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81. 发明授权

US07964744B2 Method for producing a ruthenium complex 有权
标题翻译：钌络合物的制造方法
公开(公告)号：US07964744B2
公开(公告)日：2011-06-21
申请号：US12540794
申请日：2009-08-13
申请人： Hideki Nara , Noboru Sayo , Takahiro Fujiwara
发明人： Hideki Nara , Noboru Sayo , Takahiro Fujiwara
IPC分类号： C07F15/00
CPC分类号： C07F15/0053
摘要： Provided is a method for producing a ruthenium complex comprises the step of reacting a ruthenium compound represented by general formula (1): [RuX(L)(PP)]X (1), wherein Ru represents a ruthenium atom; X represents a halogen atom; L represents an arene; and PP represents an optically active bisphosphine, with a carboxylate salt represented by general formula (2): R1CO2M (2), wherein M represents a monovalent cation; and R1 represents a group selected from the group consisting of alkyl groups, haloalkyl groups, phenyl groups optionally having a substituent(s), 1-aminoalkyl groups and 1-amino-1-phenylalkyl groups, to produce a ruthenium complex represented by general formula (3): Ru(OCOR1)2(PP) (3), wherein R1 represents the group selected from the group consisting of alkyl groups, haloalkyl groups, phenyl groups optionally having a substituent(s), 1-aminoalkyl groups and 1-amino-1-phenylalkyl groups; and PP represents the optically active bisphosphine.
摘要翻译：提供一种制备钌络合物的方法，包括使通式（1）表示的钌化合物：[RuX（L）（PP）] X（1），其中Ru表示钌原子; X表示卤原子; L代表芳烃; 和PP代表光学活性双膦，与通式（2）表示的羧酸盐：R1CO2M（2），其中M表示一价阳离子; 并且R 1表示选自烷基，卤代烷基，任选具有取代基的苯基，1-氨基烷基和1-氨基-1-苯基烷基的基团，以制备由通式（3）：Ru（OCOR1）2（PP）（3），其中R1表示选自烷基，卤代烷基，任选具有取代基的苯基，1-氨基烷基和1- 氨基-1-苯基烷基; PP代表光学活性双膦。

82. 发明授权

US07964637B2 Process for producing optically active theaspirane 失效
标题翻译：光学活性硅烷的制备方法
公开(公告)号：US07964637B2
公开(公告)日：2011-06-21
申请号：US11992067
申请日：2006-09-08
申请人： Makoto Harada , Hiroyuki Matsuda , Kenya Ishida , Yuichiro Yamazaki
发明人： Makoto Harada , Hiroyuki Matsuda , Kenya Ishida , Yuichiro Yamazaki
IPC分类号： A61K31/335 , C07D307/94
CPC分类号： C12P17/04 , A23L2/56 , A23L27/2052 , A61K8/4973 , A61Q19/00 , C07B53/00 , C07D307/94 , C11B9/0076 , C12P41/005
摘要： A simplified production method of stereoisomer of theaspiran having high optical purity has been desired. An alcohol compound having a specific skeleton is enantioselectively esterified with an enzyme, or an ester compound having a specific skeleton is enantioselectively hydrolyzed with an enzyme. The resultant optically active ester or optically active alcohol is used. Thus, optically active theaspiran having a desired configuration and having a high optical purity is obtained in a satisfactory yield.
摘要翻译：期望具有高光学纯度的阿司匹兰的立体异构体的简化制备方法。具有特定骨架的醇化合物用酶对映体选择性酯化，或者具有特定骨架的酯化合物用酶对映体选择性水解。使用所得光学活性酯或光学活性醇。因此，以令人满意的产率获得光学活性的具有所需构型并具有高光学纯度的阿司匹林。

83. 发明申请

US20110105773A1 PRODUCTION METHOD OF (2E,6Z,8E)-N-ISOBUTYL-2,6,8-DECATRIENAMIDE (SPILANTHOL), AND FOOD OR DRINK, FRAGRANCE OR COSMETIC, OR PHARMACEUTICAL COMPRISING THE SAME 有权
标题翻译：（2E，6Z，8E）-N-ISOBUTYL-2,6,8-癸胺（SPILANTHOL）的生产方法，以及食品或饮料，香料或化妆品，或包含它们的药物
公开(公告)号：US20110105773A1
公开(公告)日：2011-05-05
申请号：US12673633
申请日：2009-01-16
申请人： Shigeru Tanaka , Kenji Yagi , Hideo Ujihara , Kenya Ishida
发明人： Shigeru Tanaka , Kenji Yagi , Hideo Ujihara , Kenya Ishida
IPC分类号： C07C235/28 , C07C231/02 , C07C231/12 , C07C57/66 , C07C43/303
CPC分类号： A61K8/42 , A23G1/32 , A23G3/36 , A23G4/06 , A23L27/202 , A61Q5/00 , A61Q11/00 , A61Q15/00 , C07C43/303 , C07C45/41 , C07C57/66 , C07C231/12 , C07C233/09 , C07C235/28 , C07C309/66 , C12P13/02 , C07C47/21
摘要： A problem as an object of the invention is to provide a production method of spilanthol in a large scale without using expensive reagents. The present invention provides a production method of N-isobutyl-2,6,8-decatrienamide, wherein a column chromatography purification step is not required in all processes.
摘要翻译：作为本发明的目的的一个问题是在不使用昂贵的试剂的情况下大规模地提供大量的生产方法。本发明提供N-异丁基-2,6,8-癸三酰胺的制备方法，其中在所有方法中不需要柱色谱纯化步骤。

84. 发明申请

US20110077309A1 HUMECTANT COMPOSITION 审中-公开
标题翻译：成分组成
公开(公告)号：US20110077309A1
公开(公告)日：2011-03-31
申请号：US12959670
申请日：2010-12-03
申请人： Tetsuya Yamamoto , Kenya Ishida
发明人： Tetsuya Yamamoto , Kenya Ishida
IPC分类号： A61K47/42 , A61K47/10 , A61K47/14 , A61K47/22 , A61K47/36 , A61K47/46 , A61Q5/12 , A61Q19/00 , A61P17/00 , A61K8/33 , A61Q13/00
CPC分类号： A61K8/345 , A61Q5/00 , A61Q5/02 , A61Q5/12 , A61Q13/00 , A61Q19/00 , A61Q19/10
摘要： The present invention relates to a humectant composition containing, as component (A), at least one member selected from a menthol derivative represented by the following formula (1) and p-menthane-3,8-diol: in which R is an alkylene group having 2 to 5 carbon atoms which may be substituted with at least one member selected from the group consisting of a methyl group and a hydroxyl group, and n is an integer of 1 to 3. The humectant composition of the present invention provides an excellent moisture-retention effect.
摘要翻译：本发明涉及作为组分（A）的至少一种选自由下式（1）表示的薄荷醇衍生物和对 - 薄荷烷-3,8-二醇中的至少一种的组合物：其中R是亚烷基具有2至5个碳原子的基团，其可以被选自甲基和羟基中的至少一种取代，n是1至3的整数。本发明的保湿组合物提供优异的保湿效果。

85. 发明授权

US07893296B2 Method for producing an optically active β-amino acid 有权
标题翻译：用于制备光学活性的氨基酸的方法
公开(公告)号：US07893296B2
公开(公告)日：2011-02-22
申请号：US11290440
申请日：2005-12-01
申请人： Kazuhiko Matsumura , Xiaoyong Zhang , Takao Saito
发明人： Kazuhiko Matsumura , Xiaoyong Zhang , Takao Saito
IPC分类号： C07C229/00
CPC分类号： C07C227/16 , C07B2200/07 , C07C227/32 , C07C2601/08 , C07D333/24 , Y02P20/55 , C07C229/08 , C07C229/34 , C07C229/48 , C07C229/22
摘要： Disclosed is a producing method of an optically active β-amino acid useful as intermediate for the production of medicines, agricultural. chemicals and physiologically active substances, by means of a catalytic and asymmetric synthesis method of high performance and a high enantiomeric excess, without requiring additional procedures such as introduction and removal of protecting group and so on. The method includes subjecting an enamine to an asymmetric hydrogenation.
摘要翻译：公开了用作农药生产中间体的光学活性的氨基酸的制备方法。化学品和生理活性物质，通过高性能和高对映异构体过量的催化和不对称合成方法，而不需要额外的方法，如引入和除去保护基等。该方法包括使烯胺进行不对称氢化。

86. 发明申请

US20110009646A1 RUTHENIUM-DIAMINE COMPLEX AND METHODS FOR PRODUCING OPTICALLY ACTIVE COMPOUNDS 有权
标题翻译：罗丹明复合物及其制备光活性化合物的方法
公开(公告)号：US20110009646A1
公开(公告)日：2011-01-13
申请号：US12835626
申请日：2010-07-13
申请人： Taichiro Touge , Hideki Nara
发明人： Taichiro Touge , Hideki Nara
IPC分类号： C07F7/10 , C07C33/38 , C07C33/22 , C07D311/74 , C07C29/143 , C07C209/70
CPC分类号： C07F15/0046 , B01J31/1805 , B01J2231/643 , B01J2531/821 , C07B2200/07 , C07C29/143 , C07C29/145 , C07C309/13 , C07D311/22 , C07C33/18 , C07C33/22
摘要： There are provided a novel ruthenium-diamine complex, and methods for selectively producing an optically active alcohol and an optically active amine, which are important as precursors for the synthesis of medicinal drugs and functional materials, using the ruthenium-diamine complex as a catalyst.A novel ruthenium-diamine complex prepared by introducing a trisubstituted silyl group into an aromatic compound (arene) moiety that is coordinated with a ruthenium complex having an optically active diamine as a ligand, a catalyst for asymmetric reduction formed from the ruthenium-diamine complex, and a method for producing an optically active alcohol or an optically active amine using the catalyst.
摘要翻译：提供了一种新颖的钌 - 二胺配合物，以及使用钌 - 二胺络合物作为催化剂选择性地制备作为药物和功能材料的合成前体的光学活性的醇和光学活性胺的方法。通过将三取代甲硅烷基引入到与具有光学活性二胺作为配体的钌络合物配位的芳族化合物（芳烃）部分中制备的新型钌 - 二胺络合物，由钌 - 二胺络合物形成的不对称还原催化剂，以及使用该催化剂制造光学活性醇或光学活性胺的方法。

87. 发明授权

US07846701B2 Method for preparing optically active compound 失效
标题翻译：光学活性化合物的制备方法
公开(公告)号：US07846701B2
公开(公告)日：2010-12-07
申请号：US11667688
申请日：2005-10-31
申请人： Shigeru Tanaka , Shinya Watanabe , Ken-ichi Yamamoto , Hiroyuki Matsuda
发明人： Shigeru Tanaka , Shinya Watanabe , Ken-ichi Yamamoto , Hiroyuki Matsuda
IPC分类号： C12P7/26
CPC分类号： C12P7/26 , C12P41/003
摘要： According to the present invention, there is provided a method for preparing an optically active compound, characterized in that said method comprises permitting a mixture of optical isomers relative to the carbon atom in the β-position in relation to the carbon atom bound to an esterified hydroxy group of an enol ester to hydrolyse either one optical isomer preferentially in the presence of an enzyme and allowing the carbonyl compound resulting from such hydrolysis to enrich the proportion of its isomer having either one configuration in the β-position in relation to the carbonyl group or allowing the enol ester left non-hydrolyzed to enrich the proportion of its isomer having either one configuration on the carbon atom in the β-position in relation to the carbon atom to which the esterified hydroxyl group bonds.
摘要翻译：根据本发明，提供了一种制备光学活性化合物的方法，其特征在于所述方法包括允许相对于与一个碳原子结合的碳原子相对于碳原子的光学异构体的混合物烯醇酯的酯化羟基在酶的存在下优先水解任一种旋光异构体，并使得由这种水解产生的羰基化合物能够富集其相对于化合物中的任何一种构型的其异构体的比例使烯醇酯残留未水解以富集其相对于与酯化羟基键合的碳原子相关的碳原子上具有一个构型的异构体的比例。

88. 发明申请

US20100280110A1 (3R)-L-MENTHYL 3-HYDROXYBUTYRATE, PROCESS FOR PRODUCING THE SAME, AND SENSATE COMPOSITION COMPRISING THE SAME 失效
标题翻译：（3R）-L-戊烯3-羟基丁酸酯，其制备方法以及含有它们的感官组合物
公开(公告)号：US20100280110A1
公开(公告)日：2010-11-04
申请号：US12766162
申请日：2010-04-23
申请人： Kazuma HOJO , Takashi AIDA , Kenya ISHIDA
发明人： Kazuma HOJO , Takashi AIDA , Kenya ISHIDA
IPC分类号： A61K8/37 , C07C69/675 , A61K31/22 , A61P43/00 , A61Q90/00 , A23L1/226 , A61K8/365 , A61Q19/10 , A61Q13/00 , A61Q5/02
CPC分类号： C11B9/0034 , A23L2/56 , A23L27/203 , A61K8/37 , A61K31/22 , A61K2800/244 , A61Q5/02 , A61Q13/00 , A61Q19/00 , A61Q19/10 , C07B2200/07 , C07C67/31 , C07C69/675 , C07C2601/14
摘要： The present invention provides a cooling component or sensate component which has further strong cooling intensity and is excellent in the persistency or refresh-feeling and cool-feeling, a sensate composition comprising the same, and various products comprising the sensate composition. The present invention relates to, as a cooling component or sensate component, (3R)-1-menthyl 3-hydroxybutyrate represented by the following formula (I):
摘要翻译：本发明提供一种冷却组分或感觉组分，其具有更强的冷却强度，并且具有优异的持久性，刷新感和凉爽感，含有该组合物的感觉组合物和包含感觉组合物的各种产品。本发明涉及作为冷却成分或感官成分的由下式（I）表示的（3R）-1-薄荷基3-羟基丁酸酯：

89. 发明申请

US20100226871A1 HIGH INTENSITY FRAGRANCES 有权
标题翻译：高强度巧克力
公开(公告)号：US20100226871A1
公开(公告)日：2010-09-09
申请号：US12716392
申请日：2010-03-03
申请人： Stuart FRASER , Dominique GINDRE , Jonathan WARR
发明人： Stuart FRASER , Dominique GINDRE , Jonathan WARR
IPC分类号： A61K8/98 , A61Q13/00 , A61K8/18 , A61K8/81 , A61K31/365 , A61Q19/10 , A61Q5/02 , A61Q5/06
CPC分类号： C11B9/0015 , C11B9/00 , C11B9/0019 , C11B9/0034 , C11B9/0061 , C11B9/0076
摘要： The present invention relates to a high intensity fragrance composition for use in a cosmetic, toiletry, personal care, personal cleansing product or adsorbent article, which comprises by weight: a) 75% to 100% of at least 2 fragrance ingredients where each fragrance ingredients must contain only atoms of carbon, hydrogen, oxygen and nitrogen, comprise an ester functional group, an alcohol functional group or an aldehyde functional group, have boiling points between 100° C. and 300° C. at a pressure of 760 mm of mercury, have molecular weights within the range of 70 atomic mass units to 175 atomic mass units, and have ClogP values between 0.00 and 4.00; b) 0 to 25% of an essential oil; and c) 0 to 25% of a fragrance ingredient other than the fragrance ingredients in category a), wherein the sum of a), b) and c) equals 100%.
摘要翻译：本发明涉及一种用于化妆品，化妆品，个人护理，个人清洁产品或吸附制品中的高强度香料组合物，其包含重量：a）75％至100％的至少2种香料成分，其中每种香料成分必须只包含碳，氢，氧和氮的原子，包含酯官能团，醇官能团或醛官能团，沸点在100℃至300℃之间，压力为760毫米汞柱具有70原子质量单位至175原子质量单位范围内的分子量，并且具有0.00和4.00之间的ClogP值; b）0至25％的精油; 和c）除了a）中的香料成分之外的0至25％的香料成分，其中a），b）和c）的总和等于100％。

90. 发明申请

US20100158840A1 DEODORANT COMPOSITION 有权
标题翻译：除臭剂组合物
公开(公告)号：US20100158840A1
公开(公告)日：2010-06-24
申请号：US12293661
申请日：2007-03-22
申请人： Tadahiro Hiramoto , Kenichiro Shiroyama , Hiroyasu Kumamoto
发明人： Tadahiro Hiramoto , Kenichiro Shiroyama , Hiroyasu Kumamoto
IPC分类号： A61K8/66 , A61Q15/00
CPC分类号： A61L9/01 , A61K8/19 , A61K8/20 , A61K8/36 , A61K8/365 , A61K8/368 , A61K8/375 , A61K8/498 , A61K8/602 , A61K8/97 , A61L9/013 , A61Q15/00
摘要： The present invention relates to a deodorant composition containing (a) a polyphenol compound or a plant extract containing a polyphenol compound, (b) a basic substance, and (c) a metal salt. The deodorant composition of the present invention is capable of providing a deodorizing effect in a short period of time when it is applied to a malodor source, is capable of providing an excellent deodorizing activity and is also excellent in the store stability.
摘要翻译：本发明涉及含有（a）多酚化合物或含有多酚化合物的植物提取物，（b）碱性物质和（c）金属盐的除臭剂组合物。本发明的除臭剂组合物能够在施加到恶臭源时在短时间内提供除臭效果，能够提供优异的除臭活性，并且也具有优异的贮存稳定性。

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