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71. 发明授权

US6066768A Perhalofluorinated butanes and hexanes 失效
标题翻译：全氟化丁烷和己烷
公开(公告)号：US6066768A
公开(公告)日：2000-05-23
申请号：US738117
申请日：1996-10-25
申请人： Mario Joseph Nappa , Allen Capron Sievert
发明人： Mario Joseph Nappa , Allen Capron Sievert
IPC分类号： B01J27/125 , C07C17/23 , C07C17/278 , C07C19/08 , C07C19/10 , C07C19/14
CPC分类号： C07C19/14 , B01J27/125 , C07C17/23 , C07C17/278 , C07C19/08 , C07C19/10
摘要： The instant invention relates to producing perhalofluorobutanes and perhalofluorohexanes, more particularly it relates to their production by utilizing tetrafluoroethylene (hereinafter referred to as "TFE") and chlorotrifluoro-ethylene (hereinafter referred to as "CTFE") with selected perhalofluoroethanes containing 2 to 4 nonfluorine halogen and 2 to 4 fluorine substituents in the presence of a polyvalent metal halide such as an aluminum chloride or chlorofluoride as catalyst.
摘要翻译：本发明涉及生产全氟全氟代丁烷和全卤代己烷，更具体地说，涉及其使用四氟乙烯（以下称为“TFE”）和氯三氟乙烯（以下称为“CTFE”）的制备方法，该选择性全卤代乙烷含有2-4个非氟卤素和2至4个氟取代基在多价金属卤化物如氯化铝或氯氟化物作为催化剂存在下进行。

72. 发明授权

US5770779A Process for preparation of fluorinated hydrocarbons 失效
标题翻译：氟化烃的制备方法
公开(公告)号：US5770779A
公开(公告)日：1998-06-23
申请号：US778427
申请日：1997-01-02
申请人： Mario Joseph Nappa , William Robert Williams
发明人： Mario Joseph Nappa , William Robert Williams
IPC分类号： B01J27/10 , C07B61/00 , C07C17/20 , C07C17/21 , C07C19/08 , C07C17/08
CPC分类号： C07C17/206 , C07C17/21
摘要： This invention is a process for the selective preparation of fluorinated hydrocarbons from chlorinated hydrocarbons while minimizing formation of oligomeric and polymeric byproducts. The process comprises providing a liquid phase containing chlorinated hydrocarbon, HF, a tin catalyst, and at least one compound selected from the group consisting of metal and nonmetal alkoxides, and heating the mixture and isolating the fluorinated hydrocarbon formed.
摘要翻译：本发明是一种从氯化烃中选择性制备氟化烃的方法，同时最小化低聚物和聚合副产物的形成。该方法包括提供含有氯化烃，HF，锡催化剂和至少一种选自金属和非金属醇盐的化合物的液相，并加热混合物并分离形成的氟化烃。

73. 发明授权

US08877086B2 Compositions comprising 2,3-dichloro-1,1,1-trifluoropropane, 2-chloro-1,1,1-trifluoropropene, 2-chloro-1,1,1,2-tetrafluoropropane or 2,3,3,3-tetrafluoropropene 有权
标题翻译：包含2,3-二氯-1,1,1-三氟丙烷，2-氯-1,1,1-三氟丙烯，2-氯-1,1,1,2-四氟丙烷或2,3,3,3-四氯丙烷的组合物，四氟丙烯
公开(公告)号：US08877086B2
公开(公告)日：2014-11-04
申请号：US12937661
申请日：2009-05-07
申请人： Barry Asher Mahler , Mario Joseph Nappa
发明人： Barry Asher Mahler , Mario Joseph Nappa
IPC分类号： C09K5/04 , F25D3/10 , C07C21/04 , C07C19/10 , C07C17/04 , C08J9/14 , C07C19/12 , C07C21/18 , C07C17/20 , C09K3/30 , C07C19/08 , C07C17/087 , C07C17/25
CPC分类号： C09K5/044 , A62D1/0028 , A62D1/0057 , A62D1/0092 , B01F17/0035 , B01F17/0085 , C07C17/04 , C07C17/087 , C07C17/204 , C07C17/206 , C07C17/23 , C07C17/25 , C07C19/08 , C07C19/10 , C07C19/12 , C07C21/04 , C07C21/18 , C08J9/144 , C08J9/146 , C08J9/149 , C08J2203/14 , C08J2203/142 , C08J2203/144 , C08J2203/164 , C09K3/00 , C09K3/30 , C09K5/045 , C09K5/048 , C09K21/08 , C09K2205/12 , C09K2205/122 , C09K2205/126 , C09K2205/22 , C11D7/30 , H01B3/56
摘要： Disclosed are compositions comprising HCFC-243db, HCFO-1233xf, HCFC-244db and/or HFO-1234yf and at least one additional compound. For the composition comprising 1234yf, the additional compound is selected from the group consisting of HFO-1234ze, HFO-1243zf, HCFC-243db, HCFC-244db, HFC-245cb, HFC-245fa, HCFO-1233xf, HCFO-1233zd, HCFC-253fb, HCFC-234ab, HCFC-243fa, ethylene, HFC-23, CFC-13, HFC-143a, HFC-152a, HFC-236fa, HCO-1130, HCO-1130a, HFO-1336, HCFC-133a, HCFC-254fb, HCFC-1131, HFO-1141, HCFO-1242zf, HCFO-1223xd, HCFC-233ab, HCFC-226ba, and HFC-227ca. Compositions comprising HCFC-243db, HCFO-1233xf, and/or HCFC-244db are useful in processes to make HFO-1234yf. Compositions comprising HFO-1234yf are useful, among other uses, as heat transfer compositions for use in refrigeration, air-conditioning and heat pump systems.
摘要翻译：公开了包含HCFC-243db，HCFO-1233xf，HCFC-244db和/或HFO-1234yf和至少一种另外的化合物的组合物。对于包含1234yf的组合物，附加化合物选自HFO-1234ze，HFO-1243zf，HCFC-243db，HCFC-244db，HFC-245cb，HFC-245fa，HCFO-1233xf，HCFO-1233zd，HCFC- 253fb，HCFC-234ab，HCFC-243fa，乙烯，HFC-23，CFC-13，HFC-143a，HFC-152a，HFC-236fa，HCO-1130，HCO-1130a，HFO-1336，HCFC-133a， 254fb，HCFC-1131，HFO-1141，HCFO-1242zf，HCFO-1223xd，HCFC-233ab，HCFC-226ba和HFC-227ca。包含HCFC-243db，HCFO-1233xf和/或HCFC-244db的组合物可用于制备HFO-1234yf的方法。包括HFO-1234yf的组合物在其它用途中可用作用于制冷，空调和热泵系统的热传递组合物。

74. 发明授权

US08853472B2 Processes for reducing the amount of monofluoroacetate in hydrofluoroolefin production 有权
标题翻译：减少氢氟烯烃生产中一氟乙酸盐的用量的方法
公开(公告)号：US08853472B2
公开(公告)日：2014-10-07
申请号：US13318557
申请日：2010-05-07
申请人： Mario Joseph Nappa , Patricia Cheung , Karl R. Krause , Michael A. Sisk
发明人： Mario Joseph Nappa , Patricia Cheung , Karl R. Krause , Michael A. Sisk
IPC分类号： C07C17/38 , C07C17/25
CPC分类号： C07C17/25 , C07C21/18
摘要： A process is disclosed for reducing the amount of monofluoroacetate. The process involves (a) contacting a hydrofluorocarbon with a reactant basic aqueous solution to produce an organic phase solution containing a hydrofluoroolefin and an aqueous phase solution containing a monofluoroacetate; and (b) heating the aqueous phase solution to an effective temperature to reduce the amount of monofluoroacetate in the aqueous phase solution, wherein fluoride concentration in the aqueous phase solution is substantially high. Another process is disclosed for reducing the amount of monofluoroacetate. The process involves (a) contacting a first batch of hydrofluorocarbon with a first batch of reactant basic aqueous solution to produce a first batch of organic phase solution containing a hydrofluoroolefin and a first batch of aqueous phase solution containing a monofluoroacetate; (b) separating the first batch of organic phase solution from the first batch of aqueous phase solution; (c) mixing a second batch of hydrofluorocarbon and a second batch of reactant basic aqueous solution with the separated first batch of organic phase solution to produce a second batch of organic phase solution containing a hydrofluoroolefin and a second batch of aqueous phase solution containing a monofluoroacetate; (d) combining the first batch of aqueous phase solution with the second batch of aqueous phase solution; and (e) heating the combined aqueous phase solutions to an effective temperature to reduce the amount of monofluoroacetate in the combined aqueous phase solutions, wherein fluoride concentration in the combined aqueous phase solutions is substantially high.
摘要翻译：公开了一种减少一氟乙酸盐的量的方法。该方法包括（a）使氢氟烃与反应性碱性水溶液接触以产生含有氢氟烯烃和含有一氟乙酸盐的水相溶液的有机相溶液; 和（b）将水相溶液加热到有效温度以降低水相溶液中的一氟乙酸盐的量，其中水相溶液中的氟化物浓度基本上高。公开了用于减少一氟乙酸盐的量的另一种方法。该方法包括（a）使第一批氢氟烃与第一批反应性碱性水溶液接触，以产生含有氢氟烯烃和含有一氟乙酸盐的第一批含水相溶液的第一批有机相溶液; （b）从第一批水相溶液中分离出第一批有机相溶液; （c）将第二批氢氟烃和第二批反应性碱性水溶液与分离的第一批有机相溶液混合以产生含有氢氟烯烃的第二批有机相溶液和含有一氟乙酸盐的第二批含水相溶液 ; （d）将第一批水相溶液与第二批水相溶液组合; 和（e）将组合的水相溶液加热到有效温度以减少组合的水相溶液中的一氟乙酸盐的量，其中组合的水相溶液中的氟化物浓度基本上高。

75. 发明授权

US08663494B2 Terpene, terpenoid, and fullerene stabilizers for fluoroolefins 有权
标题翻译：萜烯，萜烯和氟烯烃的富勒烯稳定剂
公开(公告)号：US08663494B2
公开(公告)日：2014-03-04
申请号：US13325966
申请日：2011-12-14
申请人： Jon Lee Howell , Velliyur Nott Mallikarjuna Rao , Thomas J. Leck , Barbara Haviland Minor , Mario Joseph Nappa , Nandini C. Mouli , Ekaterina N. Swearingen , Andrew Edward Feiring
发明人： Jon Lee Howell , Velliyur Nott Mallikarjuna Rao , Thomas J. Leck , Barbara Haviland Minor , Mario Joseph Nappa , Nandini C. Mouli , Ekaterina N. Swearingen , Andrew Edward Feiring
IPC分类号： C09K5/04
CPC分类号： C09K5/045 , C09K2205/126
摘要： The present invention relates to compositions comprising at least one fluoroolefin and an effective amount of stabilizer that may be a terpene, terpenoid or fullerene; or a mixture of a terpene, terpenoid or fullerene with other stabilizers. The stabilized compositions may be useful in cooling apparatus, such as refrigeration, air-conditioning, chillers, and heat pumps, as well as in applications as foam blowing agents, solvents, aerosol propellants, fire extinguishants, and sterilants.
摘要翻译：本发明涉及包含至少一种氟烯烃和有效量的可以是萜烯，萜烯或富勒烯的稳定剂的组合物; 或萜烯，萜烯或富勒烯与其他稳定剂的混合物。稳定的组合物可用于冷却装置，例如制冷，空调，冷却器和热泵，以及作为泡沫发泡剂，溶剂，气溶胶推进剂，灭火剂和灭菌剂的应用。

76. 发明申请

US20140058141A1 CATALYTICAL SYNTHESIS OF HYDROHALOCARBONS 有权
标题翻译：氢氟碳酸盐的催化合成
公开(公告)号：US20140058141A1
公开(公告)日：2014-02-27
申请号：US13988121
申请日：2011-11-07
申请人： Mario Joseph Nappa , Ekaterinan N. Swearingen , Sergei Rafailovich Sterlin
发明人： Mario Joseph Nappa , Ekaterinan N. Swearingen , Sergei Rafailovich Sterlin
IPC分类号： C07C17/278
CPC分类号： C07C17/278 , C07C17/383 , C07C19/10
摘要： A process is disclosed for producing addition compound CF3CCl2CH2CClXR, wherein X=H, F, Cl or Br, and R=H or a perhalogenated alkyl group, provided that X and R are not both H. The process involves a liquid phase reaction of 1,1,1-trichlorotrifluoroethane with CH2═CXR in the presence of an addition catalyst.
摘要翻译：公开了制备加成化合物CF 3 CCl 2 CH 2 ClClR的方法，其中X = H，F，Cl或Br，以及R = H或全卤代烷基，条件是X和R不同时为H.该方法涉及1相的液相反应，在加成催化剂存在下，使用CH 2 = CXR的1,1-三氯三氟乙烷。

77. 发明授权

US08558040B2 Methods for making foams using blowing agents comprising unsaturated fluorocarbons 有权
标题翻译：使用包含不饱和碳氟化合物的发泡剂制备泡沫的方法
公开(公告)号：US08558040B2
公开(公告)日：2013-10-15
申请号：US11591349
申请日：2006-11-01
申请人： Joseph Anthony Creazzo , Mario Joseph Nappa , Allen Capron Sievert , Ekaterina N. Swearingen
发明人： Joseph Anthony Creazzo , Mario Joseph Nappa , Allen Capron Sievert , Ekaterina N. Swearingen
IPC分类号： C07C21/18
CPC分类号： C08J9/146 , B01F17/0085 , C03C23/0075 , C07C21/18 , C08G18/4208 , C08G18/4883 , C08G2101/0025 , C08J9/0019 , C08J9/144 , C08J2205/05 , C08J2205/052 , C08J2325/06 , C08J2375/06 , C08J2375/08 , C10M105/52 , C10M107/38 , C10M147/04 , C10M169/04 , C10M169/041 , C10M177/00 , C10M2211/022 , C10M2211/06 , C10M2213/04 , C10M2213/06 , C10N2230/06 , C10N2230/22 , C10N2240/20 , C10N2240/204 , C10N2250/121 , C10N2270/00 , C11D3/245 , C11D3/43 , C11D7/5018 , C11D11/0023 , C11D11/0029 , C11D11/0035 , C11D11/0047 , C23G5/02803 , C23G5/02825 , G11B5/71 , G11B5/725 , G11B5/8408 , G11B23/505
摘要： Disclosed herein are blowing agents comprising fluorocarbons and/or hydrofluorocarbons useful in foamable compositions. Also disclosed are methods for forming a foam comprising the aforementioned blowing agents.
摘要翻译：本文公开了包含可用于可发泡组合物的碳氟化合物和/或氢氟烃的发泡剂。还公开了形成包含上述发泡剂的泡沫体的方法。

78. 发明授权

US08425795B2 Compositions comprising fluoroolefins and uses thereof 有权
标题翻译：包含氟烯烃的组合物及其用途
公开(公告)号：US08425795B2
公开(公告)日：2013-04-23
申请号：US13286765
申请日：2011-11-01
申请人： Mario Joseph Nappa , Barbara Haviland Minor , Allen Capron Sievert
发明人： Mario Joseph Nappa , Barbara Haviland Minor , Allen Capron Sievert
IPC分类号： C09K5/04
CPC分类号： C09K5/045 , C07C21/18 , C09K5/04 , C09K2205/126 , C09K2205/22 , C09K2205/40 , F25B1/00 , F25B30/02 , F25B31/002 , F25B39/00 , F25B39/02 , F25B45/00 , F25B2400/12 , F25B2400/121
摘要： The present invention relates to fluoroolefin compositions. The fluoroolefin compositions of the present invention are useful as refrigerants or heat transfer fluids and in processes for producing cooling or heat. Additionally, the fluoroolefin compositions of the present invention may be used to replace currently used refrigerant or heat transfer fluid compositions that have higher global warming potential.
摘要翻译：本发明涉及氟烯烃组合物。本发明的氟代烯烃组合物可用作制冷剂或传热流体以及用于生产冷却或加热的方法。另外，本发明的氟代烯烃组合物可用于替代目前使用的具有较高全球变暖潜能的制冷剂或传热流体组合物。

79. 发明授权

US08383004B2 Amine stabilizers for fluoroolefins 失效
标题翻译：氟烯烃的胺稳定剂
公开(公告)号：US08383004B2
公开(公告)日：2013-02-26
申请号：US12377485
申请日：2007-08-31
申请人： Nandini C. Mouli , Barbara Haviland Minor , Mario Joseph Nappa , Thomas J. Leck
发明人： Nandini C. Mouli , Barbara Haviland Minor , Mario Joseph Nappa , Thomas J. Leck
IPC分类号： C09K5/04
CPC分类号： C09K5/045 , C09K2205/126
摘要： The present invention relates to compositions comprising at least one fluoroolefin and an effective amount of stabilizer that may be an amine or a mixture of an amine with other stabilizers. The stabilized compositions may be useful in cooling apparatus, such as refrigeration, air-conditioning, chillers, and heat pumps, as well as in applications as foam blowing agents, solvents, aerosol propellants, fire extinguishants, and sterilants.
摘要翻译：本发明涉及包含至少一种氟烯烃和有效量的稳定剂的组合物，其可以是胺或胺与其它稳定剂的混合物。稳定的组合物可用于冷却装置，例如制冷，空调，冷却器和热泵，以及作为泡沫发泡剂，溶剂，气溶胶推进剂，灭火剂和灭菌剂的应用。

80. 发明授权

US08377327B2 Tetrafluoropropene production processes 有权
标题翻译：四氟丙烯生产工艺
公开(公告)号：US08377327B2
公开(公告)日：2013-02-19
申请号：US12758839
申请日：2010-04-13
申请人： Velliyur Nott Mallikarjuna Rao , Mario Joseph Nappa , Allen Capron Sievert , Ralph Newton Miller
发明人： Velliyur Nott Mallikarjuna Rao , Mario Joseph Nappa , Allen Capron Sievert , Ralph Newton Miller
IPC分类号： C09K5/04
CPC分类号： C07C21/18 , C07B2200/09 , C07C17/25
摘要： A process is disclosed for the manufacture of CF3CF═CH2 and CF3CH═CHF. The process involves dehydrofluorinating CF3CHFCH2F in the presence of a dehydrofluorination catalyst to produce a product mixture comprising CF3CF═CH2 and CF3CH═CHF, and recovering said CF3CF═CH2 and CF3CH═CHF from the product mixture. The present invention also provides a composition comprising (a) the Z-isomer of CF3CH═CHF and (b) HF; wherein the HF is present in an effective amount to form an azeotropic combination with the Z—CF3CH═CHF.
摘要翻译：公开了用于制造CF 3CF≡CH2和CF 3 CH = CHF的方法。该方法包括在脱氟化氢催化剂存在下对CF 3 CHFCH 2 F进行脱氟化氢，以产生包含CF 3CF≡CH2和CF 3 CH = CHF的产物混合物，并从产物混合物中回收所述CF 3CF≡CH2和CF 3 CH = CHF。本发明还提供了包含（a）CF 3 CH = CHF的Z-异构体和（b）HF的组合物; 其中HF以有效量存在以与Z-CF 3 CH = CHF形成共沸组合。

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