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71. 发明授权

US4364845A Concentrated aqueous solutions of sulfo group-containing fluorescent brighteners which are stable on storage 失效
标题翻译：储存稳定的含磺基荧光增白剂的浓缩水溶液
公开(公告)号：US4364845A
公开(公告)日：1982-12-21
申请号：US55417
申请日：1979-07-06
申请人： Werner Fringeli
发明人： Werner Fringeli
IPC分类号： C09B67/44 , D06L3/12 , D21H21/30 , C09K11/06
CPC分类号： D06L3/1264 , D21H21/30
摘要： Concentrated aqueous solutions of sulfo group-containing fluorescent brighteners, which are stable on storage, containing a stilbene fluorescent brightener substituted by sulfo groups and a lactam of the formula ##STR1## in which m is 0 or an integer between 1 and 9, and their use for the fluorescent brightening of high molecular weight organic material.
摘要翻译：含有磺基的荧光增白剂的浓缩水溶液在储存时稳定，含有被磺基取代的芪荧光增白剂和式为“IMAGE”的内酰胺，其中m为0或1至9之间的整数，并且它们用于高分子量有机材料的荧光增白。

72. 发明授权

US4200489A Process for producing sized paper or cardboard with dyes or optical brighteners and epoxide-amine-polyamide reaction products 失效
标题翻译：用染料或荧光增白剂和环氧胺 - 聚酰胺反应产物生产大尺寸纸或纸板的方法
公开(公告)号：US4200489A
公开(公告)日：1980-04-29
申请号：US933688
申请日：1978-08-15
申请人： Hugo Tlach , Klaus-Dieter Leifels , Werner Mischler
发明人： Hugo Tlach , Klaus-Dieter Leifels , Werner Mischler
IPC分类号： D21H17/55 , D21H21/28 , D21H21/30 , D21H3/58
CPC分类号： D21H21/30 , D21H17/55 , D21H21/28
摘要： A process for producing paper or cardboard which is sized in the pulp with epoxide-amine-polyamide reaction products is disclosed.In this process there are added to the fibre suspension(A) at least one water-soluble, anionic, substantive direct dye and/or optical brightener, followed by(B) at least one water-soluble or water-dispersible salt of an epoxide-amine-polyamide reaction product,whereupon the fibre suspension is further processed into paper or into cardboard.
摘要翻译：公开了一种用于生产纸浆或纸板的方法，该纸或纸板在纸浆中具有环氧胺 - 聚酰胺反应产物。在该方法中，向纤维悬浮液（A）中加入至少一种水溶性，阴离子，实质的直接染料和/或荧光增白剂，其后是（B）至少一种环氧化物的水溶性或水分散性盐 - 胺 - 聚酰胺反应产物，于是将纤维悬浮液进一步加工成纸或纸板。

73. 发明授权

US4164500A Pyrazoline compounds 失效
公开(公告)号：US4164500A
公开(公告)日：1979-08-14
申请号：US898629
申请日：1978-04-21
申请人： Manfred Patsch , Albert Hettche
发明人： Manfred Patsch , Albert Hettche
IPC分类号： C07D231/06 , C07D231/12 , D21H21/30
CPC分类号： C07D231/06 , C07D231/12 , D21H21/30
摘要： Pyrazoline compounds of the formula (I): ##STR1## in which EACH OFB.sup.1 to B.sup.5 is hydrogen or C.sub.1 to C.sub.4 alkyl;R.sup.1 is hydrogen, alkyl or hydroxy;R.sup.2, r.sup.3, r.sup.5, r.sup.6 and R.sup.7 independently of one another are hydrogen, chloro, bromo, fluoro, methyl, ethyl, methoxy or ethoxy;R.sup.4 is hydrogen, alkyl, benzyl, phenylethyl or also phenyl optionally bearing chloro, bromo, methyl, ethyl, methoxy, ethoxy, cyano, dialkylamino or SO.sub.3 H as a substituent;X is --O--, --S--, --NR.sup.8 --, --NR.sup.8 CO--, --NR.sup.8 --SO.sub.2 --, --OSO.sub.3 -- or --SO.sub.3 --;R.sup.8 is hydrogen, alkyl or alkyl bearing hydroxy or C.sub.1 to C.sub.4 alkoxy as a substituent;A is hydrogen, sodium, potassium, unsubstituted or substituted ammonium, unsubstituted or substituted alkyl, cycloalkyl, aralkyl or aryl; and--NR.sup.8 -- and A together may be an optionally quaternized saturated or unsaturated heterocyclic ring.The compounds are eminently suitable as optical brighteners for example for acrylonitrile polymers, wool and polyamides.

74. 发明授权

US3980713A Styryl compounds and process for producing the same 失效
标题翻译：苯乙烯基化合物及其制备方法
公开(公告)号：US3980713A
公开(公告)日：1976-09-14
申请号：US361127
申请日：1973-05-17
申请人： Daisaku Matsunaga , Mitsukuni Sumitani
发明人： Daisaku Matsunaga , Mitsukuni Sumitani
IPC分类号： C07C2/86 , C07C13/547 , C07C15/42 , C07C15/50 , C07C25/24 , C07C43/215 , C07C309/29 , C07C309/32 , C08K5/00 , C08K5/41 , C08L1/00 , C08L7/00 , C08L21/00 , C08L27/00 , C08L33/00 , C08L33/02 , C08L51/00 , C08L51/02 , C08L67/00 , C08L77/00 , C09B57/00 , D06L3/12 , D21H21/30 , C07C43/20
CPC分类号： C07C309/00 , C07C13/547 , C07C2/861 , C07C309/29 , C08K5/0041 , D21H21/30 , C07C2103/18
摘要： This invention relates to compounds which are valuable as a fluorescent brightener and a novel process for producing the same.The present invention is based on the following discoveries made by the inventors:In the presence of a palladium catalyst and a base at an elevated temperature, 1 mole of a compound of the formula,X--A--X (1)is reacted with 2 moles, in total, of one or two kinds of compounds selected from the group consisting of a styrene derivative having the formula, ##SPC1##And, thereby a compound of the formula, ##SPC2##Is obtained at a high yield, wherein, in the formula (1), X represents iodine or bromine, and A represents a bivalent radical selected from the group consisting of compounds of the formula, ##SPC3##And wherein, in the formula (2), R.sub.1 represents a substituent selected from the group consisting of hydrogen, chlorine, lower alkyl, methoxy, ethoxy, sulfonic acid radical or the salts thereof, sulfonamide radical, and lower-alkyl-substituted sulfonamide radical, and R.sub.2 represents a substituent selected from the group consisting of hydrogen, chlorine, lower alkyl, sulfonic acid radical or the salts thereof, sulfonamide radical and lower-alkyl-substituted sulfonamide radical, and wherein, in the formula (3), A represents the same as in the formula (1), R.sub.1 and R.sub.1 ' may be the same or different, each denoting the same as R.sub.1 in the formula (2); R.sub.2 and R.sub.2 ' may be the same or different, each denoting the same as R.sub.2 in the formula (2).
摘要翻译：本发明涉及作为荧光增白剂有价值的化合物及其生产方法。

75. 发明授权

US3956283A Bis-(triazinylamino)-stillene derivatives 失效
标题翻译：双 - （三嗪基氨基） - 茋衍生物
公开(公告)号：US3956283A
公开(公告)日：1976-05-11
申请号：US470523
申请日：1974-05-16
申请人： Fritz Fleck
发明人： Fritz Fleck
IPC分类号： C09B57/00 , C11D3/42 , D21H21/28 , D21H21/30 , C07D403/10
CPC分类号： D21H21/30 , C11D3/42 , Y10S8/918 , Y10S8/919
摘要： Disclosed are compounds of formula I, ##SPC1##in which R.sub.1 signifies hydrogen, fluorine, bromine, chlorine, C.sub.1-6 alkyl, C.sub.1-6 alkoxy or --SO.sub.3 M,R.sub.2 signifies cyano or --CONR.sub.3 R.sub.4,in which either R.sub.3 and R.sub.4, independently, each signify hydrogen, C.sub.1-6 alkyl or C.sub.2-6 hydroxyalkyl,Or R.sub.3 and R.sub.4, together with the nitrogen atom to which they are attached, signify a pyrrolidino, piperidino or morpholino ring, andM signifies hydrogen or a non-chromophoric cation,Their production and use as optical brightening agents, particularly for cellulosic substrates such as paper and cotton.
摘要翻译：公开了式I化合物，其中R 1表示氢，氟，溴，氯，C 1-6烷基，C 1-6烷氧基或-SO 3 M，R 2表示氰基或-CONR 3 R 4，其中R 3和R 4各自独立地表示氢， C 1-6烷基或C 2-6羟烷基，OR 3和R 4与它们所连接的氮原子一起表示吡咯烷子基，哌啶子基或吗啉代环，M表示氢或非发色阳离子。它们的生产和使用作为光学增亮剂，特别是作为纸和棉的纤维基材。

76. 发明授权

US3954740A Bis-s-triazinylamino-stilbene-2,2'-disulphonic acids, their manufacture and their use as optical brighteners 失效
标题翻译：双-S-三嗪基氨基 - 二苯乙烯-2,2（40-二磺酸，它们的制造及其作为荧光增白剂的用途
公开(公告)号：US3954740A
公开(公告)日：1976-05-04
申请号：US435785
申请日：1974-01-23
申请人： Werner Fringeli
发明人： Werner Fringeli
IPC分类号： D21H21/30 , C07D403/12
CPC分类号： D21H21/30
摘要： The present invention provides new bis-s-triazinylamino-stilbene-2,2'-disulphonic acids of the formula ##SPC1##And the alkali metal, alkaline earth metal, earth metal, ammonium or amine salt thereof.The new compounds are valuable optical brighteners, especially for whitening paper in combination with the surface finishing.
摘要翻译：本发明提供了式和碱金属，碱金属金属，地球金属，氨或其盐的新的双-s-三嗪基氨基 - 二苯乙烯-2,2'-二磺酸。

77. 发明授权

US3892675A Coating compositions 失效
标题翻译：涂料组合物
公开(公告)号：US3892675A
公开(公告)日：1975-07-01
申请号：US43062374
申请日：1974-01-04
申请人： ICI LTD
发明人： CLARKE WARWICK KINGSTON , KENYON RONALD WYNFORD , ROBINSON DAVID
IPC分类号： C09D131/04 , D21H19/44 , D21H19/60 , D21H21/30 , C09K1/00 , B44D5/00
CPC分类号： D21H21/30 , C09D131/04 , D21H19/60 , C08L2666/28 , C08L2666/54
摘要： The use of sparingly water-soluble optical brightening agents in coating compositions containing white pigment extender such as clay and polyvinyl acetate latex as sole binding agent enables coatings to be obtained on, e.g., paper of improved whiteness and fastness to light. Preferred optical brightening agents are heterocyclic, especially triazinyl derivatives of pyrene or naphthalene.
摘要翻译：含有白色颜料填充剂（如粘土和聚乙酸乙烯酯胶乳）作为唯一粘合剂的涂料组合物中使用少量水溶性荧光增白剂使得可以在例如改善的白度和耐光牢度的纸上获得涂层。优选的荧光增白剂是杂环的，特别是芘或萘的三嗪衍生物。

78. 发明授权

US3790443A Hydroxymethylamino nitrile salts for quenching the fluorescence of optical brightening agents 失效
标题翻译：羟基甲基氨基甲酸钠盐，用于染色光亮剂的荧光
公开(公告)号：US3790443A
公开(公告)日：1974-02-05
申请号：US3790443D
申请日：1972-04-27
申请人： REIF W , LAUDER R
发明人： REIF W , LAUDER R
IPC分类号： D21H21/30 , D21H3/52
CPC分类号： D21H21/30
摘要： A WATER SOLUBLY HYDROXYMETHYLAMINO NITRILE SALT IS APPLIED DIRECTLY AS A DRY POWDER TO PAPERMAKING MATERIALS TO QUENCH THE FLUORESCENCE OF OPTICAL BRIGHTENING AGENTS PRESENT IN THE PAPERMAKING MATERIALS.

79. 发明授权

US3773464A Acid and direct dyes and fluorescent brightener concentrates with thiocyanates and acetylinic alcohol 失效
标题翻译：酸和直接染料和荧光增白剂浓缩物与乙醇酸和乙醇溶液
公开(公告)号：US3773464A
公开(公告)日：1973-11-20
申请号：US3773464D
申请日：1970-06-02
申请人： GAF CORP
发明人： STRECK C
IPC分类号： C09B67/42 , D06P1/651 , D06P1/673 , D21H21/28 , D21H21/30 , D06P1/68
CPC分类号： C09B67/0071 , D06P1/65118 , D06P1/67375 , D21H21/28 , D21H21/30
摘要： Pourable, stable aqueous solutions to pastes consisting essentially of about 5-50% by weight of an acid dyestuff, a direct dyestuff or a flourescent brightening agent containing at least 1 sulfonic acid substituent and about 1-20% by weight of a water soluble thiocyanate such as ammonium thiocyanate. Such compositions are characterized by greater stability and fluidity and increased color value, as compared with a solution or paste, of the same concentration, of such dyestuffs but which do not contain a water soluble thiocyanate. The incorporation of a small amount, about 0.1-2% by weight, of an acetylenic glycol into such compositions, in the case of many dyestuffs further enhances the stability, fluidity and/or color value of the composition.
摘要翻译：基本上由约5-50重量％的酸性染料，直接染料或含有至少1个磺酸取代基的荧光增亮剂和约1-20重量％的水溶性硫氰酸酯组成的可浇注稳定的水溶液如硫氰酸铵。这种组合物的特征在于与相同浓度的这种染料但不含水溶性硫氰酸盐的溶液或糊状物相比，具有更大的稳定性和流动性以及增加的颜色值。在许多染料的情况下，向该组合物中加入少量约0.1-2重量％的炔属二醇进一步提高了组合物的稳定性，流动性和/或颜色值。

80. 发明授权

US3728275A Preparations containing concentrated aqueous asymmetrically substituted bis-triazinylaminostilbenes and the use of the preparations for optical brightening 失效
标题翻译：含有浓度浓度不均匀取代的双 - 三亚氨基甲酸酯的制剂和制备用于光学照射的用途
公开(公告)号：US3728275A
公开(公告)日：1973-04-17
申请号：US3728275D
申请日：1970-10-13
申请人： CIBA GEIGY CORP
发明人： HORLACHER P , CREUTZBURG G
IPC分类号： C11D3/42 , D06L3/12 , D21H21/30
CPC分类号： D21H21/30 , C11D3/42 , D06L4/65
摘要： MIXTURES OF NEW ASYMMETRICALLY SUBSTITUTED BIS-TRIAZINYLAMINOSTILBENES ARE OPTICAL BRIGHTENERS FOR ORGANIC MATERIALS. THE MIXTURES ARE PREPARED BY REACTING CYGANIC CHLORIDE WITH AN AMINOBENZENESULFONIC ACID, 4,4''-DIAMINOSTILBENE-2,2''-DISULFONIC ACID AND A MIXTURE OF A ISOMER MIXTURE OF DIMETHYLMORPHOLINESS AND DIETHANOLAMINE.

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