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    • 8. 发明授权
    • Ordered open-cellular carbon microstructure and method of making same
    • 有序的开孔碳微观结构及其制备方法
    • US08585944B1
    • 2013-11-19
    • US11870379
    • 2007-10-10
    • Alan J. Jacobsen
    • Alan J. Jacobsen
    • B29D11/00
    • C01B31/00B29C67/20B29D11/00663G02B6/12002G02B6/1221G02B2006/1219
    • An ordered open-cellular carbon microstructure and a methods for forming the ordered open-cellular carbon microstructure capable of greatly improving the carbon yield (remaining mass % after carbonization) of an open-cellular polymer material. In one embodiment, the method starts with providing an ordered open-cellular polymer template material. The polymer template material is immersed in a reservoir containing a liquid monomer solution, wherein the liquid monomer solution swells the polymer material. Then the polymer template material is removed from the reservoir containing liquid monomer solution. Excess liquid monomer solution is removed from the polymer template material. The liquid monomer solution absorbed into the polymer template material is polymerized forming a copolymer material by irradiating the template material with ultraviolet (UV) light in a nitrogen environment. The copolymer material is heated in an inert atmosphere, wherein the copolymer material is carbonized resulting in the ordered open-cellular carbon microstructure.
    • 有序的开孔碳微观结构和形成有序的开孔细胞碳微结构的方法,能够大大提高开孔聚合物材料的碳产率(碳化后剩余质量%)。 在一个实施方案中,该方法开始于提供有序的开孔聚合物模板材料。 将聚合物模板材料浸入含有液体单体溶液的储存器中,其中液体单体溶液使聚合物材料膨胀。 然后从包含液体单体溶液的储存器中取出聚合物模板材料。 从聚合物模板材料中除去过量的液体单体溶液。 吸收到聚合物模板材料中的液体单体溶液通过在氮气环境中用紫外线(UV)光照射模板材料而聚合形成共聚物材料。 将共聚物材料在惰性气氛中加热,其中共聚物材料被碳化,导致有序的开孔碳微观结构。