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1. 发明授权

US08039646B2 Process for preparing glycidyloxyalkyltrialkoxysilanes 有权
标题翻译：缩水甘油氧基烷基三烷氧基硅烷的制备方法
公开(公告)号：US08039646B2
公开(公告)日：2011-10-18
申请号：US12521872
申请日：2007-12-20
申请人： Stefan Bade , Beate Seliger , Norbert Schladerbeck , Joerg Sauer
发明人： Stefan Bade , Beate Seliger , Norbert Schladerbeck , Joerg Sauer
IPC分类号： C07D303/22
CPC分类号： C07F7/1876 , C07F7/0829
摘要： The present invention relates to a process for preparing glycidyloxy-alkylalkoxysilanes of the general formula (I) (R″)O—CnH2nSi(R′)m(OR)3-m(I) in which R and R′ groups are each independently linear or branched alkyl groups having from 1 to 4 carbon atoms, n is 1, 2, 3, 4, 5, 6, 7 or 8 and m is 0, 1, 2 or 3, and R″ is an H2C(O)CH— or H2C(O)CHCH2— group, by reacting (i) a functionalized alkene of the general formula (II) (R″)O—CnH2n-1(II) in which R″ is an H2C(O)CH— or H2C(O)CHCH2— group and n is 1, 2, 3, 4, 5, 6, 7 or 8 with (ii) at least one hydroalkoxy-silane of the general formula (III) HSi(R′)m(OR)3-m (III) in which R and R′ groups are each independently linear or branched alkyl groups having from 1 to 4 carbon atoms and m is 0, 1, 2 or 3, in the presence (iii) of at least one homogeneous catalyst, (iv) of at least one solvent and/or of a diluent and (v) of at least one promoter.
摘要翻译：本发明涉及制备通式（I）（R“）O-C n H 2n（R'）m（OR）3-m（I）的缩水甘油氧基 - 烷基烷氧基硅烷的方法，其中R和R'各自独立地具有1至4个碳原子的直链或支链烷基，n为1,2,3,4,5,6,7或8，m为0,1,2或3，R“为H 2 C（O）通过使（i）通式（II）的官能化烯烃（R“）O-C n H 2n-1（II）反应，其中R”是H 2 C（O）CH- 或H 2 C（O）CHCH 2 - 基，n为1,2,3,4,5,6,7或8，（ii）至少一种通式（III）的氢烷氧基硅烷HSi（R'）m（ OR）3-m（III），其中R和R'基团各自独立地为具有1至4个碳原子的直链或支链烷基，m为0,1,2或3，在（iii）至少一种均相催化剂，（iv）至少一种溶剂和/或稀释剂，和（v）至少一种助催化剂。

2. 发明申请

US20110150739A1 METHOD FOR REMOVING BORON-CONTAINING IMPURITIES FROM HALOGEN SILANES AND APPARATUS FOR PERFORMING SAID METHOD 审中-公开
标题翻译：从卤素硅烷中除去含硼含量的方法和实施方法的方法
公开(公告)号：US20110150739A1
公开(公告)日：2011-06-23
申请号：US12999240
申请日：2009-04-23
申请人： Beate Seliger , Norbert Schladerbeck , Ingo Pauli , Andre Mecklenburg , Reinhold Schork , Hartwig Rauleder , Frank Kropfgans , Joachim Diefenbach
发明人： Beate Seliger , Norbert Schladerbeck , Ingo Pauli , Andre Mecklenburg , Reinhold Schork , Hartwig Rauleder , Frank Kropfgans , Joachim Diefenbach
IPC分类号： C01B33/08 , B01D3/34 , B01D3/02
CPC分类号： C01B33/03 , C01B33/107 , C01B33/10742 , C01B33/10778 , C01B33/10784
摘要： The invention relates to a method for reducing the content of boron-containing compounds in compositions I comprising at least one silicon halide, especially of chlorosilanes of the type HnSiCI4-n with n being equal to 0, 1, 2 or 3, by introducing a small amount of moisture into the composition I in a first step and separating the hydrolyzed boron- and/or silicon-containing compounds in a second step in such a way that a pre-purified composition II having a reduced boron content is obtained, wherein, in particular, the first and second steps can be run in at least one or more cycles. Also claimed is an apparatus for performing the method and an overall system into which this apparatus is integrated.
摘要翻译：本发明涉及一种降低组合物I中含硼化合物含量的方法，其包含至少一种卤化硅，特别是H nSiCl 4-n类型的氯硅烷，其中n等于0,1,2或3，通过引入在第一步骤中将少量水分加入到组合物I中，并在第二步骤中分离水解的硼和/或含硅化合物，使得获得具有降低的硼含量的预纯化组合物II，其中，特别地，第一和第二步骤可以在至少一个或多个循环中运行。还要求保护的是一种用于执行该装置的集成方法和整个系统的装置。

3. 发明申请

US20100036146A1 PROCESS FOR PREPARING GLYCIDYLOXYALKYLTRIALKOXYSILANES 有权
标题翻译：制备甘氨酰氧基甲基环氧树脂的方法
公开(公告)号：US20100036146A1
公开(公告)日：2010-02-11
申请号：US12521872
申请日：2007-12-20
申请人： Stefan Bade , Beate Seliger , Norbert Schladerbeck , Joerg Sauer
发明人： Stefan Bade , Beate Seliger , Norbert Schladerbeck , Joerg Sauer
IPC分类号： C07F7/08
CPC分类号： C07F7/1876 , C07F7/0829
摘要： The present invention relates to a process for preparing glycidyloxy-alkylalkoxysilanes of the general formula (I) (R″)O—CnH2nSi(R′)m(OR)3-m (I) in which R and R′ groups are each independently linear or branched alkyl groups having from 1 to 4 carbon atoms, n is 1, 2, 3, 4, 5, 6, 7 or 8 and m is 0, 1, 2 or 3, and R″ is an H2C(O)CH— or H2C(O)CHCH2— group, by reacting (i) a functionalized alkene of the general formula (II) (R″)O—CnH2n-1(II) in which R″ is an H2C(O)CH— or H2C(O)CHCH2— group and n is 1, 2, 3, 4, 5, 6, 7 or 8 with (ii) at least one hydroalkoxy-silane of the general formula (III) HSi(R′)m(OR)3-m (III) in which R and R′ groups are each independently linear or branched alkyl groups having from 1 to 4 carbon atoms and m is 0, 1, 2 or 3, in the presence (iii) of at least one homogeneous catalyst, (iv) of at least one solvent and/or of a diluent and (v) of at least one promoter.
摘要翻译：本发明涉及通式（I）（R“）O-C n H 2n（R'）m（OR）3-m（I）的缩水甘油氧基 - 烷基烷氧基硅烷的制备方法，其中R和R'各自为具有1至4个碳原子的独立的直链或支链烷基，n为1,2,3,4,5,6,7或8，m为0,1,2或3，R“为H 2 C（ O）CH-或H 2 C（O）CHCH 2 - 基，通过使（i）通式（II）的官能化烯烃（R“）O-C n H 2n-1（II）（其中R”是H 2 C O）CH-或H 2 C（O）CHCH 2 - 基，n为1,2,3,4,5,6,7或8，（ii）至少一种通式（III）的氢烷氧基硅烷HSi（R '）m（OR）3-m（III）其中R和R'各自独立地为具有1至4个碳原子的直链或支链烷基，m为0,1,2或3，（iii ）至少一种均相催化剂，（iv）至少一种溶剂和/或稀释剂和（v）至少一种助催化剂。

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