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81. 发明授权

US07771636B2 Single stage drawing for MPD-I yarn 有权
标题翻译： MPD-I纱单级拉丝
公开(公告)号：US07771636B2
公开(公告)日：2010-08-10
申请号：US12004142
申请日：2007-12-19
申请人： Mark H. Headinger , Edgar N. Rudisill , David W. Luckey
发明人： Mark H. Headinger , Edgar N. Rudisill , David W. Luckey
IPC分类号： B29C47/88 , D01D5/04 , D01D5/84 , D01D5/12
CPC分类号： D01D5/04 , D01D5/12 , D01D11/00 , D01F6/605
摘要： The invention relates to a continuous dry spinning process for preparing a fiber from a polymer solution having concentrations of polymer, salt, solvent and water. After the fiber is extruded and quenched, the fiber is placed in contact with a conditioning solution comprising concentrations of solvent, salt, and water. The conditioning solution acts upon the fiber to plasticize the fiber prior to being drawn. The conditioning solution has concentrations of solvent, salt, and water so that the fiber is plasticized to the extent necessary for drawing but does not plasticize the fiber to such an extent as to re-dissolve the fiber into a polymeric solution. A heat-treated fiber manufactured from this process has improved shrinkage and can be colored to darker shades.
摘要翻译：本发明涉及一种从具有聚合物，盐，溶剂和水的浓度的聚合物溶液制备纤维的连续干法纺丝方法。纤维被挤出和淬火后，将纤维置于与包含溶剂，盐和水的浓度的调理溶液接触。调理溶液作用于纤维，以在拉伸之前使纤维增塑。调理溶液具有溶剂，盐和水的浓度，使得纤维被塑化到拉伸所需的程度，但是不会将纤维增塑到使纤维再溶解成聚合物溶液的程度。由该方法制造的经热处理的纤维具有改善的收缩率并且可以着色到较暗的色调。

82. 发明申请

US20100122517A1 UHMWPE FIBER AND PROCESS FOR PRODUCING THEREOF 审中-公开
标题翻译： UHMWPE纤维及其制造方法
公开(公告)号：US20100122517A1
公开(公告)日：2010-05-20
申请号：US12598295
申请日：2008-04-25
申请人： Joseph Arnold Paul Maria Simmelink , Roelof Marissen , Victor Litvinov
发明人： Joseph Arnold Paul Maria Simmelink , Roelof Marissen , Victor Litvinov
IPC分类号： D02G3/02 , C08F110/02
CPC分类号： D01F6/04 , D01D5/04 , D01D5/12
摘要： The invention relates to gel-spun ultra high molecular weight polyethylene (UHMWPE) fibers and to a process for producing thereof. Specifically, the invention relates a gel-spun UHMWPE fiber comprising an UHMWPE having an intrinsic viscosity in decaline at 135° C. of at least 8 dl/g, and having a T1 relaxation time as measured by Solid-State proton NMR at 26° C. of at least 600 ms. The invention further relates to ropes, nets and composites, in particular composites for ballistic applications containing the UHMWPE fibers of the invention.
摘要翻译：本发明涉及凝胶纺超高分子量聚乙烯（UHMWPE）纤维及其制备方法。具体地说，本发明涉及包含UHFWPE的凝胶纺丝UHMWPE纤维，该UHMWPE在135℃下的十氢化萘中的特性粘度为至少8dl / g，并且具有通过26°固体质子NMR测量的T1弛豫时间 C.至少600 ms。本发明还涉及绳索，网和复合材料，特别是用于包含本发明的UHMWPE纤维的弹道应用的复合材料。

83. 发明申请

US20100028999A1 METHODS, APPARATUS, AND SYSTEMS FOR FABRICATION OF POLYMERIC NANO- AND MICRO-FIBERS IN ALIGNED CONFIGURATIONS 有权
标题翻译：用于制备聚对纳米和微型纤维在对准配置中的方法，装置和系统
公开(公告)号：US20100028999A1
公开(公告)日：2010-02-04
申请号：US12512893
申请日：2009-07-30
申请人： Amrinder Singh Nain
发明人： Amrinder Singh Nain
IPC分类号： C12N5/071 , B29C51/00 , B32B5/00 , B29C45/76
CPC分类号： C12N5/0075 , A61L27/3804 , A61L27/3895 , B81C99/003 , C12N5/0068 , C12N2513/00 , C12N2533/30 , C12N2533/40 , C12N2533/54 , C12N2537/00 , D01D5/04 , D01F6/22 , D10B2321/121 , D10B2331/041 , Y10T428/269
摘要： Provided herein are apparatus and systems for fabricating highly aligned arrays of polymeric fibers having isodiameters ranging from sub 50 nm to microns with lengths of several millimeters. The approach disclosed herein uses (e.g.) a micropipette to deliver polymeric solution which is collected in the form of aligned fibers on a rotating and linearly translating substrate. The methods deposit polymeric fibers on spherical surfaces and gapped surfaces with precise control, thus heralding new opportunities for a variety of applications employing polymeric fibers. The design workspace for depositing fibers disclosed herein is dependent upon processing parameters of rotational/linear translational speeds and material properties of solution rheologies. Techniques for fabrication of multilayer fiber arrays, for fabrication of cell growth scaffolds and for attachment of particles to the fiber arrays are also disclosed.
摘要翻译：本文提供了用于制造聚合物纤维的高度排列的阵列的装置和系统，其具有范围在几百毫米长度的小于50nm至微米的特征参数。本文公开的方法使用（例如）微量移液管将以对准纤维的形式收集的聚合物溶液输送到旋转和线性平移的基底上。该方法将聚合物纤维沉积在具有精确控制的球形表面和间隙表面上，从而为使用聚合物纤维的各种应用预示了新的机会。本文公开的用于沉积纤维的设计工作区取决于旋转/线性平移速度和溶液流变学的材料性质的处理参数。还公开了用于制造多孔纤维阵列，用于制造细胞生长支架和用于将颗粒附着到纤维阵列的技术。

84. 发明申请

US20090160082A1 Multistage draw with relaxation step 有权
标题翻译：多步绘制放松步骤
公开(公告)号：US20090160082A1
公开(公告)日：2009-06-25
申请号：US12004330
申请日：2007-12-19
申请人： Mark H. Headinger , Edgar N. Rudisill , David W. Luckey
发明人： Mark H. Headinger , Edgar N. Rudisill , David W. Luckey
IPC分类号： D01F6/00
CPC分类号： D01D5/04 , D01D5/12 , D01D11/00 , D01F6/605
摘要： The invention relates to a continuous dry spinning process for preparing a fiber from a polymer solution having concentrations of polymer, salt, solvent and water. After the fiber is extruded and quenched, the fiber is placed in contact with a conditioning solution comprising concentrations of solvent, salt, and water. The conditioning solution acts upon the fiber to plasticize the fiber prior to being drawn. The conditioning solution has concentrations of solvent, salt, and water so that the fiber is plasticized to the extent necessary for drawing but does not plasticize the fiber to such an extent as to re-dissolve the fiber into a polymeric solution. A heat-treated fiber manufactured from this process has improved shrinkage and can be colored to darker shades.
摘要翻译：本发明涉及一种从具有聚合物，盐，溶剂和水的浓度的聚合物溶液制备纤维的连续干法纺丝方法。纤维被挤出和淬火后，将纤维置于与包含溶剂，盐和水的浓度的调理溶液接触。调理溶液作用于纤维，以在拉伸之前使纤维增塑。调理溶液具有溶剂，盐和水的浓度，使得纤维被塑化到拉伸所需的程度，但是不会将纤维增塑到使纤维再溶解成聚合物溶液的程度。由该方法制造的经热处理的纤维具有改善的收缩率并且可以着色到较暗的色调。

85. 发明申请

US20090160081A1 Rapid plasticization of quenched yarns 有权
标题翻译：淬火丝的快速增塑
公开(公告)号：US20090160081A1
公开(公告)日：2009-06-25
申请号：US12004435
申请日：2007-12-19
申请人： Mark H. Headinger , Edgar N. Rudisill , David W. Luckey
发明人： Mark H. Headinger , Edgar N. Rudisill , David W. Luckey
IPC分类号： D01F6/54
CPC分类号： D01D5/04 , D01D5/12 , D01F6/605 , D01F11/08
摘要： The invention relates to a continuous dry spinning process for preparing a fiber from a polymer solution having concentrations of polymer, salt, solvent and water. After the fiber is extruded and quenched, the fiber is placed in contact with a conditioning solution comprising concentrations of solvent, salt, and water. The conditioning solution acts upon the fiber to plasticize the fiber prior to being drawn. The conditioning solution has concentrations of solvent, salt, and water so that the fiber is plasticized to the extent necessary for drawing but does not plasticize the fiber to such an extent as to re-dissolve the fiber into a polymeric solution. A heat-treated fiber manufactured from this process has improved shrinkage and can be colored to darker shades.
摘要翻译：本发明涉及一种从具有聚合物，盐，溶剂和水的浓度的聚合物溶液制备纤维的连续干法纺丝方法。纤维被挤出和淬火后，将纤维置于与包含溶剂，盐和水的浓度的调理溶液接触。调理溶液作用于纤维，以在拉伸之前使纤维增塑。调理溶液具有溶剂，盐和水的浓度，使得纤维被塑化到拉伸所需的程度，但是不会将纤维增塑到使纤维再溶解成聚合物溶液的程度。由该方法制造的经热处理的纤维具有改善的收缩率并且可以着色到较暗的色调。

86. 发明申请

US20090160080A1 High-speed meta-aramid fiber production 有权
标题翻译：高速间位芳纶纤维生产
公开(公告)号：US20090160080A1
公开(公告)日：2009-06-25
申请号：US12004331
申请日：2007-12-19
申请人： Mark H. Headinger , Edgar N. Rudisill , David W. Luckey
发明人： Mark H. Headinger , Edgar N. Rudisill , David W. Luckey
IPC分类号： D01F6/54
CPC分类号： D01D5/04 , D01F6/605
摘要： The invention relates to a continuous dry spinning process for preparing a fiber from a polymer solution having concentrations of polymer, salt, solvent and water. After the fiber is extruded and quenched, the fiber is placed in contact with a conditioning solution comprising concentrations of solvent, salt, and water. The conditioning solution acts upon the fiber to plasticize the fiber prior to being drawn. The conditioning solution has concentrations of solvent, salt, and water so that the fiber is plasticized to the extent necessary for drawing but does not plasticize the fiber to such an extent as to re-dissolve the fiber into a polymeric solution. A heat-treated fiber manufactured from this process has improved shrinkage and can be colored to darker shades.
摘要翻译：本发明涉及一种从具有聚合物，盐，溶剂和水的浓度的聚合物溶液制备纤维的连续干法纺丝方法。纤维被挤出和淬火后，将纤维置于与包含溶剂，盐和水的浓度的调理溶液接触。调理溶液作用于纤维，以在拉伸之前使纤维增塑。调理溶液具有溶剂，盐和水的浓度，使得纤维被塑化到拉伸所需的程度，但是不会将纤维增塑到使纤维再溶解成聚合物溶液的程度。由该方法制造的经热处理的纤维具有改善的收缩率并且可以着色到较暗的色调。

87. 发明申请

US20090072498A1 ALUMINA-SILICA-BASED FIBER, CERAMIC FIBER, CERAMIC FIBER COMPLEX, RETAINING SEAL MATERIAL, PRODUCTION METHOD THEREOF, AND ALUMINA FIBER COMPLEX PRODUCTION METHOD 有权
公开(公告)号：US20090072498A1
公开(公告)日：2009-03-19
申请号：US12269949
申请日：2008-11-13
申请人： Kazutomo TANAHASHI , Masakage DOUSHITA , Hidetomo TAKAHASHI
发明人： Kazutomo TANAHASHI , Masakage DOUSHITA , Hidetomo TAKAHASHI
IPC分类号： F16J15/10
CPC分类号： C04B35/62245 , B82Y30/00 , C04B35/117 , C04B35/803 , C04B2235/422 , C04B2235/526 , C04B2235/5264 , C04B2235/5268 , C04B2235/5284 , C04B2235/656 , C04B2235/6567 , C04B2235/658 , C04B2235/80 , C04B2235/96 , C04B2235/9661 , D01D5/04 , D01D5/253 , D01F9/10 , F01N3/2853 , F01N3/2864 , F01N2330/06 , F01N2330/14 , F01N2350/04 , Y10T428/249928
摘要： A manufacturing method by which alumina-silica based fibers excellent in mechanical strength can be readily and securely obtained. The method obtains precursor fibers as a material by using an alumina-silica based fiber spinning stock solution for use in an inorganic salt method. Next, the precursor fibers are heated under an environment which makes it difficult to carry out an oxidizing reaction on the carbon component contained in the precursor fibers. Thus, the precursor fibers are sintered to obtain alumina-silica based fibers.

88. 发明申请

US20050283959A1 Cellulose acetate tow and method of making same 有权
公开(公告)号：US20050283959A1
公开(公告)日：2005-12-29
申请号：US10877947
申请日：2004-06-25
申请人： Philip Caenen , Gary Ellison , David Kutscher , Williams Sanderson , Mark Scarborough , Donald Stilwell
发明人： Philip Caenen , Gary Ellison , David Kutscher , Williams Sanderson , Mark Scarborough , Donald Stilwell
IPC分类号： D01D5/04 , D01D5/12 , D02G1/12
CPC分类号： D02G1/12 , D01D5/04
摘要： An apparatus and process for making a cigarette tow comprising: means for spinning a dope comprising a solution of cellulose acetate and solvent; means for taking-up the as-spun cellulose acetate filaments; means for lubricating the cellulose acetate filaments; means for forming a tow from the cellulose acetate filaments; means for crimping the tow, the means for crimping comprising a stuffer box crimper comprising a pair of nip rollers adapted to engage the tow, a pair of cheek plates juxtaposed to the pair of nip rollers adapted to keep the tow between the pair of nip rollers, a pair of doctor blades adjacent to an exit end of said pair of nip rollers, and a stuffer box having a stuffer channel adjacent the pair of doctor blades adapted to receive the tow into the channel from the pair of nip rollers, a flapper located at a distal end of the channel adapted to bearingly engage the tow; means for drying the crimped tow; and means for baling the dried crimped tow. The apparatus and process further comprises at least two of the following: A. wherein the means for crimping further comprising one roller of the pair of nip rollers being adapted to induce crimp into the tow; B. wherein the means for crimping further comprising one roller of the pair of nip rollers being made of a solid ceramic material; C. wherein the means for crimping further comprising a pair of tow edge lubricators adapted to lubricate lateral edges of the tow immediately prior to contact with the pair of nip rollers and being ahead of and in contact with the pair of cheek plates; D. wherein the means for crimping further comprising a steam injector being in communication with the channel; E. further comprising a means for plasticizing the tow being located after means for forming the tow and before the means for crimping the tow; F. wherein means for lubricating the filaments further comprises a finish comprising an emulsion of 62.0 to 65.0 weight percent of mineral oil; 27.0 to 28.0 weight percent of emulsifiers, the emulsifiers being a mixture of 50.0 to 52.0 weight percent sorbitan monolaurate, and 48.0 to 50.0 weight percent POE (20) sorbitan monolaurate; and the balance being water.

89. 发明授权

US06887409B2 Method and device for the production of cellulose fibers and cellulose filament yarns 失效
标题翻译：用于生产纤维素纤维和纤维素长丝纱线的方法和装置
公开(公告)号：US06887409B2
公开(公告)日：2005-05-03
申请号：US10220870
申请日：2001-03-06
申请人： Birgit Kosan , Christoph Michels
发明人： Birgit Kosan , Christoph Michels
IPC分类号： D01D5/04 , D01F2/00 , B29C47/34 , B29C47/12 , B29C55/00 , B29D7/00
CPC分类号： D01F2/00 , D01D5/04
摘要： A method for the production of cellulose fibers or filaments from cell material, by the dry-wet extrusion method with aqueous amine oxides, in particular, N-methylmorpholine-N-oxide as solve is described comprising the following steps: a) dispersion of a cell material, or a cell material mixture with a cuoxam DP from 250-3000, in aqueous amine oxide, b) transformation of the obtained dispersion, by water evaporation with shear, at elevated temperature, into a homogeneous solution with a zero shear viscosity of 600 to 6000 Pa·s and a relaxation time of 0.3 to 50 seconds all at 85° C., c) feeding the solution to a spinning jet, previous to which it is passed through flow chamber prior the jet(s), in which the retention time at the spinning temperature, d) forming the solution into at least one capillary in each spinning jet, drawing the capillary(ies) from each jet through anon-precipitating medium and then precipitating the cellulose fibers on drawing through a precipitating bath and e) at the end of the precipitating bath section drawing off the fibers by deflecting the precipitation flow. In stage d) the capillary bundle(s) are treated with a gas flow, just before the entry thereof into the precipitating bath, at an angle α to the capillary flow, wherein 45°
摘要翻译：描述了从细胞材料制备纤维素纤维或长丝的方法，通过干法湿法挤出法用含氧化胺水溶液，特别是N-甲基吗啉-N-氧化物作为解决方案，包括以下步骤：a）细胞材料或具有250-3000的cuoxam DP的细胞材料混合物，在氧化胺水溶液中，b）通过在高温下用剪切水蒸发将所得分散体转化成具有零剪切粘度的均匀溶液 600至6000Pa.s，并且在85℃下均为0.3至50秒的松弛时间，c）将溶液送入纺丝喷嘴，之前在喷射流体之前通过流动室，其中在纺丝温度下的保留时间，d）在每个纺丝射流中将溶液形成至少一个毛细管，从每个喷射流中抽出毛细管通过anon-沉淀介质，然后通过沉淀浴沉淀纤维素纤维， e ）在沉淀浴段的末端通过偏转沉淀流而拉出纤维。在阶段d），毛细管束在其进入沉淀浴之前用气流以与毛细管流的角度α进行处理，其中45°<90°。

90. 发明授权

US5445785A Method of preparing a nonwoven web of poly(vinyl alcohol) fibers 失效
标题翻译：制备聚（乙烯醇）纤维的非织造网的方法
公开(公告)号：US5445785A
公开(公告)日：1995-08-29
申请号：US172513
申请日：1993-12-22
申请人： Hannong Rhim
发明人： Hannong Rhim
IPC分类号： A61F13/53 , A61F13/15 , A61F13/20 , A61F13/49 , D01F6/14 , D04H1/42 , D04H1/56 , D04H3/03 , D04H3/16 , D01D5/04
CPC分类号： D04H3/16 , D01D5/04 , D01D5/14 , D01F6/14 , D04H1/56
摘要： A method of preparing a nonwoven web of poly(vinyl alcohol) fibers which involves the steps of (1) preparing an aqueous polymer solution of a defined poly(vinyl alcohol); (2) extruding the resulting polymer solution under defined conditions through a die having a plurality of orifices to form a plurality of threadlines; (3) attenuating the resulting threadlines with a defined primary gaseous source to form fibers under conditions of controlled macro scale turbulence and under conditions sufficient to permit the viscosity of each threadline, as it leaves a die orifice and for a distance of no more than about 8 cm, to incrementally increase with increasing distance from the die, while substantially maintaining uniformity of viscosity in the radial direction, at a rate which is sufficient to provide fibers having the desired attenuation and mean fiber diameter without significant fiber breakage; (4) drying the attenuated threadlines with a defined secondary gaseous source; and (5) depositing the resulting fibers randomly on a moving foraminous surface to form a substantially uniform web, the moving foraminous surface being from about 10 to about 100 cm from the opening from which the last gaseous source to contact the threadlines emerges, which fibers have a mean fiber diameter in the range of from about 0.1 to about 30 .mu.m and are substantially free of shot, with the attenuating and drying steps being carried out under conditions of controlled macro scale turbulence.
摘要翻译：一种制备聚（乙烯醇）纤维的非织造纤维网的方法，其包括以下步骤：（1）制备定义的聚（乙烯醇）的聚合物水溶液; （2）在限定的条件下通过具有多个孔口的模头挤出所得的聚合物溶液以形成多根线; （3）用限定的主要气体源使得到的丝线衰减，以在受控的大规模湍流的条件下和在足以允许每个丝线的粘度的条件下形成纤维，因为它离开模口并且距离不大于约 8厘米，随着与模具的距离的增加而逐渐增加，同时基本上保持径向粘度的均匀性，其速率足以提供具有期望的衰减和平均纤维直径的纤维而没有显着的纤维断裂; （4）用限定的二次气源干燥衰减的丝线; 和（5）将所得纤维随机地沉积在移动的多孔表面上以形成基本上均匀的网状物，所述移动多孔表面距离最后气态源接触丝线的开口出现约10至约100cm，哪个纤维平均纤维直径在约0.1至约30μm的范围内，并且基本上没有喷射，衰减和干燥步骤在受控的大规模湍流的条件下进行。

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