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1. 发明授权

US06197844B1 Floor finish compositions 有权
标题翻译：地板成分
公开(公告)号：US06197844B1
公开(公告)日：2001-03-06
申请号：US09242078
申请日：1999-02-04
申请人： Steven J. Hamrock , Fidelis C. Onwumere , Bradford B. Wright , Michael A. Yandrasits
发明人： Steven J. Hamrock , Fidelis C. Onwumere , Bradford B. Wright , Michael A. Yandrasits
IPC分类号： C08F248
CPC分类号： C08G18/672 , C07D251/34 , C08G18/2875 , C08G18/792 , Y10S524/914 , Y10T428/31547
摘要： A monomer useful in the formulation of a radiation curable coatable composition comprises (a) polyfunctional isocyanurate having at least three terminal reactive groups reacted with (b) hydroxyalkyl acrylate and (c) tertiary amine alcohol in a molar ratio of a:b:c of about 1:1-2.5:0.5-2, wherein b+c is at least 3 and no greater than the total number of terminal reactive groups of (a). The monomer is included in a radiation curable coatable composition suitable for use as a floor finish and in a floor finishing system comprising the foregoing coatable composition with a primer. A method for the treatment of a substrate using the floor finish and the floor finishing system is also described.
摘要翻译：可用于制备可辐射固化涂层组合物的单体包含（a）具有至少三个末端反应性基团与（b）丙烯酸羟烷基酯和（c）叔胺醇的摩尔比a:b:c的至少三个末端反应性基团反应的多官能异氰脲酸酯约1：1-2.5：0.5-2，其中b + c为至少3且不大于（a）的末端反应性基团的总数。该单体包括在适合用作地板表面的可辐射固化的可涂覆组合物中，以及包含前述可涂覆组合物与底漆的地板整理系统中。还描述了使用地板漆和地板整理系统处理基板的方法。

2. 发明授权

US5656333A Method of producing nonwoven articles 失效
标题翻译：无纺布制品的制造方法
公开(公告)号：US5656333A
公开(公告)日：1997-08-12
申请号：US653856
申请日：1996-05-28
申请人： Jack G. Truong , Willa M. Studiner , Bradford B. Wright , Michael M. Rock, Jr.
发明人： Jack G. Truong , Willa M. Studiner , Bradford B. Wright , Michael M. Rock, Jr.
IPC分类号： D06M15/356 , D04H1/64 , D06M13/02 , D06M13/503 , D06M15/333 , D06M101/00 , D06M101/02 , D06M101/06 , D06M101/16 , D06M101/18 , D06M101/30 , D06M101/32 , B05D1/02
CPC分类号： D04H1/64 , D04H1/587 , Y10T442/20 , Y10T442/2352 , Y10T442/2369 , Y10T442/2861 , Y10T442/2877 , Y10T442/60 , Y10T442/676
摘要： Nonwoven articles having high durability and absorbent characteristics, and their methods of manufacture, are presented. One preferred article is characterized by(a) a nonwoven web comprised of organic fibers comprised of polymers having a plurality of pendant hydroxyl groups; and(b) a binder comprising an at least partially crosslinked and at least partially hydrolyzed polymeric resin having a plurality of pendant resin hydroxyl groups, the resin crosslinked by a crosslinking agent, the crosslinking agent selected from the group consisting of organic titanates and amorphous metal oxides, the polymeric resin derived from monomers selected from the group consisting of monomers within the general formula ##STR1## wherein: X is selected from the group consisting of Si(OR.sup.4 OR.sup.5 OR.sup.6) and O(CO)R.sup.7 ; andR.sup.1 -R.sup.7 inclusive are independently selected from the group consisting of hydrogen and organic radicals having from 1 to about 10 carbon atoms, inclusive, and combinations thereof.
摘要翻译：提出了具有高耐久性和吸收特性的非织造物品及其制造方法。一个优选的制品的特征在于：（a）由具有多个侧基羟基的聚合物组成的有机纤维组成的非织造网; 和（b）包含至少部分交联和至少部分水解的聚合物树脂的粘合剂，所述树脂具有多个侧链树脂羟基，所述树脂由交联剂交联，所述交联剂选自有机钛酸盐和非晶态金属氧化物，衍生自选自以下通式的单体的单体的聚合物树脂：其中：X选自Si（OR 4 OR 5 OR 6）和O（CO）R 7; 和R 1 -R 7独立地选自氢和具有1至约10个碳原子的有机基团，以及它们的组合。

3. 发明授权

US5380923A Polymeric sulfonium salts and method of preparation thereof 失效
标题翻译：聚合锍盐及其制备方法
公开(公告)号：US5380923A
公开(公告)日：1995-01-10
申请号：US55031
申请日：1993-04-29
申请人： Bradford B. Wright , Omar Farooq , Robert J. DeVoe
发明人： Bradford B. Wright , Omar Farooq , Robert J. DeVoe
IPC分类号： C08G75/02 , C07C323/65 , C07C381/12
CPC分类号： C08G75/02 , Y10S522/904
摘要： Polymeric triarylsulfonium salts are provided having a repeating structural unit with the formula: ##STR1## where R represents a substituted or unsubstituted aryl group, X.sup.- represents a non-nucleophilic anion, n represents an integer greater than or equal to 0 and p represents an integer greater than or equal to 2 and may be prepared by combining (a) an arylbis(p-fluorophenyl)substituted sulfonium salt with a bis(trimethylsilylated)dithiol in a polar aprotic solvent.
摘要翻译：提供聚合三芳基锍盐，其具有下式的重复结构单元：取代的芳基，X-表示非亲核阴离子，n表示大于或等于0的整数，p表示大于或等于2的整数，并且可以通过将（a）芳基双（对氟苯基）取代的锍盐与双（三甲基硅烷基化）二硫醇在极性非质子溶剂中组合来制备。

4. 发明授权

US4880705A Siloxy ketenes and products prepared therefrom 失效
标题翻译：硅氧烯及其制备的产品
公开(公告)号：US4880705A
公开(公告)日：1989-11-14
申请号：US289987
申请日：1988-12-22
申请人： Bradford B. Wright
发明人： Bradford B. Wright
IPC分类号： C07F7/18 , C08C19/25
CPC分类号： C07F7/188 , C07F7/1856 , C08C19/25 , Y10T428/31663
摘要： A method of combining a siloxy group (--SiO--) with a ketene-reactive compound to form a siloxy-containing product comprises:(a) subjecting a silyl diketone to photolysis under conditions effective for generating a siloxy ketene intermediate therefrom, said silyl diketone having the formula ##STR1## wherein Si is silicon, R.sub.1 and R.sub.4 are hydrocarbon groups containing from 1 to 18 carbons, and R.sub.2 and R.sub.3 are hydrocarbon groups containing from 1 to 6 carbons, said photolysis being carried out by irradiating said silyl diketone with light of a wavelength from 200 to 800 nm; and, thereafter,(b) contacting the generated siloxy ketene intermediate with a ketene-reactive compound under conditions effective for reaction therewith, said compound being selected from the group consisting of (i) a diene polymer containing a plurality of unsaturated carbon bonds, (ii) an alkylene or cycloalkylene compound containing at least one unsaturated linkage; and (iii) an aldehyde containing one or more aldehyde groups.
摘要翻译：将甲硅烷氧基（-SiO-）与乙烯酮反应性化合物结合以形成含甲硅烷氧基的产物的方法包括：（a）在有效地从其产生甲硅烷氧基乙烯酮中间体的条件下使甲硅烷基二酮进行光解，所述甲硅烷基二酮具有其中Si是硅的式“IMAGE”，R 1和R 4是含有1至18个碳的烃基，R 2和R 3是含有1至6个碳的烃基，所述光解是通过用光照射所述甲硅烷基二酮波长为200至800nm; （b）使生成的甲硅烷氧基乙烯酮中间体与乙烯酮反应性化合物在有效反应的条件下接触，所述化合物选自：（i）含有多个不饱和碳键的二烯聚合物，（ ii）含有至少一个不饱和键的亚烷基或亚环烷基化合物; 和（iii）含有一个或多个醛基的醛。

5. 发明授权

US4812214A Method of combining siloxy groups with ketene-reactive compounds 失效
标题翻译：将甲硅烷氧基与烯酮反应性化合物组合的方法
公开(公告)号：US4812214A
公开(公告)日：1989-03-14
申请号：US101589
申请日：1987-09-28
申请人： Bradford B. Wright
发明人： Bradford B. Wright
IPC分类号： C07F7/18 , C08C19/25 , B01J19/08
CPC分类号： C07F7/188 , C07F7/1856 , C08C19/25
摘要： A method of combining a siloxy group (--SiO--) with a ketene-reactive compound to form a siloxy-containing product comprises:(a) subjecting a silyl diketone to photolysis under conditions effective for generating a siloxy ketene intermediate therefrom, said silyl diketone having the formula ##STR1## wherein Si is silicon, R.sub.1 and R.sub.4 are hydrocarbon groups containing from 1 to 18 carbons, and R.sub.2 and R.sub.3 are hydrocarbon groups containing from 1 to 6 carbons, said photolysis being carried out by irradiating said silyl diketone with light of a wavelength from 200 to 800 nm; and, thereafter,(b) contacting the generated siloxy ketene intermediate with a ketene-reactive compound under conditions effective for reaction therewith, said compound being selected from the group consisting of (i) a diene polymer containing a plurality of unsaturated carbon bonds, (ii) an alkylene or cycloalkylene compound containing at least one unsaturated linkage; and (iii) an aldehyde containing one or more aldehyde groups.
摘要翻译：将甲硅烷氧基（-SiO-）与乙烯酮反应性化合物结合以形成含甲硅烷氧基的产物的方法包括：（a）在有效地从其产生甲硅烷氧基乙烯酮中间体的条件下使甲硅烷基二酮进行光解，所述甲硅烷基二酮具有其中Si是硅的式“IMAGE”，R 1和R 4是含有1至18个碳的烃基，R 2和R 3是含有1至6个碳的烃基，所述光解是通过用光照射所述甲硅烷基二酮波长为200至800nm; （b）使生成的甲硅烷氧基乙烯酮中间体与乙烯酮反应性化合物在有效反应的条件下接触，所述化合物选自：（i）含有多个不饱和碳键的二烯聚合物，（ ii）含有至少一个不饱和键的亚烷基或亚环烷基化合物; 和（iii）含有一个或多个醛基的醛。

6. 发明授权

US06132860A Abrasive article comprising organometallic coupling agent 失效
标题翻译：包含有机金属偶联剂的磨料制品
公开(公告)号：US06132860A
公开(公告)日：2000-10-17
申请号：US886737
申请日：1997-07-01
申请人： Wesley J. Bruxvoort , Steven J. Keipert , Fred B. McCormick , Jerry W. Williams , Bradford B. Wright
发明人： Wesley J. Bruxvoort , Steven J. Keipert , Fred B. McCormick , Jerry W. Williams , Bradford B. Wright
IPC分类号： B24D3/02 , B24D11/00 , B32B5/16
CPC分类号： B24D3/02 , B24D11/00 , Y10T428/24372 , Y10T428/24413 , Y10T428/25 , Y10T428/252 , Y10T428/257
摘要： An energy sensitive composition comprising a monomeric organometallic complex essentially free of nucleophilic groups and which, upon exposure to energy, bonds to basic reactive sites on a substrate via the metal center, leaving the polymerizable group of the complex unreacted and unrestricted; an energy sensitive composition at least one energy sensitive organometallic group is incorporated in or appended to the backbone of a polymer, such that the resulting coordinatively unsaturated organometallic group or groups bond to basic reactive sites on a substrate, thus forming permanent bonds, and further, the adherent compositions are useful in applications such as adhesion of polymers to substrates, protective coatings, printing plates, durable release coatings, primers, binders, and paints.
摘要翻译：一种能量敏感性组合物，其包含基本上不含亲核基团的单体有机金属络合物，并且在暴露于能量之后，经由金属中心与基底上的碱性反应位点键合，使复合物的可聚合基团未反应和不受限制; 能量敏感组合物至少一个能量敏感的有机金属基团被引入聚合物的主链或连接到聚合物的骨架上，使得所得到的协调不饱和的有机金属基团与基底上的碱性反应位点相连，从而形成永久的键，粘合剂组合物可用于诸如将聚合物粘合到基材，保护涂层，印刷版，耐久脱模涂料，底漆，粘合剂和涂料等应用中。

7. 发明授权

US06217984B1 Organometallic monomers and polymers with improved adhesion 失效
标题翻译：有机金属单体和具有改善粘附性的聚合物
公开(公告)号：US06217984B1
公开(公告)日：2001-04-17
申请号：US07890593
申请日：1992-05-21
申请人： Wesley J. Bruxvoort , Steven J. Keipert , Fred B. McCormick , Jerry W. Williams , Bradford B. Wright
发明人： Wesley J. Bruxvoort , Steven J. Keipert , Fred B. McCormick , Jerry W. Williams , Bradford B. Wright
IPC分类号： B32B500
CPC分类号： G03F7/027 , B24D3/28 , C08G18/3206 , C08G18/3897 , C08G18/73 , C09D175/04 , G03F7/038 , G03F7/0752 , Y10S430/107 , Y10S430/115 , Y10S430/117 , Y10T428/24802 , Y10T428/25 , Y10T428/256 , Y10T428/2839 , Y10T428/31507 , Y10T428/31511 , Y10T428/31663
摘要： An energy sensitive composition comprising a monomeric organometallic complex essentially free of nucleophilic groups and which, upon exposure to energy, bonds to basic reactive sites on a substrate via the metal center, leaving the polymerizable group of the complex unreacted and unrestricted; an energy sensitive composition at least one energy sensitive organometallic group is incorporated in or appended to the backbone of a polymer, such that the resulting coordinatively unsaturated organometallic group or groups bond to basic reactive sites on a substrate, thus forming permanent bonds, and further, the adherent compositions are useful in applications such as adhesion of polymers to substrates, protective coatings, printing plates, durable release coatings, primers, binders, and paints.
摘要翻译：一种能量敏感性组合物，其包含基本上不含亲核基团的单体有机金属络合物，并且在暴露于能量之后，经由金属中心与基底上的碱性反应位点键合，使复合物的可聚合基团未反应和不受限制; 能量敏感组合物至少一个能量敏感的有机金属基团被引入聚合物的主链或连接到聚合物的骨架上，使得所得到的协调不饱和的有机金属基团与基底上的碱性反应位点相连，从而形成永久的键，粘合剂组合物可用于诸如将聚合物粘合到基材，保护涂层，印刷版，耐久脱模涂料，底漆，粘合剂和涂料等应用中。

8. 发明授权

US6013587A Nonwoven articles 失效
标题翻译：无纺布制品
公开(公告)号：US6013587A
公开(公告)日：2000-01-11
申请号：US655048
申请日：1996-05-29
申请人： Jack G. Truong , Willa M. Studiner , Bradford B. Wright , Michael M. Rock, Jr.
发明人： Jack G. Truong , Willa M. Studiner , Bradford B. Wright , Michael M. Rock, Jr.
IPC分类号： D06M15/356 , D04H1/64 , D06M13/02 , D06M13/503 , D06M15/333 , D06M101/00 , D06M101/02 , D06M101/06 , D06M101/16 , D06M101/18 , D06M101/30 , D06M101/32
CPC分类号： D04H1/64 , D04H1/587 , Y10T442/20 , Y10T442/2352 , Y10T442/2369 , Y10T442/2861 , Y10T442/2877 , Y10T442/60 , Y10T442/676
摘要： Nonwoven articles having high durability and absorbent characteristics, and their methods of manufacture, are presented. One preferred article is characterized by(a) a nonwoven web comprised of organic fibers comprised of polymers having a plurality of pendant hydroxyl groups; and(b) a binder comprising an at least partially crosslinked and at least partially hydrolyzed polymeric resin having a plurality of pendant resin hydroxyl groups, the resin crosslinked by a crosslinking agent, the crosslinking agent selected from the group consisting of organic titanates and amorphous metal oxides, the polymeric resin derived from monomers selected from the group consisting of monomers within the general formula ##STR1## wherein: X is selected from the group consisting of Si(OR.sup.4 OR.sup.5 OR.sup.6) and O(CO)R.sup.7 ; andR.sup.1 -R.sup.7 inclusive are independently selected from the group consisting of hydrogen and organic radicals having from 1 to about 10 carbon atoms, inclusive, and combinations thereof.
摘要翻译：提出了具有高耐久性和吸收特性的非织造物品及其制造方法。一个优选的制品的特征在于：（a）由具有多个侧基羟基的聚合物组成的有机纤维组成的非织造网; 和（b）包含至少部分交联和至少部分水解的聚合物树脂的粘合剂，所述树脂具有多个侧链树脂羟基，所述树脂由交联剂交联，所述交联剂选自有机钛酸盐和非晶态金属氧化物，衍生自选自以下通式的单体的单体的聚合物树脂其中：X选自Si（OR 4 OR 5 OR 6）和O（CO）R 7; 和R 1 -R 7独立地选自氢和具有1至约10个碳原子的有机基团，以及它们的组合。

9. 发明授权

US5883019A Nonwoven articles 失效
标题翻译：无纺布制品
公开(公告)号：US5883019A
公开(公告)日：1999-03-16
申请号：US653878
申请日：1996-05-28
申请人： Jack G. Troung , Bradford B. Wright , Michael M. Rock, Jr.
发明人： Jack G. Troung , Bradford B. Wright , Michael M. Rock, Jr.
IPC分类号： D06M15/356 , D04H1/64 , D06M13/02 , D06M13/503 , D06M15/333 , D06M101/00 , D06M101/02 , D06M101/06 , D06M101/16 , D06M101/18 , D06M101/30 , D06M101/32 , D04H1/58
CPC分类号： D04H1/64 , D04H1/587 , Y10T442/20 , Y10T442/2352 , Y10T442/2369 , Y10T442/2861 , Y10T442/2877 , Y10T442/60 , Y10T442/676
摘要： Nonwoven articles having high durability and absorbent-characteristics, and their methods of manufacture, are presented. One preferred article is characterized by(a) a nonwoven web comprised of organic fibers comprised of polymers having a plurality of pendant hydroxyl groups; and(b) a binder comprising an at least partially crosslinked and at least partially hydrolyzed polymeric resin having a plurality of pendant resin hydroxyl groups, the resin crosslinked by a crosslinking agent, the crosslinking agent selected from the group consisting of organic titanates and amorphous metal oxides, the polymeric resin derived from monomers selected from the group consisting of monomers within the general formula ##STR1## wherein: X is selected from the group consisting of Si(OR.sup.4 OR.sup.5 OR.sup.6) and O(CO)R.sup.7 ; andR.sup.1 -R.sup.7 inclusive are independently selected from the group consisting of hydrogen and organic radicals having from 1 to about 10 carbon atoms, inclusive, and combinations thereof.
摘要翻译：提出了具有高耐久性和吸收特性的非织造制品及其制造方法。一个优选的制品的特征在于：（a）由具有多个侧基羟基的聚合物组成的有机纤维组成的非织造网; 和（b）包含至少部分交联和至少部分水解的聚合物树脂的粘合剂，所述树脂具有多个侧链树脂羟基，所述树脂由交联剂交联，所述交联剂选自有机钛酸盐和非晶态金属氧化物，衍生自选自以下通式的单体的单体的聚合物树脂：其中：X选自Si（OR 4 OR 5 OR 6）和O（CO）R 7; 和R 1 -R 7独立地选自氢和具有1至约10个碳原子的有机基团，以及它们的组合。

10. 发明授权

US4954416A Tethered sulfonium salt photoinitiators for free radical polymerization 失效
标题翻译：用于自由基聚合的连接的锍盐光引发剂
公开(公告)号：US4954416A
公开(公告)日：1990-09-04
申请号：US287909
申请日：1988-12-21
申请人： Bradford B. Wright , Robert J. DeVoe
发明人： Bradford B. Wright , Robert J. DeVoe
IPC分类号： C07C381/12 , C07D209/86 , C07D295/096 , C07D295/112 , C07D295/135 , C08F2/50 , G03F7/029
CPC分类号： C07D295/096 , C07C381/12 , C07D209/86 , C07D295/112 , C07D295/135 , C08F2/50 , G03F7/029 , Y10S430/117 , Y10S430/122
摘要： Free radical polymerizable compositions contain a sulfonium salt which is tethered to at least one of an electron donor and a sensitizer, and a polymerizable monomer, demonstrate substantially enhanced photosensitivity. This invention also provides layered structures comprising a substrate coated with a free radical polymerizable composition containing a sulfonium salt which is tethered to at least one of an electron donor and a sensitizer, and the polymerized layered structures. A method for the preparation of certain tethered sulfonium salts is described.

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