing agents, buffering acids and sequestering agents are disclosed.
摘要翻译：本发明涉及改善地毯纤维耐污染性的方法和组合物。改进的方法涉及染色地毯织物的连续后处理和批次间歇，间歇连续或连续连续的两步法。改进的组合物用于增强地毯或地毯纤维的抗污性和克服各种先前缺点的方法，例如变黄，氧化和对清洁的耐久性。磺化芳族缩合物用于增强耐污染性，并且可以与用于土壤抗性的碳氟化合物，硫氰酸盐和/或具有二价阳离子的盐如硫酸镁组合。还公开了各种分散剂，缓冲酸和螯合剂。

6. 发明授权

US4310659A Two-stage hydrolysis process for the preparation of nylon 6 失效
标题翻译：二阶段水解法制备尼龙6
公开(公告)号：US4310659A
公开(公告)日：1982-01-12
申请号：US141827
申请日：1980-04-21
申请人： Samuel L. Yates , Charles J. Cole , Albert H. Wiesner , John W. Wagner
发明人： Samuel L. Yates , Charles J. Cole , Albert H. Wiesner , John W. Wagner
IPC分类号： C08G69/00 , C08G69/16
CPC分类号： C08G69/16
摘要： A two-stage hydrolysis process for polymerizing epsilon-caprolactam is disclosed comprising a first stage from a temperature of about 180.degree. C.-260.degree. C., a pressure of 20 to 150 psig, for a period of about 0.5 to 4 hours, then before equilibrium conditions are reached a second stage at a temperature of about 200.degree. C.-260.degree. C., a pressure of about 100-900 Torr for a period of about 2 to 15 hours, while continuously removing most of the water so that water is removed both during hydrolyzation and during the subsequent polycondensation, whereby the cyclic dimer content of the shaped polymer article is below 0.2 percent by weight.
摘要翻译：公开了用于聚合ε-己内酰胺的两阶段水解方法，其包括在约180℃-260℃的温度，20至150psig的压力下进行约0.5至4小时的第一阶段，然后在平衡条件达到约200℃-260℃的温度的第二阶段，约100-900乇的压力下进行约2至15小时的时间，同时连续地除去大部分水在水解过程中和在随后的缩聚过程中除去水，由此成型聚合物制品的环状二聚体含量低于0.2重量％。

7. 外观设计

USD252837S Shoe bottom 失效
公开(公告)号：USD252837S
公开(公告)日：1979-09-11
申请号：US821901
申请日：1977-08-04
申请人： Charles J. Cole
设计人： Charles J. Cole

8. 发明授权

US5190565A Sulfonated 2-(2'-hydroxyaryl)-2H-benzotriazoles and/or sulfonated aromatic formaldehyde condensates and their use to improve stain resistance and dye lightfasteness 失效
标题翻译：磺化的2-（2'-羟基芳基）-2H-苯并三唑和/或磺化的芳族甲醛缩合物及其用于改善耐污染性和染料耐光性
公开(公告)号：US5190565A
公开(公告)日：1993-03-02
申请号：US650400
申请日：1991-02-01
申请人： Morris B. Berenbaum , John H. Bonfield , Charles J. Cole , Paul W. Harris , Thomas P. J. Izod , Harry E. Ulmer , Frederick R. Hopf , James T. Yardley , Karen M. Bland
发明人： Morris B. Berenbaum , John H. Bonfield , Charles J. Cole , Paul W. Harris , Thomas P. J. Izod , Harry E. Ulmer , Frederick R. Hopf , James T. Yardley , Karen M. Bland
IPC分类号： C07D249/20 , D06M13/256 , D06M13/352 , D06M13/355 , D06M15/41 , D06P1/56 , D06P1/642
CPC分类号： C07D249/20 , D06M13/256 , D06M13/352 , D06M13/355 , D06M15/412 , D06P1/56 , D06P1/6426 , D06M2101/34 , Y10S8/924
摘要： A new class of sulfonated 2-(2'-hydroxyaryl)-2H-benzotriazole compounds and method for using them and other sulfonated hydroxyaryl benzotriazoles on nylon fibers to improve stain resistance and dye lightfastness has been discovered. A process is provided for improving stain resistance of nylon fibers by treatment with sulfonated aromatic-formaldehyde condensate and fluorinated dry soil resist agents.
摘要翻译：已经发现了一类新的磺化2-（2'-羟基芳基）-2H-苯并三唑化合物及其在尼龙纤维上的使用及其它磺化羟基芳基苯并三唑的方法，以提高耐污染性和耐染色性。提供了一种通过用磺化芳族 - 甲醛缩合物和氟化干土抗蚀剂处理来改善尼龙纤维的耐污性的方法。

9. 发明授权

US5152803A Methods and compositions to enhance stain resistance of carpet fibers with water-soluble thiocyanate 失效
标题翻译：用水溶性硫氰酸盐提高地毯纤维耐污染性的方法和组合物
公开(公告)号：US5152803A
公开(公告)日：1992-10-06
申请号：US671624
申请日：1991-03-19
申请人： Dale A. Hangey , Paul W. Harris , Daniel J. Corcoran, Jr. , Michael P. Friedberger , Charles J. Cole , William A. Archie , Roger N. Spitz
发明人： Dale A. Hangey , Paul W. Harris , Daniel J. Corcoran, Jr. , Michael P. Friedberger , Charles J. Cole , William A. Archie , Roger N. Spitz
IPC分类号： D06M15/277 , D06M15/41
CPC分类号： D06M15/412 , D06M15/277 , D06M2101/12 , D06M2101/34 , Y10S8/924 , Y10S8/929
摘要： This invention relates to improved methods and compositions to enhance stain resistance of carpet fiber. The improved methods relate to a continuous aftertreatment for dyed carpet fabric and to two-step processes, either batch-batch, batch-continuous or continuous-continuous. The improved compositions are used in the processes to enhance stain resistance of carpet or carpet fiber and to overcome various prior drawbacks, such as, yellowing, oxidation and durability to cleaning. The sulfonated aromatic condensates are used to enhance stain resistance, and can be combined with fluorocarbon compounds for soil resistance, thiocyanates, and/or salts having divalent cations, such as magnesium sulfate. Also various dispersing agents, buffering acids and sequestering agents are disclosed.
摘要翻译：本发明涉及改善地毯纤维耐污染性的方法和组合物。改进的方法涉及染色地毯织物的连续后处理和批次间歇，间歇连续或连续连续的两步法。改进的组合物用于增强地毯或地毯纤维的抗污性和克服各种先前缺点的方法，例如变黄，氧化和对清洁的耐久性。磺化芳族缩合物用于增强耐污染性，并且可以与用于土壤抗性的碳氟化合物，硫氰酸盐和/或具有二价阳离子的盐如硫酸镁组合。还公开了各种分散剂，缓冲酸和螯合剂。

10. 发明授权

US4990623A Sulfonated 2-(2'-hydroxyaryl)-2H-benzotriazoles and/or sulfonated aromatic formaldehyde condensates 失效
标题翻译：磺化2-（2'-羟基芳基）-2H-苯并三唑和/或磺化芳族甲醛缩合物
公开(公告)号：US4990623A
公开(公告)日：1991-02-05
申请号：US384234
申请日：1989-07-24
申请人： Morris B. Berenbaum , John H. Bonfield , Charles J. Cole , Paul W. Harris , Thomas P. J. Izod , Harry E. Ulmer , Frederick R. Hopf , James T. Yardley , Karen M. Bland
发明人： Morris B. Berenbaum , John H. Bonfield , Charles J. Cole , Paul W. Harris , Thomas P. J. Izod , Harry E. Ulmer , Frederick R. Hopf , James T. Yardley , Karen M. Bland
IPC分类号： C07D249/20 , D06M13/256 , D06M13/352 , D06M13/355 , D06M15/41 , D06P1/56 , D06P1/642
CPC分类号： C07D249/20 , D06M13/256 , D06M13/352 , D06M13/355 , D06M15/412 , D06P1/56 , D06P1/6426 , D06M2101/34
摘要： A new class of sulfonated 2-(2'-hydroxyaryl)-2H-benzotriazole compounds and method for using them and other sulfonated hydroxyaryl benzotriazoles on nylon fibers to improve stain resistance and dye lightfastness has been discovered. A process is provided for improving stain resistance of nylon fibers by treatment with sulfonated aromatic-formaldehyde condensate and fluorinated dry soil resist agents.
摘要翻译：已经发现了一类新的磺化2-（2'-羟基芳基）-2H-苯并三唑化合物及其在尼龙纤维上的使用及其它磺化羟基芳基苯并三唑的方法，以提高耐污染性和耐染色性。提供了一种通过用磺化芳族 - 甲醛缩合物和氟化干土抗蚀剂处理来改善尼龙纤维的耐污性的方法。

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