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1. 发明授权

US08734547B2 Processes for preparing a catalyzed carbonaceous particulate 有权
标题翻译：制备催化碳质颗粒的方法
公开(公告)号：US08734547B2
公开(公告)日：2014-05-27
申请号：US12648469
申请日：2009-12-29
申请人： Alkis S. Rappas , Robert A. Spitz
发明人： Alkis S. Rappas , Robert A. Spitz
IPC分类号： B01J23/04 , C07C4/00
CPC分类号： C10J3/00 , C10J3/482 , C10J2300/0903 , C10J2300/0916 , C10J2300/0943 , C10J2300/0973 , C10J2300/0986 , C10J2300/1807 , C10J2300/1853 , C10L3/08 , C10L9/08 , Y02P20/52
摘要： Processes are provided for preparing a substantially free-flowing alkali metal gasification catalyst-loaded carbonaceous particulate suitable for use as a feedstock for the production of gaseous products, and in particular methane, via the catalytic gasification of the catalyst-loaded carbonaceous particulate in the presence of steam.
摘要翻译：提供了制备基本上自由流动的碱金属气化催化剂负载的碳质颗粒的方法，该碳质颗粒适合用作生产气态产物，特别是甲烷的原料，通过在存在下催化剂负载的碳质颗粒的催化气化的蒸汽。

2. 发明申请

US20110262323A1 HYDROMETHANATION OF A CARBONACEOUS FEEDSTOCK WITH VANADIUM RECOVERY 有权
标题翻译：一种具有VANADIUM恢复的碳酸饲料的水解
公开(公告)号：US20110262323A1
公开(公告)日：2011-10-27
申请号：US13094438
申请日：2011-04-26
申请人： Alkis S. Rappas , Robert A. Spitz
发明人： Alkis S. Rappas , Robert A. Spitz
IPC分类号： C01G31/00
CPC分类号： C10J3/00 , C10J2300/0943 , C10J2300/0966 , C10J2300/0973 , C10J2300/0986 , C10J2300/1807 , C10J2300/1823 , C10L3/08 , C22B7/00 , C22B34/22 , C22B34/225 , Y02P10/23
摘要： The present invention relates to processes and apparatuses for hydromethanating a vanadium-containing carbonaceous feedstock while recovering at least a portion of the vanadium content originally present in the carbonaceous feedstock.
摘要翻译：本发明涉及用于在含钒原料中初始存在的至少一部分钒含量的同时含钒含碳原料进行氢化反应的方法和装置。

3. 发明申请

US20100168495A1 Processes for Preparing a Catalyzed Carbonaceous Particulate 有权
标题翻译：制备催化的碳质颗粒的方法
公开(公告)号：US20100168495A1
公开(公告)日：2010-07-01
申请号：US12648469
申请日：2009-12-29
申请人： Alkis S. Rappas , Robert A. Spitz
发明人： Alkis S. Rappas , Robert A. Spitz
IPC分类号： C07C1/00 , B05D3/02
CPC分类号： C10J3/00 , C10J3/482 , C10J2300/0903 , C10J2300/0916 , C10J2300/0943 , C10J2300/0973 , C10J2300/0986 , C10J2300/1807 , C10J2300/1853 , C10L3/08 , C10L9/08 , Y02P20/52
摘要： Processes are provided for preparing a substantially free-flowing alkali metal gasification catalyst-loaded carbonaceous particulate suitable for use as a feedstock for the production of gaseous products, and in particular methane, via the catalytic gasification of the catalyst-loaded carbonaceous particulate in the presence of steam.
摘要翻译：提供了制备基本上自由流动的碱金属气化催化剂负载的碳质颗粒的方法，该碳质颗粒适合用作生产气态产物，特别是甲烷的原料，通过在存在下催化剂负载的碳质颗粒的催化气化的蒸汽。

4. 发明申请

US20090165382A1 Catalytic Gasification Process with Recovery of Alkali Metal from Char 审中-公开
标题翻译：催化气化过程，从碱中回收碱金属
公开(公告)号：US20090165382A1
公开(公告)日：2009-07-02
申请号：US12342715
申请日：2008-12-23
申请人： Alkis S. Rappas , Robert A. Spitz
发明人： Alkis S. Rappas , Robert A. Spitz
IPC分类号： C10J3/00 , C22B26/10
CPC分类号： C10J3/00 , C10J3/463 , C10J2300/0903 , C10J2300/093 , C10J2300/0943 , C10J2300/0973 , C10J2300/0986 , C10J2300/16 , C10J2300/1631 , C10J2300/169 , C10J2300/1807 , C10J2300/1853 , C10K1/004 , C10K1/101 , C10K1/122 , C10K1/143 , C10K1/146 , C10K1/16 , C10K1/165
摘要： Processes for extracting and recycling alkali metal compounds present in the char produced from the catalytic gasification of carbonaceous materials are provided involving at least contacting the char with and alkali metal hydroxide followed by carbon dioxide. Both the alkali metal hydroxide and carbon dioxide treatments serve to convert at least a portion of the insoluble alkali metal compounds in the char into soluble species which can be recovered and recycled.
摘要翻译：提供了提取和回收存在于由碳质材料的催化气化产生的焦炭中的碱金属化合物的方法，其涉及至少使焦炭与碱金属氢氧化物接触二氧化碳接触。碱金属氢氧化物和二氧化碳处理都用于将焦炭中的至少一部分不溶性碱金属化合物转化为可回收和再循环的可溶性物质。

5. 发明授权

US06402940B1 Process for removing low amounts of organic sulfur from hydrocarbon fuels 失效
标题翻译：从碳氢燃料中除去少量有机硫的方法
公开(公告)号：US06402940B1
公开(公告)日：2002-06-11
申请号：US09654016
申请日：2000-09-01
申请人： Alkis S. Rappas
发明人： Alkis S. Rappas
IPC分类号： C10G2922
CPC分类号： C10G27/12
摘要： A process for desulfurizing fuels such as diesel oil and similar petroleum products to reduce the sulfur content to a range of from about 2 to 15 ppm sulfur is described. The sulfur containing fuel is contacted at slightly elevated temperatures with an oxidizing/extracting solution of formic acid, a small amount of hydrogen peroxide, and no more than about 25 wt % water. A removal process for separating substituted dibenzothiophene oxidation products from tile fuel is also described.
摘要翻译：描述了将柴油和类似石油产品的燃料脱硫以将硫含量降低至约2至15ppm硫的范围的方法。含硫燃料在稍高的温度下与甲酸，少量过氧化氢和不超过约25重量％的水的氧化/萃取溶液接触。还描述了从瓦片燃料中分离取代的二苯并噻吩氧化产物的去除方法。

6. 发明授权

US4891067A Processes for the treatment of smelter flue dust 失效
标题翻译：冶炼烟尘处理工艺
公开(公告)号：US4891067A
公开(公告)日：1990-01-02
申请号：US193873
申请日：1988-05-13
申请人： Alkis S. Rappas , Brett T. Waterman
发明人： Alkis S. Rappas , Brett T. Waterman
IPC分类号： C22B7/02
CPC分类号： C22B7/02 , Y02P10/212
摘要： A process for the treatment of flue dust from copper and lead smelters includes the steps of subjecting a slurry (10) of water and flue dust to a first caustic leach (12) to form a first liquids soluble sulfate solution (14) and a first solids portion (15), subjecting the solids portion to a second caustic leach (16) to solubilize lead and arsenic in a second liquid portion (22) and, selectively extracting the arsenic from the second liquid portion by precipitation (23). A related process for the treatment of flue dust allows for the recovery of bismuth and includes the steps of separating (53) a slurry of water and flue dust into a first liquids (54) and first solids (63) portion, neutralizing (55) the first liquids portion to form a second liquids soluble sulfate solution (58) and a second solids portion (59), subjecting the first solids (63) portion to a first caustic leach (61) to produce a third liquids (66) and third solids portion (82), subjecting the third liquids portion (66) and the second solids portion (59) to a second caustic leach (60) to produce a fourth liquids (68) and fourth solids portion (91) and, selectively extracting arsenic from the fourth liquids portion (68) and bismuth from the third solids portion (82). A process for the recovery of soluble lead values from lead compounds includes the steps of subjecting a slurry (100) of the lead compound to a caustic leach (101) to solubilize the lead and oxidizing the lead in an electrolytic cell (38) to form lead oxide.
摘要翻译：用于处理来自铜和铅冶炼厂的烟道灰尘的方法包括以下步骤：使水和烟道灰尘的浆料（10）进行第一苛性浸出（12）以形成第一液体可溶性硫酸盐溶液（14）和第一固体部分（15），使固体部分进行第二苛性浸出（16）以将铅和砷溶解在第二液体部分（22）中，并且通过沉淀（23）选择性地从第二液体部分提取砷。用于处理烟道灰尘的相关方法允许回收铋，并且包括将水和烟道灰分的浆料分离（53）到第一液体（54）和第一固体（63）部分中的步骤，中和（55）所述第一液体部分形成第二液体可溶性硫酸盐溶液（58）和第二固体部分（59），使所述第一固体（63）部分经受第一苛性浸出物（61）以产生第三液体（66）和第三液体固体部分（82），使第三液体部分（66）和第二固体部分（59）经受第二苛性浸出（60）以产生第四液体（68）和第四固体部分（91），并且选择性地提取砷从第四液体部分（68）和来自第三固体部分（82）的铋。从铅化合物回收可溶性铅值的方法包括以下步骤：使铅化合物的浆料（100）进行苛性浸出（101）以溶解铅并将铅氧化成电解池（38）以形成氧化铅

7. 发明授权

US4128416A Nickel recovery employing carbonyl ferrates 失效
标题翻译：使用羰基高铁酸盐的镍回收
公开(公告)号：US4128416A
公开(公告)日：1978-12-05
申请号：US868054
申请日：1978-01-09
申请人： Alkis S. Rappas , J. Paul Pemsler
发明人： Alkis S. Rappas , J. Paul Pemsler
IPC分类号： C22B23/06 , C22B23/04
CPC分类号： C22B23/065 , Y02P10/212
摘要： A novel process for recovering nickel metal from aqueous ammoniacal nickel solutions such as leach liquors at or close to ambient temperatures and pressures. The process comprises contacting the nickel solution with carbonyl ferrate ions such as HFe(CO).sub.4.sup.- or Fe(CO).sub.4.sup.-- in the presence of carbon monoxide to produce nickel carbonyl. The nickel carbonyl is collected as a gas, concentrated, and decomposed to produce nickel metal and carbon monoxide. The carbonyl ferrate ions may conveniently be produced by subjecting an iron pentacarbonyl solution to an aqueous alkaline solution containing potassium hydroxide or the like. The nickel depleted ammoniacal liquor is purged of iron resulting from the nickel carbonylation treatment by oxidizing the ferrous values to iron oxide and may thereafter be recycled to solubilize additional nickel values. The iron oxide in turn may be reduced to iron pentacarbonyl and treated with an aqueous alkaline solution for reuse in carbonylation of additional nickel values.
摘要翻译：一种从或接近环境温度和压力从含水氨溶液如浸出液中回收镍金属的新方法。该方法包括在一氧化碳存在下使镍溶液与羰基高铁酸根离子例如HFe（CO）4-或Fe（CO）4-）接触以产生羰基镍。将羰基镍作为气体收集，浓缩并分解以产生镍金属和一氧化碳。羰基高铁酸盐离子可以方便地通过使铁五羰基铁溶液经受含有氢氧化钾等的碱性水溶液来制备。将镍贫化的氨水从镍羰基化处理中清除出来，通过将亚铁值氧化成氧化铁，然后再循环以溶解额外的镍值。氧化铁又可以还原成五羰基铁，并用碱性水溶液处理以再次用于另外的镍值的羰基化。

8. 发明授权

US4097272A Winning nickel and cobalt with mercaptide extractants and carbon monoxide strip 失效
标题翻译：获得镍和钴与硫醇萃取剂和一氧化碳条
公开(公告)号：US4097272A
公开(公告)日：1978-06-27
申请号：US831502
申请日：1977-09-08
申请人： Alkis S. Rappas , J. Paul Pemsler
发明人： Alkis S. Rappas , J. Paul Pemsler
IPC分类号： C01G51/00 , C01G53/00 , C22B3/34 , C22B23/06 , C22B23/04 , C01G51/02 , C01G53/02 , C07C149/00
CPC分类号： C22B23/065 , C01G51/003 , C01G53/003 , C22B3/0031 , Y02P10/234
摘要： A novel process for extracting, concentrating, and isolating nickel and cobalt from aqueous solution thereof. A cobalt and/or nickel bearing solution is contacted with an extractant comprising a substantially water immiscible organic solvent containing solubilized mercaptide anion to form water insoluble cobalt and nickel mercaptides in the organic phase. The organic phase is then separated from the raffinate and contacted with an alkaline solution and carbon monoxide to produce nickel and cobalt carbonyl compounds. Typically, the nickel carbonyl produced is gaseous Ni(CO).sub.4 which may be easily isolated by known methods from other components in the off-gas stream. Pure nickel metal is then obtained from the nickel tetracarbonyl by known methods. The cobalt carbonyl compound produced is typically water soluble carbonyl cobaltate ion, Co(CO).sub.4.sup.-, which may be oxidized to form water insoluble cobalt carbonyl compounds. The stripped extractant, the cobalt and nickel-free raffinate, and the carbon monoxide from the decomposition of carbonyl may be recycled.
摘要翻译：一种从其水溶液中提取，浓缩和分离镍和钴的新方法。将含钴和/或镍的溶液与包含基本上与水溶性的含硫醇阴离子的水不混溶的有机溶剂的萃取剂接触，以在有机相中形成不溶于水的钴和镍硫醇。然后将有机相与萃余液分离，并与碱性溶液和一氧化碳接触以产生镍和钴羰基化合物。通常，生产的羰基镍是气态Ni（CO）4，其可以通过已知方法从废气流中的其它组分容易地分离。然后通过已知的方法从四羰基镍获得纯镍金属。所生产的羰基钴化合物通常是水溶性羰基钴酸根离子Co（CO）4-，其可被氧化形成水不溶性羰基钴化合物。剥离的萃取剂，不含钴和镍的提余液和羰基分解中的一氧化碳可以循环使用。

9. 发明申请

US20120213680A1 HYDROMETHANATION OF A CARBONACEOUS FEEDSTOCK WITH NICKEL RECOVERY 有权
标题翻译：具有镍回收率的碳酸饲料的水解
公开(公告)号：US20120213680A1
公开(公告)日：2012-08-23
申请号：US13402022
申请日：2012-02-22
申请人： Alkis S. Rappas , Robert A. Spitz
发明人： Alkis S. Rappas , Robert A. Spitz
IPC分类号： C01G53/00 , C25C1/08 , C22B23/00 , C07C1/00
CPC分类号： C10J3/00 , C10J2300/0903 , C10J2300/0943 , C10J2300/0976 , C10J2300/0986 , C10J2300/1628 , C10J2300/1662 , C10J2300/1807 , C10J2300/1823 , C22B7/008 , C22B23/04 , C22B23/0446 , Y02P10/234
摘要： The present invention relates to processes for hydromethanating a nickel-containing (and optionally vanadium-containing) carbonaceous feedstock while recovering at least a portion of the nickel content (and optionally vanadium content) originally present in the carbonaceous feedstock.
摘要翻译：本发明涉及含镍（和任选含钒的）碳质原料的氢化氢化方法，同时回收原始存在于碳质原料中的至少一部分镍含量（和任选的钒含量）。

10. 发明申请

US20090217590A1 Coal Compositions for Catalytic Gasification 有权
公开(公告)号：US20090217590A1
公开(公告)日：2009-09-03
申请号：US12395348
申请日：2009-02-27
申请人： Alkis S. Rappas , George Frederick Salem
发明人： Alkis S. Rappas , George Frederick Salem
IPC分类号： C10J3/00 , B01J23/02 , B01J23/34 , B01J23/78
CPC分类号： C10J3/00 , B01J23/02 , B01J23/04 , B01J23/34 , B01J23/745 , B01J23/78 , B01J35/0006 , C10J3/482 , C10J2300/0903 , C10J2300/093 , C10J2300/0973 , C10J2300/0983 , C10J2300/0986 , C10J2300/1853 , C10L5/00 , C10L9/00 , Y02P20/52
摘要： Particulate compositions are described comprising an intimate mixture of a coal and a gasification catalyst in the presence of steam to yield a plurality of gases including methane and at least one or more of hydrogen, carbon monoxide, carbon dioxide, hydrogen sulfide, ammonia and other higher hydrocarbons are formed. Processes are also provided for the preparation of the particulate compositions and converting the particulate composition into a plurality of gaseous products.

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