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    • 4. 发明授权
    • Process for the flame-retardant treatment of textiles
    • 纺织品阻燃处理工艺
    • US5942006A
    • 1999-08-24
    • US904238
    • 1997-07-31
    • Robert Cole
    • Robert Cole
    • D06B19/00D06B23/16D06M13/285D06M13/447D06M15/431D06M15/673
    • D06M13/447D06B19/00D06B23/16D06M13/285D06M15/431D06M15/673Y10T442/2672Y10T442/268Y10T442/2689Y10T442/2697
    • A process for the flame-retardant treatment of a cellulosic fabric by impregnating a fabric with an aqueous solution of a tetrakis (hydroxyorgano) phosphonium (THP) and then at least partially drying it. The partially dried impregnated fabric is passed at a speed of 30 to 100 m/minute once through a chamber containing ammonia for a single cure. Both the moisture contained in the fabric and water produced as a by-product of curing are volatilized and condensed on an interior wall of the chamber and flow down the walls to a drain for removal of the condensed water from the apparatus. The process further includes measuring the rate of ammonia in the gas fed into the chamber, determining the ammonia content of the gas and measuring the temperature within the chamber, for maintaining the initial concentration of ammonia in the gas at 70% to 90% by volume and for maintaining the ratio of ammonia input to the THP composition in the range of at least 1.2 to 1, on the basis of ammonia to phosphorus; withdrawing the treated fabric from the chamber, removing at least some of the gas from the chamber; and recycling at least some of the gas back into the chamber.
    • 通过用四(羟基有机)鏻(THP)的水溶液浸渍织物然后至少部分干燥纤维素织物来阻燃处理纤维素织物的方法。 部分干燥的浸渍织物以30-100m /分钟的速度通过一次通过含有氨的室,以进行单次固化。 包含在织物中的水分和作为固化的副产物产生的水都在室的内壁上挥发和冷凝,并且从壁流下到排水口,以从设备中除去冷凝水。 该方法还包括测量供给到室中的气体中的氨的速率,确定气体的氨含量和测量室内的温度,以保持气体中氨的初始浓度为70〜90体积% 并且用于将氨输入与THP组成的比例保持在至少1.2至1的范围内,基于氨与磷; 从室中取出经处理的织物,从室中去除至少一些气体; 并将至少一些气体再循环回到室中。