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1. 发明授权

US09956539B2 Apparatus for location-independent treatment of biomass 有权
公开(公告)号：US09956539B2
公开(公告)日：2018-05-01
申请号：US14659777
申请日：2015-03-17
申请人： AVA-CO2 Schweiz AG
发明人： Jan Vyskocil , Stepan Kusche
IPC分类号： A61L2/00 , F26B3/34 , F26B19/00 , B01J19/24 , C10L9/08
CPC分类号： B01J19/24 , B01J2219/0002 , B01J2219/2401 , C10L9/086 , Y02E50/10 , Y02E50/30
摘要： Within the scope of hydrothermal carbonization, biomass is converted to bio-coal and other products. Because biomass occurs at irregular intervals at different locations and also, in part, only individual method steps are required at different locations, however, an apparatus for treatment of biomass is integrated into a variable, mobile container, and mobile containers adapted to the individual steps of the method are provided, which can be transported in compact manner and can be adapted, in terms of size, in the setup situation. This arrangement allows effective equipping of the individual containers, which can be expanded into a setup situation on location.

2. 发明申请

US20170007980A1 PROCESS FOR THE PRODUCTION OF HIGH-QUALITY ACTIVATED CARBONS AS WELL AS ACTIVATED CARBONS PRODUCED ACCORDING TO THE PROCESS 审中-公开
标题翻译：生产高品质活性炭的方法，如活性炭生产过程中的碳
公开(公告)号：US20170007980A1
公开(公告)日：2017-01-12
申请号：US15272779
申请日：2016-09-22
申请人： AVA-CO2 Schweiz AG
发明人： Jan VYSKOCIL , Olga SAHIN , Mei Yun LAI , Andrea KRUSE
IPC分类号： B01J20/20 , C01B31/08 , C01B31/12 , B01J20/28
CPC分类号： B01J20/20 , B01J20/28064 , B01J20/28066 , B01J20/28095 , B01J20/3064 , C01B32/324 , C01B32/342
摘要： A process for the production of high-quality activated carbons from carbonized, self-regenerating, carbon-containing biomasses selects the carbonized biomasses from HTC carbon from fruit stones and HTC carbon from nut shells. The carbonized biomasses together with potassium hydroxide, sodium hydroxide or a mixture of both hydroxides as activator are subjected to a heat treatment at temperatures at which the activator exists in the form of a melt. The activator and the carbonized biomasses are present in a weight ratio of 0.5:1 to 6:1 at the beginning of the heat treatment.
摘要翻译：从碳化，自再生，含碳生物质生产高质量活性炭的方法选择来自果实结晶的HTC碳和来自坚果壳的HTC碳的碳化生物质。将碳化的生物质与氢氧化钾，氢氧化钠或氢氧化物作为活化剂的混合物一起在熔融物形式存在的活化剂的温度下进行热处理。在热处理开始时，活化剂和碳化生物质以0.5:1至6:1的重量比存在。

3. 发明申请

US20150259209A1 METHOD AND APPARATUS FOR CARRYING OUT A HYDROTHERMAL CARBONIZATION REACTION AND USE OF A SENSOR OR ANALYSIS DEVICE FOR THIS PURPOSE 审中-公开
标题翻译：用于实施氢热碳化反应的方法和装置以及用于本发明的传感器或分析装置的用途
公开(公告)号：US20150259209A1
公开(公告)日：2015-09-17
申请号：US14644369
申请日：2015-03-11
申请人： AVA-CO2 Schweiz AG
发明人： Jan VYSKOCIL
IPC分类号： C01B31/02 , G05B15/02 , B01J19/24
CPC分类号： G05B15/02 , B01J19/24 , B01J2219/00164 , B01J2219/24 , C01B32/05 , C10L3/101 , C10L9/086 , C10L2290/546 , C10L2290/548 , Y02E50/10 , Y02E50/30
摘要： It is the goal of a hydrothermal carbonization reaction to obtain the best possible yield of specific substances, for example the greatest possible carbon yield. However, biomass of very different types and grades is fed into the process, so that the reaction can take place very differently within each individual batch. Influencing the process is generally problematical, because the process proceeds in closed manner. For this reason, it is proposed to assign a sensor or an analysis device for the total organic carbon for the dissolved organic carbon, or for fractions of the total organic carbon. An adaptation of the process parameters can then be undertaken manually or by way of a process controller, as a function of the sensor's measurement results.
摘要翻译：水热碳化反应的目标是获得最佳可能的特定物质的产率，例如最大的碳产量。然而，将非常不同类型和等级的生物质进料到该过程中，使得反应可以在每个单独的批次中发生非常不同。影响该过程通常是有问题的，因为该过程以封闭的方式进行。因此，建议为溶解的有机碳或总有机碳的部分分配用于总有机碳的传感器或分析装置。然后可以根据传感器的测量结果手动或通过过程控制器进行过程参数的调整。

4. 发明申请

US20150299874A1 METHOD FOR RECOVERY OF PHOSPHATE FROM A LIQUID PHASE 有权
标题翻译：从液相中回收磷酸盐的方法
公开(公告)号：US20150299874A1
公开(公告)日：2015-10-22
申请号：US14686924
申请日：2015-04-15
申请人： AVA-CO2 SCHWEIZ AG
发明人： Jan VYSKOCIL , Stepan KUSCHE , François BADOUX
IPC分类号： C25B1/18
CPC分类号： C25B1/18 , C02F1/46114 , C02F2001/46133 , C02F2101/105
摘要： Known phosphorus recovery methods from liquid phases proceed from the presence of ammonia or nitrate, and phosphate, in the liquid phase. Wastewater that is supposed to be freed of nitrate and phosphate pollution in sewage treatment facilities can be used as the liquid phase. In electrochemical methods, a magnesium electrode is used as a sacrificial anode, and ammonium and phosphate together are bound to the magnesium to form struvite, which in turn can be used in agriculture as a fertilizer, in useful manner. In an alternative method of procedure, first, only phosphates are removed from a liquid phase that occurs from the filtration of products of hydrothermal carbonization. A magnesium electrode is used as the cathode, so that the resulting magnesium phosphate does not go into solution and first must be precipitated, but rather is removed from the electrolysis cell directly with the cathode, after the reaction occurs.
摘要翻译：来自液相的已知磷回收方法在液相中从氨或硝酸盐和磷酸盐的存在进行。污水处理设施中应避免硝酸盐和磷酸盐污染的废水可用作液相。在电化学方法中，使用镁电极作为牺牲阳极，铵和磷酸盐一起结合镁形成鸟粪石，这又可用于农业作为肥料，以有用的方式。在另一种方法中，首先，从水热碳化产物的过滤产生的液相中仅除去磷酸盐。使用镁电极作为阴极，使得得到的磷酸镁不进入溶液中，并且首先必须沉淀，而是在反应发生后直接从阴极除去电解池。

5. 发明申请

US20150266001A1 APPARATUS FOR LOCATION-INDEPENDENT TREATMENT OF BIOMASS 有权
标题翻译：用于位置独立处理生物量的装置
公开(公告)号：US20150266001A1
公开(公告)日：2015-09-24
申请号：US14659777
申请日：2015-03-17
申请人： AVA-CO2 SCHWEIZ AG
发明人： Jan VYSKOCIL , Stepan KUSCHE
IPC分类号： B01J19/24
CPC分类号： B01J19/24 , B01J2219/0002 , B01J2219/2401 , C10L9/086 , Y02E50/10 , Y02E50/30
摘要： Within the scope of hydrothermal carbonization, biomass is converted to bio-coal and other products. Because biomass occurs at irregular intervals at different locations and also, in part, only individual method steps are required at different locations, however, an apparatus for treatment of biomass is integrated into a variable, mobile container, and mobile containers adapted to the individual steps of the method are provided, which can be transported in compact manner and can be adapted, in terms of size, in the setup situation. This arrangement allows effective equipping of the individual containers, which can be expanded into a setup situation on location.
摘要翻译：在水热碳化的范围内，生物质转化为生物煤等产品。因为生物体在不同位置处以不规则的间隔发生，并且部分地，在不同位置仅需要单独的方法步骤，然而，用于处理生物质的装置被集成到可变的移动容器中，并且适于各个步骤的移动容器的方法，其可以紧凑的方式运输，并且可以根据大小在设置情况下进行调整。这种布置允许单个容器的有效装备，其可以扩展到位置上的安装情况。

6. 发明申请

US20150209692A1 PROCESS AND APPARATUS FOR PURIFYING PROCESS WATER IN A HYDROTHERMAL CARBONIZATION PROCESS 审中-公开
标题翻译：在热水碳酸化工艺中净化工艺水的工艺和设备
公开(公告)号：US20150209692A1
公开(公告)日：2015-07-30
申请号：US14421537
申请日：2013-08-15
申请人： AVA-CO2 Schweiz AG
发明人： Jan Vyskocil
IPC分类号： B01D21/00 , B01D3/00 , C02F1/04 , C10L9/08 , C02F1/02
CPC分类号： B01D21/0087 , B01D3/00 , C02F1/025 , C02F1/04 , C02F1/38 , C02F11/10 , C02F2103/00 , C10L9/086 , C10L2290/06 , C10L2290/08 , C10L2290/146 , C10L2290/56 , Y02W10/40
摘要： Hydrothermal carbonization allows the production of charcoal from biomass. However, this biomass can at the beginning of the carbonization process contain constituents which are not suitable for carbonization. Apart from large contaminants such as broken glass, etc., these constituents are, in particular, sand and clay, with the clay not being able to be removed by simple filtration methods because of its fineness. The invention therefore provides for process water to be taken from the reaction space and subjected to purification in a sedimentation filter after the carbonization reaction has commenced and the clay is no longer held in the biomass. The process water is then sprayed back into the reaction space in order to keep the biomass/process water mixture in motion and avoid sedimentation of the clay at the bottom of the reaction space.
摘要翻译：水热碳化允许生物质生产木炭。然而，在碳化过程开始时，该生物质可以含有不适于碳化的成分。除了诸如碎玻璃等大的污染物之外，这些成分尤其是砂和粘土，由于其细度，粘土不能通过简单的过滤方法除去。因此，本发明提供了从碳酸化反应开始并且粘土不再保持在生物质中之后，从反应空间中取出的工艺用水并在沉淀过滤器中进行净化。然后将工艺水喷射回反应空间，以保持生物质/工艺水混合物的运动，并避免反应空间底部的粘土沉淀。

7. 发明授权

US09416030B2 Method for treatment of process water 有权
标题翻译：处理水处理方法
公开(公告)号：US09416030B2
公开(公告)日：2016-08-16
申请号：US14565673
申请日：2014-12-10
申请人： AVA-CO2 Schweiz AG
发明人： Jan Vyskocil , Stephan Koehler , François Badoux
IPC分类号： C02F1/44 , C10L9/08 , B01D63/00 , C07C51/47 , C07D307/48 , B01D61/14 , C02F1/26 , C02F103/36 , C02F101/34
CPC分类号： C02F1/44 , B01D61/142 , B01D63/00 , B01D2311/263 , B01D2313/38 , B01D2315/16 , B01D2317/02 , B01D2317/022 , B01D2317/025 , C02F1/26 , C02F2101/34 , C02F2103/365 , C07C51/47 , C07D307/48 , C10L9/086
摘要： Within the scope of hydrothermal carbonization of biomass, not only the main product, coal, but also the platform chemical 5-hydroxymethyl furfural, as well as furfural and levulinic acid, are formed. These are extracted from the process water of the carbonization reaction. However, in this connection, the problem exists that humic substances deposit on the container walls of the extraction column and can only be removed again by means of great cleaning effort. Furthermore, oligomers clearly worsen the purity of the product. This problem is solved by a filtration cascade through which the process water passes before extraction. In this connection, first the impurities mentioned are removed in a first filtration stage, and the remaining products and educts are separated from one another in a second filtration stage. Only the products are passed to extraction.
摘要翻译：在生物质水热碳化的范围内，不仅形成了主要产品，煤，而且平台化学的5-羟甲基糠醛，以及糠醛和乙酰丙酸。这些从碳化反应的工艺水中提取出来。然而，在这方面，存在腐殖质沉积在提取塔的容器壁上的问题，并且只能通过很大的清洁力再次去除。此外，低聚物显然恶化了产品的纯度。这个问题通过过滤级联来解决，通过该过滤级联，萃取前通过该过程。在这方面，首先在第一过滤阶段除去所提及的杂质，并且在第二过滤阶段将剩余的产物和溶出物彼此分离。只有产品才能提取。

8. 发明授权

US09816191B2 Method for recovery of phosphate from a liquid phase 有权
公开(公告)号：US09816191B2
公开(公告)日：2017-11-14
申请号：US14686924
申请日：2015-04-15
申请人： AVA-CO2 Schweiz AG
发明人： Jan Vyskocil , Stepan Kusche , François Badoux
IPC分类号： C02F1/461 , C25B1/18 , C02F101/10
CPC分类号： C25B1/18 , C02F1/46114 , C02F2001/46133 , C02F2101/105
摘要： Known phosphorus recovery methods from liquid phases proceed from the presence of ammonia or nitrate, and phosphate, in the liquid phase. Wastewater that is supposed to be freed of nitrate and phosphate pollution in sewage treatment facilities can be used as the liquid phase. In electrochemical methods, a magnesium electrode is used as a sacrificial anode, and ammonium and phosphate together are bound to the magnesium to form struvite, which in turn can be used in agriculture as a fertilizer, in useful manner. In an alternative method of procedure, first, only phosphates are removed from a liquid phase that occurs from the filtration of products of hydrothermal carbonization. A magnesium electrode is used as the cathode, so that the resulting magnesium phosphate does not go into solution and first must be precipitated, but rather is removed from the electrolysis cell directly with the cathode, after the reaction occurs.

9. 发明申请

US20160060141A1 METHOD FOR TREATMENT OF PROCESS WATER 有权
标题翻译：处理工艺水的方法
公开(公告)号：US20160060141A1
公开(公告)日：2016-03-03
申请号：US14565673
申请日：2014-12-10
申请人： AVA-CO2 Schweiz AG
发明人： Jan VYSKOCIL , Stephan KOEHLER , François BADOUX
IPC分类号： C02F1/44 , C07D307/48 , C07C51/47 , B01D63/00
CPC分类号： C02F1/44 , B01D61/142 , B01D63/00 , B01D2311/263 , B01D2313/38 , B01D2315/16 , B01D2317/02 , B01D2317/022 , B01D2317/025 , C02F1/26 , C02F2101/34 , C02F2103/365 , C07C51/47 , C07D307/48 , C10L9/086
摘要： Within the scope of hydrothermal carbonization of biomass, not only the main product, coal, but also the platform chemical 5-hydroxymethyl furfural, as well as furfural and levulinic acid, are formed. These are extracted from the process water of the carbonization reaction. However, in this connection, the problem exists that humic substances deposit on the container walls of the extraction column and can only be removed again by means of great cleaning effort. Furthermore, oligomers clearly worsen the purity of the product. This problem is solved by a filtration cascade through which the process water passes before extraction. In this connection, first the impurities mentioned are removed in a first filtration stage, and the remaining products and educts are separated from one another in a second filtration stage. Only the products are passed to extraction.
摘要翻译：在生物质水热碳化的范围内，不仅形成了主要产品，煤，而且平台化学的5-羟甲基糠醛，以及糠醛和乙酰丙酸。这些从碳化反应的工艺水中提取出来。然而，在这方面，存在腐殖质沉积在提取塔的容器壁上的问题，并且只能通过很大的清洁力再次去除。此外，低聚物显然恶化了产品的纯度。这个问题通过过滤级联来解决，通过该过滤级联，萃取前通过该过程。在这方面，首先在第一过滤阶段除去所提及的杂质，并且在第二过滤阶段将剩余的产物和溶出物彼此分离。只有产品才能提取。

10. 发明申请

US20160038913A1 PROCESS FOR THE PRODUCTION OF HIGH-QUALITY ACTIVATED CARBONS AS WELL AS ACTIVATED CARBONS PRODUCED ACCORDING TO THE PROCESS 审中-公开
标题翻译：生产高品质活性炭的方法，如活性炭生产过程中的碳
公开(公告)号：US20160038913A1
公开(公告)日：2016-02-11
申请号：US14820909
申请日：2015-08-07
申请人： AVA-CO2 Schweiz AG
发明人： Jan VYSKOCIL , Olga SAHIN , Mei Yun LAI , Andrea KRUSE
IPC分类号： B01J20/20 , B01J20/28 , B01J20/30 , C01B31/12
CPC分类号： B01J20/20 , B01J20/28064 , B01J20/28066 , B01J20/28095 , B01J20/3064 , C01B32/324 , C01B32/342
摘要： A process for the production of high-quality activated carbons from carbonized, self-regenerating, carbon-containing biomasses selects the carbonized biomasses from HTC carbon from fruit stones and HTC carbon from nut shells. The carbonized biomasses together with potassium hydroxide, sodium hydroxide or a mixture of both hydroxides as activator are subjected to a heat treatment at temperatures at which the activator exists in the form of a melt. The activator and the carbonized biomasses are present in a weight ratio of 0.5:1 to 6:1 at the beginning of the heat treatment.
摘要翻译：从碳化，自再生，含碳生物质生产高质量活性炭的方法选择来自果实结晶的HTC碳和来自坚果壳的HTC碳的碳化生物质。将碳化的生物质与氢氧化钾，氢氧化钠或氢氧化物作为活化剂的混合物一起在熔融物形式存在的活化剂的温度下进行热处理。在热处理开始时，活化剂和碳化生物质以0.5:1至6:1的重量比存在。

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