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81. 发明授权

US09540342B2 Processes for the preparation of pesticidal compounds 有权
公开(公告)号：US09540342B2
公开(公告)日：2017-01-10
申请号：US14989295
申请日：2016-01-06
申请人： Dow AgroSciences LLC
发明人： Qiang Yang , Beth Lorsbach , Gregory Whiteker , Gary Roth , Carl DeAmicis , Thomas Clark , Kaitlyn Gray , Belgin Canturk , Elisabeth J. Kane , Yu Zhang , Joseck M. Muhuhi
IPC分类号： C07D401/04 , C07D231/40 , A01N43/56 , C07C321/14 , C07C321/16 , C07D231/38
CPC分类号： C07D231/38 , A01N43/56 , C07C321/14 , C07C321/16 , C07C2601/02 , C07D231/40 , C07D401/04
摘要： The present application provides processes for making pesticidal compounds and compounds useful both as pesticides and in the making of pesticidal compounds.

82. 发明申请

US20160362363A1 A PROCESS FOR THE REMOVAL OF SODIUM FROM DI-SULFIDE OIL 有权
标题翻译：从脱硫油中去除钠的方法
公开(公告)号：US20160362363A1
公开(公告)日：2016-12-15
申请号：US15121535
申请日：2015-03-13
申请人： RELLANCE INDUSTRIES LIMITED
发明人： Biswajit Shown , Nagarathinam Shenbaga Murthy , Asit Kumar Das , Swapan Ghosh , Bidhayak Das , Rajeshwer Dongara , Anirban Ray , Chirag Dalpatbhai Panseriya , Udayan Sivathanu Ramalakshmi , Atul Kathiria
IPC分类号： C07C319/30
CPC分类号： C07C319/30 , C07C321/04 , C07C321/14
摘要： In the present disclosure there is provided a process for obtaining di-sulfide oil having sodium level below 0.1 ppm wherein a stream comprising di-sulfide oil having sodium level 1 ppm, collected as a waste stream from LPG desulfurization unit, is passed through an alumina bed packed in a column at a pre-determined liquid hourly space velocity (LHSV) and at pre-determined temperature to obtain a treated stream comprising di-sulfide oil having sodium level below 0.1 ppm.
摘要翻译：在本公开内容中，提供了一种获得钠含量低于0.1ppm的二硫化物油的方法，其中将含有1ppm钠含量的二硫化物物流作为来自LPG脱硫装置的废物流的物流通过氧化铝床以预定的液体时空速（LHSV）和预定温度填充在柱中，以获得包含钠水平低于0.1ppm的二硫化物油的处理流。

83. 发明授权

US09505714B2 Conversion of alkanes to organoseleniums and organotelluriums 有权
标题翻译：烷烃转化为有机硒和有机碲
公开(公告)号：US09505714B2
公开(公告)日：2016-11-29
申请号：US14910275
申请日：2014-08-06
申请人： The Scripps Research Institute
发明人： Roy A. Periana , Michael M. Konnick , Brian G. Hashiguchi
IPC分类号： C07C45/00 , C07C395/00 , C07C1/00 , C07C209/00 , C07C319/00 , C07F7/00 , C07C391/00 , C07C1/32 , C07C319/02 , C07C319/14 , C07C17/093 , C07B39/00 , C07B41/06 , C07B43/04 , C07B45/00 , C07B47/00 , C07C209/22 , C07C231/10 , C07F7/22 , C07F9/50
CPC分类号： C07C395/00 , C07B39/00 , C07B41/06 , C07B43/04 , C07B45/00 , C07B47/00 , C07C1/321 , C07C17/093 , C07C45/00 , C07C209/22 , C07C231/10 , C07C319/02 , C07C319/14 , C07C391/00 , C07F7/2208 , C07F9/5004 , C07C321/04 , C07C321/14 , C07C11/02
摘要： The invention provides processes and materials for the efficient and costeffective functionalization of alkanes and heteroalkanes, comprising contacting the alkane or heteroalkane and a soft oxidizing electrophile comprising Se(VI) or Te(VI), in an acidic medium, optionally further comprising an aprotic medium, which can be carried out at a temperature of less than 300 C. Isolation of the alkylselenium or alkyltellurium intermediate allows the subsequent conversion to products not necessarily compatible with the initial reaction conditions, such as amines, stannanes, organosulfur compounds, acyls, halocarbons, and olefins.
摘要翻译：本发明提供用于烷烃和杂烷烃的有效和成本有效的功能化的方法和材料，包括在酸性介质中使烷烃或杂烷烃与包含Se（VI）或Te（VI）的软氧化亲电试剂接触，任选地还包含非质子介质可以在小于300℃的温度下进行。烷基硒或烷基碲中间体的分离允许随后转化成与初始反应条件不一致的产物，例如胺，锡烷，有机硫化合物，酰基，卤代烃，和烯烃。

84. 发明申请

US20160229799A1 PROCESS FOR OBTAINING METHIONINE 有权
标题翻译：获得甲磺酸的方法
公开(公告)号：US20160229799A1
公开(公告)日：2016-08-11
申请号：US15021541
申请日：2014-09-10
申请人： Stefan REICHERT , Harald JAKOB , Hans Joachim HASSELBACH , Martin KÖRFER
发明人： Stefan REICHERT , Harald JAKOB , Hans Joachim HASSELBACH , Martin KOERFER
IPC分类号： C07C321/14
CPC分类号： C07C321/14 , C07B2200/13 , C07C319/20 , C07C319/26 , C07C319/28 , C07C323/58
摘要： The invention relates to a method for crystallizing D,L-methionine from aqueous solutions and/or suspensions containing D,L-methionine and D,L-methionine ammonium salts, having a Met content of 70-180 g/kg, an NH4+ content of 1-5 g/kg, in the presence of a crystallization additive, which comprises a nonionic or anionic surfactant or a mixture of various nonionic or anionic surfactants, in which the temperature of the solution and/or suspension is lowered directly or stepwise from T1=85-110° C. to T2=30-50° C., so that D,L-methionine precipitates as a solid.
摘要翻译：本发明涉及从含有D，L-甲硫氨酸和D，L-甲硫氨酸铵盐的水溶液和/或悬浮液中结晶D，L-甲硫氨酸的方法，其Met含量为70-180g / kg，NH4 +含量在结晶添加剂存在下，其包含非离子或阴离子表面活性剂或各种非离子或阴离子表面活性剂的混合物，其中溶液和/或悬浮液的温度直接或逐步从 T1 = 85-110℃至T2 = 30-50℃，因此D，L-甲硫氨酸作为固体沉淀。

85. 发明申请

US20160176812A1 CONVERSION OF ALKANES TO ORGANOSELENIUMS AND ORGANOTELLURIUMS 有权
标题翻译：碱向有机物和有机物的转化
公开(公告)号：US20160176812A1
公开(公告)日：2016-06-23
申请号：US14910275
申请日：2014-08-06
申请人： Roy A. PERIANA , Michael M. KONNICK , Brian G. HASHIGUCHI , THE SCRIPPS RESEARCH INSTITUTE
发明人： Roy A. PERIANA , Michael M. KONNICK , Brian G. HASHIGUCHI
IPC分类号： C07C395/00 , C07C209/22 , C07F7/22 , C07C319/02 , C07C231/10 , C07F9/50 , C07C45/00 , C07C17/093 , C07B47/00 , C07B45/00 , C07B43/04 , C07B41/06 , C07B39/00 , C07C1/32 , C07C391/00
CPC分类号： C07C395/00 , C07B39/00 , C07B41/06 , C07B43/04 , C07B45/00 , C07B47/00 , C07C1/321 , C07C17/093 , C07C45/00 , C07C209/22 , C07C231/10 , C07C319/02 , C07C319/14 , C07C391/00 , C07F7/2208 , C07F9/5004 , C07C321/04 , C07C321/14 , C07C11/02
摘要： The invention provides processes and materials for the efficient and costeffective functionalization of alkanes and heteroalkanes, comprising contacting the alkane or heteroalkane and a soft oxidizing electrophile comprising Se(VI) or Te(VI), in an acidic medium, optionally further comprising an aprotic medium, which can be carried out at a temperature of less than 300 C. Isolation of the alkylselenium or alkyltellurium intermediate allows the subsequent conversion to products not necessarily compatible with the initial reaction conditions, such as amines, stannanes, organosulfur compounds, acyls, halocarbons, and olefins.
摘要翻译：本发明提供用于烷烃和杂烷烃的有效和成本有效的功能化的方法和材料，包括在酸性介质中使烷烃或杂烷烃与包含Se（VI）或Te（VI）的软氧化亲电试剂接触，任选地还包含非质子介质可以在小于300℃的温度下进行。烷基硒或烷基碲中间体的分离允许随后转化成与初始反应条件不一致的产物，例如胺，锡烷，有机硫化合物，酰基，卤代烃，和烯烃。

86. 发明申请

US20160152594A1 PROCESSES FOR THE PREPARATION OF PESTICIDAL COMPOUNDS 有权
公开(公告)号：US20160152594A1
公开(公告)日：2016-06-02
申请号：US14989295
申请日：2016-01-06
申请人： Dow AgroSciences LLC
发明人： Qiang YANG , Beth LORSBACH , Gregory WHITEKER , Gary ROTH , Carl DeAMICIS , Thomas CLARK , Kaitlyn GRAY , Belgin CANTURK , Elisabeth J. KANE , Yu ZHANG , Joseck M. MUHUHI
IPC分类号： C07D401/04 , C07C321/16 , C07D231/38 , C07C321/14 , C07D231/40 , A01N43/56
CPC分类号： C07D231/38 , A01N43/56 , C07C321/14 , C07C321/16 , C07C2601/02 , C07D231/40 , C07D401/04
摘要： The present application provides processes for making pesticidal compounds and compounds useful both as pesticides and in the making of pesticidal compounds.

87. 发明申请

US20160022713A1 Compositions and Products for Infectious or Inflammatory Diseases or Conditions 审中-公开
标题翻译：感染或炎症疾病或病症的组成和产品
公开(公告)号：US20160022713A1
公开(公告)日：2016-01-28
申请号：US14775952
申请日：2014-03-13
申请人： Huiru WANG
发明人： Huiru WANG
IPC分类号： A61K31/7008 , C07C321/14 , A23K1/16 , A61K45/06 , A23L1/305 , A23L1/30 , C07H15/12 , A61K31/198
CPC分类号： A61K31/7008 , A23K20/142 , A23K20/147 , A23L33/10 , A23L33/17 , A23L33/175 , A23V2002/00 , A61K9/0019 , A61K9/0043 , A61K9/0095 , A61K9/08 , A61K9/10 , A61K9/107 , A61K31/198 , A61K45/06 , A61K47/02 , C07C321/14 , C07H15/12 , A61K2300/00
摘要： Composition and methods for treating infectious and inflammatory diseases using saccharide based products and therapies. Products can be implemented as a nutritional supplement, a food, a feed, a food additive, a feed additive, a therapeutic product, a rehydration salt, or a rehydration solution. The present disclosure relates generally to the fields of compositions and products containing the compositions, and the use of the compositions or the products for preventing and/or treating infectious or inflammatory diseases or conditions in particular gastrointestinal and respiratory diseases (diarrhea and influenza infections) or inflammatory.
摘要翻译：使用糖基产品和疗法治疗感染性和炎症性疾病的组合物和方法。产品可以实现为营养补充剂，食品，饲料，食品添加剂，饲料添加剂，治疗产品，补液盐或补液。本公开一般涉及包含组合物的组合物和产品的领域，以及组合物或产品用于预防和/或治疗感染性或炎性疾病或病症，特别是胃肠和呼吸道疾病（腹泻和流感感染）或炎症。

88. 发明申请

US20160017085A1 METHOD FOR PRODUCING POLYTHIOL COMPOUND, POLYMERIZABLE COMPOSITION FOR OPTICAL MATERIAL, AND USES THEREOF 有权
标题翻译：用于生产聚合物的方法，用于光学材料的可聚合组合物及其用途
公开(公告)号：US20160017085A1
公开(公告)日：2016-01-21
申请号：US14871479
申请日：2015-09-30
申请人： MITSUI CHEMICALS, INC
发明人： Masaru KAWAGUCHI , Takeshi NISHIMURA
IPC分类号： C08G18/38 , G02B1/04 , C07C335/32 , C07C319/20 , C08G18/76 , C07C319/14
CPC分类号： C08G18/3876 , C07C319/08 , C07C319/14 , C07C319/20 , C07C335/32 , C07C381/00 , C08G18/7642 , G02B1/041 , C08L75/04 , C08L81/00 , C07C323/12 , C07C321/14
摘要： Provided is a method for producing a molded product comprising preparing a polymerizable composition for optical materials and curing the polymerizable composition for optical materials to produce the molded product. The preparation of the polymerizable composition comprises preparing a polythiol compound containing, as a main component, one kind or two or more kinds selected from a defined group of compounds, and preparing the polymerizable composition from the polythiol compound. The preparation of the polythiol compound comprises reacting 2-mercaptoethanol with a defined epihalohydrin compound to obtain a defined compound, reacting the defined compound with sodium sulfide to obtain a defined polyalcohol compound, reacting the polyalcohol compound with thiourea in the presence of hydrogen chloride to obtain an isothiuronium salt, adding aqueous ammonia to a reaction solution containing the isothiuronium salt thereby hydrolyzing the isothiuronium salt to obtain the polythiol compound and purifying the polythiol compound with hydrochloric acid.
摘要翻译：本发明提供一种成型品的制造方法，其包括制备光学材料用聚合性组合物，使光学材料用聚合性组合物固化，制造成型品。可聚合组合物的制备包括制备含有选自定义的一组化合物中的一种或两种以上的作为主要成分的多硫醇化合物，并由多硫醇化合物制备可聚合组合物。多硫醇化合物的制备包括使2-巯基乙醇与定义的表卤代醇化合物反应以获得规定的化合物，使定义的化合物与硫化钠反应，得到定义的多元醇化合物，使多元醇化合物与硫脲在氯化氢存在下反应，得到异硫脲鎓盐，向含有异硫脲鎓盐的反应溶液中加入氨水，从而水解异硫脲鎓盐，得到多硫醇化合物，并用盐酸纯化多硫醇化合物。

89. 发明申请

US20150336929A1 PROCESSES FOR THE PREPARATION OF PESTICIDAL COMPOUNDS 有权
公开(公告)号：US20150336929A1
公开(公告)日：2015-11-26
申请号：US14816600
申请日：2015-08-03
申请人： Dow AgroSciences LLC
发明人： Qiang YANG , Beth LORSBACH , Ronald ROSS, JR. , Kaitlyn GRAY , Yu ZHANG , Gary ROTH
IPC分类号： C07D401/04 , C07C319/20 , C07C319/18 , A01N43/56 , C07D231/40
CPC分类号： C07D401/04 , A01N43/56 , C07C319/18 , C07C319/20 , C07D231/38 , C07D231/40 , C07C321/14
摘要： The present application provides processes for making pesticidal compounds and compounds useful both as pesticides and in the making of pesticidal compounds.

90. 发明申请

US20150133692A1 METHOD FOR PRODUCING POLYTHIOL COMPOUND, POLYMERIZABLE COMPOSITION FOR OPTICAL MATERIAL, AND USES THEREOF 有权
标题翻译：用于生产聚合物的方法，用于光学材料的可聚合组合物及其用途
公开(公告)号：US20150133692A1
公开(公告)日：2015-05-14
申请号：US14405222
申请日：2013-02-28
申请人： MITSUI CHEMICALS, INC.
发明人： Masaru Kawaguchi , Takeshi Nishimura
IPC分类号： C07C319/08 , C07C381/00
CPC分类号： C08G18/3876 , C07C319/08 , C07C319/14 , C07C319/20 , C07C335/32 , C07C381/00 , C08G18/7642 , G02B1/041 , C08L75/04 , C08L81/00 , C07C323/12 , C07C321/14
摘要： Provided is a method for producing a polythiol compound, comprising: a step for reacting 2-mercaptoethanol with a defined epihalohydrin compound at a temperature of 10° C. to 50° C. to obtain a defined polyalcohol compound; a step for reacting the polyalcohol compound thus obtained with thiourea in the presence of hydrogen chloride to obtain an isothiuronium salt; a step for adding, while maintaining a reaction solution containing the isothiuronium salt thus obtained at a temperature of 15° C. to 60° C., aqueous ammonia to the reaction solution within 80 minutes, thereby hydrolyzing the isothiuronium salt to obtain a defined polythiol compound; and a step for adding hydrochloric acid which is a concentration of 25% to 36% to the solution containing the polythiol compound thus obtained, washing the solution at a temperature of 10° C. to 50° C. to purify the polythiol compound.
摘要翻译：本发明提供一种多硫醇化合物的制造方法，其特征在于，包括：在10℃〜50℃的温度下使2-巯基乙醇与定义的表卤代醇化合物反应的步骤，得到规定的多元醇化合物; 将由此获得的多元醇化合物与硫脲在氯化氢存在下反应得到异硫脲鎓盐的步骤; 将在15℃至60℃的温度下将含有异硫脲鎓盐的反应溶液保持在反应溶液中的反应溶液在80分钟内加入到反应溶液中，从而水解异硫脲鎓盐以获得定义的多硫醇复合; 向含有所述多硫醇化合物的溶液中加入浓度为25％〜36％的盐酸的步骤，在10℃〜50℃的温度下洗涤，纯化多硫醇化合物。

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